Skip to main content
Log in

Synthesis and Characterization of AgBr–Silk Nanocomposite Under Ultrasound Irradiation

  • Published:
Journal of Inorganic and Organometallic Polymers and Materials Aims and scope Submit manuscript

Abstract

The growth of silver bromide nanoparticles on silk yarn was achieved by sequential dipping in alternating bath of potassium bromide and silver nitrate under ultrasound irradiation. The effect of concentration, power of ultrasound irradiation and the numerous of sequential dipping steps in growth of the AgBr nanoparticles on silk yarn were studied. The samples were characterized with powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and Inductive Coupled Plasma (ICP). The lower average size and the higher crowded AgBr nanoparticles upon silk yarn are the result of using ultrasound irradiation.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. W. Hu, S. Chen, X. Li, S. Shi, W. Shen, X. Zhang, H. Wang, In situ synthesis of silver chloride nanoparticles into bacterial cellulose membranes. Mater. Sci. Eng. C 29, 1216–1219 (2009)

    Article  CAS  Google Scholar 

  2. H. Tan, W.Y. Fan, Laser-based synthesis of core Ag-shell AgI nanoparticles. Chem. Phys. Lett. 406, 289–293 (2005)

    Article  CAS  Google Scholar 

  3. H.J. Lee, S.Y. Yeo, S.H. Jeong, Antibacterial effect of nanosized silver colloidal solution on textile fabrics. J. Mater. Sci. 38, 2199–2204 (2003)

    Article  CAS  Google Scholar 

  4. I. Perelshtein, G. Applerot, N. Perkas, E. Wehrschuetz-Sigl, A. Hasmann, G. Guebitz, A. Gedanken, CuO–cotton nanocomposite: formation, morphology, and antibacterial activity. Surf. Coat. Technol. 204, 54–57 (2009)

    Article  CAS  Google Scholar 

  5. J. Bai, Y. Li, M. Li, S. Wang, C. Zhang, Q. Yang, Electrospinning method for the preparation of silver chloride nanoparticles in PVP nanofiber. Appl. Surf. Sci. 254, 4520–4523 (2008)

    Article  CAS  Google Scholar 

  6. J.P. Tiwari, R.K. Rao, Template synthesized high conducting silver chloride nanoplates. Solid State Ion. 179, 299–304 (2008)

    Article  CAS  Google Scholar 

  7. M.M. Husein, E. Rodil, J.H. Vera, A novel method for the preparation of silver chloride nanoparticles starting from their solid powder using microemulsions. J. Colloid Interface Sci. 288, 457–467 (2005)

    Article  CAS  Google Scholar 

  8. M. Husein, E. Rodil, J.H. Vera, Formation of silver bromide precipitate of nanoparticles in a single microemulsion utilizing the surfactant counterion. J. Colloid Interface Sci. 273, 426–434 (2004)

    Article  CAS  Google Scholar 

  9. M.G. Spirin, S.B. Brichkin, V.F. Razumov, Growth kinetics for AgI nanoparticles in AOT reverse micelles: effect of molecular length of hydrocarbon solvents. J. Colloid Interface Sci. 326, 117–120 (2008)

    Article  CAS  Google Scholar 

  10. L. Zhao, Y. Wang, Z. Chen, Y. Zou, Preparation, characterization, and optical properties of host–guest nanocomposite material SBA-15/AgI. J. Phys. B 403, 1775–1780 (2008)

    Article  CAS  Google Scholar 

  11. I.L. Validzic, V. Jokanovic, D.P. Uskokovi, J.M. Nedeljkovi, Influence of solvent on the structural and morphological properties of AgI particles prepared using ultrasonic spray pyrolysis. Mater. Chem. Phys. 107, 28–32 (2008)

    Article  Google Scholar 

  12. N. Perkas, Y. Wang, Y. Koltypin, A. Gedanken, S. Chandrasekaran, Mesoporous iron–titania catalyst for cyclohexane oxidation. Chem. Commun. 988–989 (2001)

  13. M.V. Landau, L. Vradman, M. Herskowitz, Y. Koltypin, A. Gedanken, Ultrasonically controlled deposition–precipitation: Co–Mo HDS catalysts deposited on wide-pore MCM material. J. Catal. 201, 22–36 (2001)

    Article  CAS  Google Scholar 

  14. K.S. Suslick, Sonochemistry. Science 247, 1439–1445 (1990)

    Article  CAS  Google Scholar 

  15. K.H. Kim, K.B. Kim, Ultrasound assisted synthesis of nano-sized lithium cobalt oxide. Ultrason. Sonochem. 15, 1019–1025 (2008)

    Article  CAS  Google Scholar 

  16. I.L. Validzic, I.A. Jankovic, M. Mitric, N. Bibic, J.M. Nedeljkovic, Growth and quantum confinement in AgI nanowires. Mater. Lett. 61, 3522–3525 (2007)

    Article  CAS  Google Scholar 

  17. P. Potiyaraj, P. Kumlangdudsana, S.T. Dubas, Synthesis of silver chloride nanocrystal on silk fibers. Mater. Lett. 61, 2464–2466 (2007)

    Article  CAS  Google Scholar 

  18. M.A. Alavi, A. Morsali, Syntheses and characterization of Mg(OH)2 and MgO nanostructures by ultrasonic method. Ultrason. Sonochem. 17, 441–446 (2010)

    Article  CAS  Google Scholar 

  19. K.S. Suslick, D.A. Hammerton, R.E. Cline, Sonochemical hot spot. J. Am. Chem. Soc. 108, 5641–5642 (1986)

    Article  CAS  Google Scholar 

  20. M.W. Grinstaff, A.A. Cichowlas, S.B. Choe, K.S. Suslick, Effect of cavitation conditions on amorphous metal synthesis. Ultrasonics 30, 168–172 (1992)

    Article  CAS  Google Scholar 

  21. A. Morsali, H.H. Monfared, A. Morsali, Synthesis and characterization of Mn3O4 nanoparticles via thermal decomposition of a new synthesized hydrogen bonded polymer. J. Mol. Struct. 938, 10–14 (2009)

    Article  CAS  Google Scholar 

  22. J. Yang, C. Lin, Zh. Wang, J. Lin, In(OH)3 and In2O3 nanorod bundles and spheres: microemulsion-mediated hydrothermal synthesis and luminescence properties. Inorg. Chem. 45, 8973–8979 (2006)

    Article  CAS  Google Scholar 

  23. A. Askarinejad, A. Morsali, Synthesis and characterization of mercury oxide unusual nanostructures by ultrasonic method. Chem. Eng. J. 153, 183–186 (2009)

    Article  CAS  Google Scholar 

  24. M.A. Alavi, A. Morsali, Syntheses of BaCO3 nanostructures by ultrasonic method. Ultrason. Sonochem. 15, 833–838 (2008)

    CAS  Google Scholar 

Download references

Acknowledgments

Support of this investigation by Tarbiat Modares University and Iran Water Resources Management Co. are gratefully acknowledged.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Ali Morsali.

Electronic supplementary material

Below is the link to the electronic supplementary material.

Supplementary material 1 (DOC 241 kb)

Rights and permissions

Reprints and permissions

About this article

Cite this article

Abbasi, A.R., Morsali, A. Synthesis and Characterization of AgBr–Silk Nanocomposite Under Ultrasound Irradiation. J Inorg Organomet Polym 20, 825–832 (2010). https://doi.org/10.1007/s10904-010-9408-z

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10904-010-9408-z

Keywords

Navigation