Skip to main content
SpringerLink
Log in

Molecular structure of di-tert-butylamine-containing the monoedge-functionalized clathrochelate iron(II) tris-dioximate

  • Brief Communications
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

The structure of 1,8-bis(fluoroboro)-2,7,9,14,15,20-hexaoxa-3,6,10,13,16,19-hexaaza-4,5,11,12-tetraphenyl-17,18-bisc(tert-butylamino)-bicyclo[6.6.6]eicosa-3,5,10,12,16,18-hexaene(2−)iron(2+) tris-dioximate clathrochelate was determined by X-ray diffraction (XRD) analysis. The compound has a molecular structure and crystallizes as triclinic crystals: a = 10.7673(2) Å, b = 11.9520(4) Å, c = 22.5473(7) Å, α = 75.729(1)°, β = 89.161(1)°, γ = 65.334(1)°, V = 2542.64(13) Å3, Z = 2, space group 1. P1¯.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. Ya. Z. Voloshin, V. E. Zavodnik, O. A. Varzatskii, et al., Inorg. Chim. Acta, 321, 116–134 (2001).

    Article  CAS  Google Scholar 

  2. APEX2 (Version 1.08), SAINT (Version 7.03), and SADABS (Version 2.11). Bruker Advanced X-ray Solutions, Bruker AXS Inc., Madison, WI, USA (2004).

  3. M. C. Burla, R. Caliandro, M. Camalli, et al., J. Appl. Crystallogr., 38, 381–388 (2005).

    Article  CAS  Google Scholar 

  4. G. M. Sheldrick, SHELXS-97 and SHELXL-97. Programs for the Refinement of Crystal Structures, Univ. Göttingen, Germany (1997).

    Google Scholar 

  5. Ya. Z. Voloshin, N. A. Kostromina, and R. Krämer, Clathrochelates: Synthesis, Structure, and Properties, Elsevier, Amsterdam (2002).

    Google Scholar 

  6. Ya. Z. Voloshin, E. V. Polshin, and A. Y. Nazarenko, Hyperfine Interact., 141/142, 309 (2002).

    Article  CAS  Google Scholar 

  7. A. B. Burdukov, E. G. Boguslavskii, V. A. Reznikov, et al., Izv. Ross. Akad. Nauk, Ser. Khim., No. 5, 1097–1102 (2005).

  8. Yu. V. Zefirov and P. M. Zorkii, Usp. Khim., LVIII, No. 5, 713–746 (1989).

    Google Scholar 

  9. C. K. Mathews and K. E. V. Holde, Biochemistry, Benjamin&Cummings, Menlo Park (1996).

    Google Scholar 

  10. Cambridge structural database, ver. 5.27; F. H. Allen and O. Kennard, Chem. Des. Automat. News, 8, 31 (1993).

Download references

Author information

Authors and Affiliations

  1. A. V. Nikolaev Insitute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk

    A. B. Burdukov, N. V. Pervukhina & M. A. Vershinin

  2. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow

    Ya. Z. Voloshin

Authors
  1. A. B. Burdukov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. N. V. Pervukhina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. A. Vershinin
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Ya. Z. Voloshin
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Original Russian Text Copyright © 2007 by A. B. Burdukov, N. V. Pervukhina, M. A. Vershinin, and Ya. Z. Voloshin

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 48, No. 2, pp. 366–369, March–April, 2007.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Burdukov, A.B., Pervukhina, N.V., Vershinin, M.A. et al. Molecular structure of di-tert-butylamine-containing the monoedge-functionalized clathrochelate iron(II) tris-dioximate. J Struct Chem 48, 358–361 (2007). https://doi.org/10.1007/s10947-007-0053-5

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10947-007-0053-5

Keywords

Search

Navigation