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Microstructural, Magnetic, and Nanoindentation Studies of the Ball-Milled Ti80Ni20 Alloy

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Abstract

Nanostructured Ti80Ni20 material was elaborated by mechanical alloying from pure Ti and Ni powders in a planetary ball-mill P7 under argon atmosphere at ambient temperature. Morphological, microstructural, magnetic, and nanoindentation properties were studied using scanning electron microscopy, X-ray diffraction, magnetic measurements, and nanoindentation test. The morphological observations show the predominance of the welding phenomenon during the milling process. The Rietveld refinement of the X-ray diffraction pattern reveals, after 4 h of milling, the formation of the disordered hcp-Ti (Ni) solid solution in addition to elemental hcp-Ti and fcc-Ni. On further milling (20 h), the interdiffusion between Ti and Ni atoms is evidenced by the formation of disordered hcp-Ti (Ni) and fcc-Ni (Ti) solid solutions. The saturation magnetization and coercivity values are about of 159.8 emu/g and 80.79 Oe, respectively, after 20 h of milling. Mr/Ms ratio indicates the existence of small magnetic particles which are typically single domains (Mr/Ms 0.1–0.5) and/or multidomain (Mr/Ms < 0.1). Nanohardness values of the sintered powders fluctuates between 1.53 and 5.98 GPa while those of the elastic modulus varies in the range 130.73 to 164.53 GPa.

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Acknowledgements

The authors are very grateful to Zerniz Nawel from the Laboratoire de Chimie organique, Département de Chimie, Faculté des Sciences, Université Badji-Mokhtar, Annaba, Algérie, for the elaboration of the nanostructured powders; to A.M. Mercier from the Laboratoire des Fluorures, Université du Maine, Le Mans, France, for the XRD measurements; to Beldi Mounira for sintering; and to Boulakraa Mohamed from the Unité de recherches des matériaux avancés, Annaba, Algérie, for the cold compaction.

Funding

This research work was supported by the Ministère de l’Enseignement Supérieur et de la Recherche Scientifique, Algérie.

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Authors and Affiliations

  1. Laboratoire de Mise en forme des Matériaux Métalliques (LMF2M), Département de Métallurgie et Génie des Matériaux, Faculté des Sciences de l’Ingéniorat, Université Badji—Mokhtar, B.P. 12, 23000, Annaba, Algeria

    L. Dekhil

  2. Département de Physique, Faculté des Sciences, Université 20 aout 1955, Skikda, Algeria

    S. Louidi

  3. Department of Physics, College of Science, University of Bahrain, PO Box 32038, Zallaq, Kingdom of Bahrain

    M. Bououdina

  4. Mechanical Engineering Department, Abbes Laghrour University, P. O. 1252, 40004, Khenchela, Algeria

    M. Fellah

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  1. L. Dekhil
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  2. S. Louidi
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Correspondence to L. Dekhil.

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Dekhil, L., Louidi, S., Bououdina, M. et al. Microstructural, Magnetic, and Nanoindentation Studies of the Ball-Milled Ti80Ni20 Alloy. J Supercond Nov Magn 32, 3623–3636 (2019). https://doi.org/10.1007/s10948-019-05145-1

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  • DOI: https://doi.org/10.1007/s10948-019-05145-1

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