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Preparation and Characterization of NiO Nanoparticles via Solid-State Thermal Decomposition of Ni(II) Complex

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Abstract

Nickel(II) complex, Ni(Brsalph)(NO3) was synthesized and characterized by elemental analyses and Fourier-transformed infrared (FT-IR) spectroscopy. Heating of Ni(Brsalph)(NO3) at 550 °C for 3.5 h have resulted NiO nanoparticles. Fourier-transformed infrared spectrum confirmed the composition of products. The crystalline structures and morphology of NiO nanoparticles were studied by X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy.

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Acknowledgments

I am grateful to the Council of Iran National Science Foundation and Golestan University for financial support of this work.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran

    Aliakbar Dehno Khalaji

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  1. Aliakbar Dehno Khalaji
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Correspondence to Aliakbar Dehno Khalaji.

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Dehno Khalaji, A. Preparation and Characterization of NiO Nanoparticles via Solid-State Thermal Decomposition of Ni(II) Complex. J Clust Sci 24, 189–195 (2013). https://doi.org/10.1007/s10876-012-0542-3

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  • DOI: https://doi.org/10.1007/s10876-012-0542-3

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