Abstract
The growth of silver bromide nanoparticles on silk yarn was achieved by sequential dipping in alternating bath of potassium bromide and silver nitrate under ultrasound irradiation. The effect of concentration, power of ultrasound irradiation and the numerous of sequential dipping steps in growth of the AgBr nanoparticles on silk yarn were studied. The samples were characterized with powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and Inductive Coupled Plasma (ICP). The lower average size and the higher crowded AgBr nanoparticles upon silk yarn are the result of using ultrasound irradiation.
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W. Hu, S. Chen, X. Li, S. Shi, W. Shen, X. Zhang, H. Wang, In situ synthesis of silver chloride nanoparticles into bacterial cellulose membranes. Mater. Sci. Eng. C 29, 1216–1219 (2009)
H. Tan, W.Y. Fan, Laser-based synthesis of core Ag-shell AgI nanoparticles. Chem. Phys. Lett. 406, 289–293 (2005)
H.J. Lee, S.Y. Yeo, S.H. Jeong, Antibacterial effect of nanosized silver colloidal solution on textile fabrics. J. Mater. Sci. 38, 2199–2204 (2003)
I. Perelshtein, G. Applerot, N. Perkas, E. Wehrschuetz-Sigl, A. Hasmann, G. Guebitz, A. Gedanken, CuO–cotton nanocomposite: formation, morphology, and antibacterial activity. Surf. Coat. Technol. 204, 54–57 (2009)
J. Bai, Y. Li, M. Li, S. Wang, C. Zhang, Q. Yang, Electrospinning method for the preparation of silver chloride nanoparticles in PVP nanofiber. Appl. Surf. Sci. 254, 4520–4523 (2008)
J.P. Tiwari, R.K. Rao, Template synthesized high conducting silver chloride nanoplates. Solid State Ion. 179, 299–304 (2008)
M.M. Husein, E. Rodil, J.H. Vera, A novel method for the preparation of silver chloride nanoparticles starting from their solid powder using microemulsions. J. Colloid Interface Sci. 288, 457–467 (2005)
M. Husein, E. Rodil, J.H. Vera, Formation of silver bromide precipitate of nanoparticles in a single microemulsion utilizing the surfactant counterion. J. Colloid Interface Sci. 273, 426–434 (2004)
M.G. Spirin, S.B. Brichkin, V.F. Razumov, Growth kinetics for AgI nanoparticles in AOT reverse micelles: effect of molecular length of hydrocarbon solvents. J. Colloid Interface Sci. 326, 117–120 (2008)
L. Zhao, Y. Wang, Z. Chen, Y. Zou, Preparation, characterization, and optical properties of host–guest nanocomposite material SBA-15/AgI. J. Phys. B 403, 1775–1780 (2008)
I.L. Validzic, V. Jokanovic, D.P. Uskokovi, J.M. Nedeljkovi, Influence of solvent on the structural and morphological properties of AgI particles prepared using ultrasonic spray pyrolysis. Mater. Chem. Phys. 107, 28–32 (2008)
N. Perkas, Y. Wang, Y. Koltypin, A. Gedanken, S. Chandrasekaran, Mesoporous iron–titania catalyst for cyclohexane oxidation. Chem. Commun. 988–989 (2001)
M.V. Landau, L. Vradman, M. Herskowitz, Y. Koltypin, A. Gedanken, Ultrasonically controlled deposition–precipitation: Co–Mo HDS catalysts deposited on wide-pore MCM material. J. Catal. 201, 22–36 (2001)
K.S. Suslick, Sonochemistry. Science 247, 1439–1445 (1990)
K.H. Kim, K.B. Kim, Ultrasound assisted synthesis of nano-sized lithium cobalt oxide. Ultrason. Sonochem. 15, 1019–1025 (2008)
I.L. Validzic, I.A. Jankovic, M. Mitric, N. Bibic, J.M. Nedeljkovic, Growth and quantum confinement in AgI nanowires. Mater. Lett. 61, 3522–3525 (2007)
P. Potiyaraj, P. Kumlangdudsana, S.T. Dubas, Synthesis of silver chloride nanocrystal on silk fibers. Mater. Lett. 61, 2464–2466 (2007)
M.A. Alavi, A. Morsali, Syntheses and characterization of Mg(OH)2 and MgO nanostructures by ultrasonic method. Ultrason. Sonochem. 17, 441–446 (2010)
K.S. Suslick, D.A. Hammerton, R.E. Cline, Sonochemical hot spot. J. Am. Chem. Soc. 108, 5641–5642 (1986)
M.W. Grinstaff, A.A. Cichowlas, S.B. Choe, K.S. Suslick, Effect of cavitation conditions on amorphous metal synthesis. Ultrasonics 30, 168–172 (1992)
A. Morsali, H.H. Monfared, A. Morsali, Synthesis and characterization of Mn3O4 nanoparticles via thermal decomposition of a new synthesized hydrogen bonded polymer. J. Mol. Struct. 938, 10–14 (2009)
J. Yang, C. Lin, Zh. Wang, J. Lin, In(OH)3 and In2O3 nanorod bundles and spheres: microemulsion-mediated hydrothermal synthesis and luminescence properties. Inorg. Chem. 45, 8973–8979 (2006)
A. Askarinejad, A. Morsali, Synthesis and characterization of mercury oxide unusual nanostructures by ultrasonic method. Chem. Eng. J. 153, 183–186 (2009)
M.A. Alavi, A. Morsali, Syntheses of BaCO3 nanostructures by ultrasonic method. Ultrason. Sonochem. 15, 833–838 (2008)
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Support of this investigation by Tarbiat Modares University and Iran Water Resources Management Co. are gratefully acknowledged.
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Abbasi, A.R., Morsali, A. Synthesis and Characterization of AgBr–Silk Nanocomposite Under Ultrasound Irradiation. J Inorg Organomet Polym 20, 825–832 (2010). https://doi.org/10.1007/s10904-010-9408-z
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DOI: https://doi.org/10.1007/s10904-010-9408-z