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Microwave assisted synthesis of ETS-10

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Abstract

Engelhard Titanium Silicate-10 (ETS-10) has attracted interest for gas adsorption, catalysis, separations and ion-exchange. The practical application of ETS-10 would benefit from improvements in the synthesis. In this paper we present a 30 h microwave assisted synthesis at 230 °C which can be compared with the 72 h required by conventional heating. The effects of different titanium precursors, pH, heating time, and organic templates on ETS-10 were also investigated.

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Acknowledgements

We also thank the Robert A. Welch Foundation and the Strategic Partnership for Research in Nanotechnology (SPRING), for the supporting of this project.

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  1. Department of Chemistry and the Alan G. MacDiarmid Nanotech Institute, The University of Texas at Dallas, Richardson, TX, 75083-0688, USA

    Jose A. Losilla & Kenneth J. Balkus Jr.

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  1. Jose A. Losilla
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  2. Kenneth J. Balkus Jr.
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Correspondence to Kenneth J. Balkus Jr..

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Losilla, J.A., Balkus, K.J. Microwave assisted synthesis of ETS-10. J Porous Mater 16, 487–496 (2009). https://doi.org/10.1007/s10934-008-9223-x

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