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Simple One-Pot Preparation of In2O3 Nano-particles Using a Supramolecular 3D Framework Polymer

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Abstract

An indium(III) three-dimensional coordination framework, [In2(OH)3(O4C8H4)1.5] n (1), was synthesized by hydrothermal method and characterized by elemental analyses, X-ray powder diffraction (XRD) and IR spectroscopy. Indium(III) oxide nanoparticles was prepared by direct thermal decomposition of 1 at 450 °C in air. The indium(III) oxide nanoparticles were characterized by scanning electron microscopy, X-ray powder diffraction (XRD) and energy-dispersive X-ray analysis (EDAX). This study demonstrates the coordination polymer frameworks may be suitable precursors for a simple one-pot preparation of nanoscale metal oxide materials with different and interesting morphologies.

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References

  1. H.T. Shi, L.M. Qi, J.M. Ma, H.M. Cheng, J. Am. Chem. Soc. 125, 3450–3451 (2003)

    Article  CAS  Google Scholar 

  2. H. Zhang, D.R. Yang, D.S. Li, X.Y. Ma, S.Z. Li, D.L. Que, Cryst. Growth Des. 5, 547–550 (2005)

    Article  CAS  Google Scholar 

  3. D.B. Kuang, A.W. Xu, Y.P. Fang, H.Q. Liu, C. Frommen, D. Fenske, Adv. Mater. 15, 1747–1750 (2003)

    Article  CAS  Google Scholar 

  4. L.X. Zhang, Y.C. Zhang, M. Zhang, Mater. Lett. 64, 966–968 (2010)

    Article  CAS  Google Scholar 

  5. K.K. Makhiga, A. Ray, R.M. Patel, U.B. Trivedi, H.N. Kapse, Bull. Mater. Sci. 28, 9–17 (2005)

    Article  Google Scholar 

  6. G. Neri, A. Bonavita, G. Micali, G. Rizzo, E. Callone, G. Carturan, Sens. Actuators B 132, 224–233 (2008)

    Article  Google Scholar 

  7. H. Steffes, C. Imawan, F. Solzbacher, E. Obermeier, Sens. Actuators B 68, 249–253 (2000)

    Article  Google Scholar 

  8. M. Ivanovskaya, A. Gurlo, P. Bogdanov, Sens. Actuators B 77, 264–367 (2001)

    Article  Google Scholar 

  9. E. Comini, A. Cristalli, G. Faglia, G. Sberveglieri, Sens. Actuators B 65, 260–263 (2000)

    Article  Google Scholar 

  10. M. Epifani, E. Comini, J. Arbiol, R. Díaz, N. Sergent, T. Pagnier, J.R. Morante et al., Sens. Actuators B Chem. 130, 483–487 (2008)

    Article  Google Scholar 

  11. A. Vomiero, S. Bianchi, E. Comini, G. Faglia, M. Ferroni, N. Poli et al., Thin Solid Films 515, 8356–8359 (2007)

    Article  CAS  Google Scholar 

  12. J. Kim, J. Park, K. Kim, C. Kim, H. Jang, Curr. Appl. Phys. 6, e198–e201 (2006)

    Google Scholar 

  13. Z. Cheng, X. Dong, Q. Pan, J. Zhang, X. Dong, Mater. Lett. 60, 3137–3140 (2006)

    Article  CAS  Google Scholar 

  14. H. Yang, Z. Yang, H. Liang, L. Liu, J. Guo, Y. Yang, Mater. Lett. 64, 1418–1420 (2010)

    Article  CAS  Google Scholar 

  15. Y. Zhang, H. Ago, J. Liu, M. Yumura, K. Uchida, S. Ohshima, J. Zhu, X. Zhang et al., J. Cryst. Growth 264, 363–368 (2004)

    Article  CAS  Google Scholar 

  16. Q. Wang, K. Yu, F. Xu, J. Wu, Y. Xu, Z. Zhu, Mater. Lett. 62, 2710–2713 (2008)

    Article  CAS  Google Scholar 

  17. H. Yang, H. Zhao, H. Dong, W. Yang, D. Chen, Mater. Res. Bull. 44, 1148–1153 (2009)

    Article  CAS  Google Scholar 

  18. Y. Liu, W. Yang, D. Hou, Superlattices Microstruct. 43, 93–100 (2008)

    Article  CAS  Google Scholar 

  19. K.G. Gopchandran, B. Joseph, J.T. Abraham, P. Koshy, V.K. Vaidyan, Vacuum 86, 547–550 (1997)

    Article  Google Scholar 

  20. R.W. Hewitt, N. Winograd, J. Appl. Phys. 51, 2620–2625 (1980)

    Article  CAS  Google Scholar 

  21. A. Morsali, M.Y. Masoomi, Coord. Chem. Rev. 253, 1882–1906 (2009)

    Article  CAS  Google Scholar 

  22. B. Moulton, M.J. Zaworotko, Chem. Rev. 101, 1629–1658 (2001)

    Article  CAS  Google Scholar 

  23. R. Kitaura, S. Kitagawa, Y. Kubota, T.C. Kobayashi, K. Kindo, Y. Mita, Science. 298, 2358–2361 (2002)

    Article  CAS  Google Scholar 

  24. B. Gomez-Lor, E. Gutie′rrez-Puebla, M. Iglesias, M.A. Monge, C. Ruiz-Valero, N. Snejko, Inorg. Chem. 41, 2429–2434 (2002)

    Article  CAS  Google Scholar 

  25. W. Yin, M. Cao, S. Luo, C. Hu, B. Wei, Cryst. Growth Des. 9, 2145–2173 (2009)

    Google Scholar 

  26. T. Ko, C. Chu, J. Chen, T. Lu, H. Kuo, S. Wang, J. Cryst. Growth 310, 2264–2267 (2008)

    Article  CAS  Google Scholar 

  27. M.S. Yazdan Parast, A. Morsali, Ultrason. Sonochem. 18, 375–381 (2011)

    Article  Google Scholar 

Download references

Acknowledgment

Supporting of this investigation by The National Science Foundation is gratefully acknowledged.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14155-4838, Tehran, Islamic Republic of Iran

    Mohammad Sadegh Yazdan Parast & Ali Morsali

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  1. Mohammad Sadegh Yazdan Parast
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  2. Ali Morsali
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Correspondence to Ali Morsali.

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Parast, M.S.Y., Morsali, A. Simple One-Pot Preparation of In2O3 Nano-particles Using a Supramolecular 3D Framework Polymer. J Inorg Organomet Polym 21, 365–368 (2011). https://doi.org/10.1007/s10904-010-9451-9

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