Skip to main content
Fachgebiete
Automobil + Motoren Bauwesen + Immobilien Business IT + Informatik Elektrotechnik + Elektronik Energie + Nachhaltigkeit Finance + Banking Management + Führung Marketing + Vertrieb Maschinenbau + Werkstoffe Versicherung + Risiko
DE
EN
Bücher
Zeitschriften
Themenseiten
Organisationspsychologie Projektmanagement Marketing Smart Manufacturing
Weitere Formate
Podcasts Webinare Technik Webinare Wirtschaft Kongresse Veranstaltungskalender Awards
Jetzt Einzelzugang starten
Zugang für Unternehmen
Referenzkunden
SLX-Digitalkonferenz: Zukunftswerkstatt 2024

Mehr Umsatz mit Top-Kontakten

Am 7. Mai erfahren Sie, wie Vertriebsteams Leadgenerierung, Leadnurturing und Leadstrategien effizient steuern können.
Erweiterte Suche
Anmelden
nach oben
Journal of Sol-Gel Science and Technology
Erschienen in: Journal of Sol-Gel Science and Technology 1/2014

01.04.2014 | Original Paper

Synthesis and characterization of non-transformable tetragonal YSZ nanopowder by means of Pechini method for thermal barrier coatings (TBCs) applications

verfasst von: Morteza Hajizadeh-Oghaz, Reza Shoja Razavi, Mohammad Reza Loghman-Estarki

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 1/2014

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

A simple soft chemical method of synthesizing tetragonal yttria stabilized zirconia nanopowders is described here. Zirconium oxy-chloride octahydrate and yttrium nitrate hexahydrate were taken as a source of zirconium, citric acid was taken as a chelating agent, and ethylene glycol was used as a polysterification agent. The synthesized powders were characterized by X-ray diffraction, thermogravimetric analysis and differential scanning calorimetry, transmission electron microscopy, field emission scanning electron microscope, Fourier transform infrared spectroscopy and Raman spectroscopy. Furthermore, precise cell parameters were calculated in order to exactly determine non-transformable tetragonal crystal structure, which was the best zirconia phase for thermal barrier coatings applications. In this process, tetragonal yttria stabilized zirconia nanopowders could be prepared at a temperature of 1,000 °C and the process was simple and cost-effective.
Vorheriger Artikel Preparation of silica nanoparticles catalysed by small organic tertiary amine and applications in surface coating with antireflective/antifogging properties
Nächster Artikel Novel bulk synthesis of magnesium oxide nanobelts networks by microwave hydrothermal route

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren
Literatur
1.
Kumari L, Li W, Xu J, Leblanc R, Wang D, Li Y, Guo H, Zhang J (2009) Controlled hydrothermal synthesis of zirconium oxide nanostructures and their optical properties. Cryst Growth Des 9(9):3874–3880CrossRef
2.
Liu H, Jazi H, Bussmann M, Mostaghimi J (2009) Experiments and modeling of rapid solidification of plasma-sprayed yttria-stabilized zirconia. Acta Mater 57(20):6013–6021CrossRef
3.
Li P, Chen IW, Penner-Hahn JE (1994) Effect of dopants on zirconia stabilization—an X-ray absorption study: I, trivalent dopants. J Am Ceram Soc 77(1):118–128CrossRef
4.
Li P, Chen IW, Penner-Hahn JE (1994) Effect of dopants on zirconia stabilization—an X-ray absorption study: II, tetravalent dopants. J Am Ceram Soc 77(5):1281–1288CrossRef
5.
Li P, Chen IW, Penner-Hahn JE (1994) Effect of dopants on zirconia stabilization—an X-ray absorption study: III, charge-compensating dopants. J Am Ceram Soc 77(5):1289–1295CrossRef
6.
Viazzi C, Bonino J-P, Ansart F, Barnabé A (2008) Structural study of metastable tetragonal YSZ powders produced via a sol–gel route. J Alloys Compd 452(2):377–383CrossRef
7.
Miller RA, Smialek JL, Garlick RG (1981) Phase stability in plasma-sprayed, partially stabilized zirconia-yttria
8.
Comelli RA, Vera CR, Parera JM (1995) Influence of ZrO2 crystalline structure and sulfate ion concentration on the catalytic activity of So2 − 4-ZrO2. J Catal 151(1):96–101CrossRef
9.
Shukla S, Seal S (2005) Mechanisms of room temperature metastable tetragonal phase stabilisation in zirconia. Int Mater Rev 50(1):45–64CrossRef
10.
Štefanić G, Musić S, Gržeta B, Popović S, Sekulić A (1998) Influence of pH on the stability of low temperature t-ZrO2. J Phys Chem Solids 59(6):879–885
11.
Pacheco G, Fripiat J (2000) Physical chemistry of the thermal transformation of mesoporous and microporous zirconia. J Phys Chem B 104(50):11906–11911CrossRef
12.
Nettleship I, Stevens R (1987) Tetragonal zirconia polycrystal (TZP)—a review. Int J High Technol Ceram 3(1):1–32CrossRef
13.
Subbarao E (1981) Ceramic dielectrics for capacitors. Ferroelectrics 35(1):143–148CrossRef
14.
Scott H (1975) Phase relationships in the zirconia-yttria system. J Mater Sci 10(9):1527–1535CrossRef
15.
Mevrel R, Rio C, Poulain M, Diot C, Nardou F (1987) Technical Report No. 28/2019M. ONERA
16.
Miller RA (1997) Thermal barrier coatings for aircraft engines: history and directions. J Therm Spray Technol 6(1):35–42CrossRef
17.
Bose S (2011) High temperature coatings. Butterworth-Heinemann, UK
18.
Srinivasan R, De Angelis RJ, Ice G, Davis BH (1991) Identification of tetragonal and cubic structures of zirconia using synchrotron x-radiation source. J Mater Res 6(6):1287–1292CrossRef
19.
Kontoyannis CG, Carountzos G (1994) Quantitative determination of the cubic-to-monoclinic phase transformation in fully stabilized Zirconias by Raman spectroscopy. J Am Ceram Soc 77(8):2191–2194CrossRef
20.
Pechini M (1967) Patent No. 3,330,697. United States Patent Office
21.
Cullity BD, Stock SR (2001) Elements of X-ray diffraction, vol 3. Prentice Hall Upper Saddle River, NJ
22.
Suryanarayana C, Norton MG (1998) X-ray diffraction: a practical approach. Springer, BerlinCrossRef
23.
da Silva RS, Bernardi MIB, Hernandes AC (2007) Synthesis of non-agglomerated Ba0. 77Ca0. 23TiO3 nanopowders by a modified polymeric precursor method. J Sol-Gel Sci Technol 42(2):173–179CrossRef
24.
Singh K, Pathak L, Roy S (2007) Effect of citric acid on the synthesis of nano-crystalline yttria stabilized zirconia powders by nitrate–citrate process. Ceram Int 33(8):1463–1468CrossRef
25.
Sakka S (2005) Handbook of sol-gel science and technology. 1. Sol-gel processing, vol 1. Springer
26.
Kakihana M, Yoshimura M (1999) Synthesis and characteristics of complex multicomponent oxides prepared by polymer complex method. Bull Chem Soc Jpn 72(7):1427–1443CrossRef
27.
Xu Y, Yuan X, Huang G, Long H (2005) Polymeric precursor synthesis of Ba2Ti9O20. Mater Chem Phys 90(2):333–338CrossRef
28.
Socrates G, Socrates G (2001) Infrared and Raman characteristic group frequencies: tables and charts. Wiley, Chichester
29.
Zhang Y, Li A, Yan Z, Xu G, Liao C, Yan C (2003) (ZrO2) 0.85 (REO1. 5) 0.15 (Re. J Solid State Chem 171(1–2):434–438CrossRef
30.
Laberty-Robert C, Ansart F, Deloget C, Gaudon M, Rousset A (2001) Powder synthesis of nanocrystalline ZrO2–8% Y2O3 via a polymerization route. Mater Res Bull 36(12):2083–2101CrossRef
31.
Zhang Y-W, Yan Z-G, Liao F-H, Liao C-S, Yan C-H (2004) Citrate gel synthesis and characterization of (ZrO2)0.85 (REO1.5) 0.15 (RE = Y, Sc) solid solutions. Mater Res Bull 39(11):1763–1777CrossRef
32.
Thackeray D (1974) The Raman spectrum of zirconium dioxide. Spectrochimica Acta Part A Mol Spectrosc 30(2):549–550CrossRef
33.
Li C, Li M (2002) UV Raman spectroscopic study on the phase transformation of ZrO2, Y2O3–ZrO2 and SO42−/ZrO2. J Raman Spectrosc 33(5):301–308CrossRef
34.
Naumenko A, Berezovska N, Biliy M, Shevchenko O (2008) Vibrational analysis and Raman spectra of tetragonal Zirconia. Phys Chem Solid State 9(1):121–125
35.
Gazzoli D, Mattei G, Valigi M (2007) Raman and X-ray investigations of the incorporation of Ca2+ and Cd2+ in the ZrO2 structure. J Raman Spectrosc 38(7):824–831CrossRef
36.
Perry C, Liu DW, Ingel RP (1985) Phase characterization of partially stabilized zirconia by Raman spectroscopy. J Am Ceram Soc 68(8):C184–C187CrossRef
37.
Kim DJ, Jung HJ, Yang IS (1993) Raman spectroscopy of tetragonal zirconia solid solutions. J Am Ceram Soc 76(8):2106–2108CrossRef
38.
Nitsche R, Rodewald M, Skandan G, Fuess H, Hahn H (1996) HRTEM study of nanocrystalline zirconia powders. Nanostructured Mater 7(5):535–546CrossRef
39.
Chen H, Ding C (2003) Transmission electron microscopy observation of microstructure of plasma-sprayed nanostructured zirconia coating. J Therm Spray Technol 12(4):523–529CrossRef
40.
Ryu J-H, Kil H-S, Song J-H, Lim D-Y, Cho S-B (2012) Glycothermal synthesis of 3 mol% yttria stabilized tetragonal ZrO2 nano powders at low temperature without mineralizers. Powder Technol 221:228–235CrossRef
41.
Handbook A (1979) Metals handbook. Powder Metallurgy 9
Metadaten
Titel
Synthesis and characterization of non-transformable tetragonal YSZ nanopowder by means of Pechini method for thermal barrier coatings (TBCs) applications
verfasst von
Morteza Hajizadeh-Oghaz
Reza Shoja Razavi
Mohammad Reza Loghman-Estarki
Publikationsdatum
01.04.2014
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 1/2014
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-014-3266-z

Weitere Artikel der Ausgabe 1/2014

Journal of Sol-Gel Science and Technology 1/2014 Zur Ausgabe

Original Paper

Synthesis and characterization of new silica–titania mixed oxide in the presence of 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl) imide by sol–gel technique

Original Paper

Synthesis and characterization of highly preferred orientation polycrystalline Co-doped ZnO thin films prepared by improved sol–gel method

Original Paper

Controllable synthesis and enhanced visible photocatalytic degradation performances of Bi2WO6–carbon nanofibers heteroarchitectures

Original Paper

Hierarchical meso–macroporous bioglass for bone tissue engineering

Original Paper

Synthesis of monoclinic BiVO4 microribbons by sol–gel combined with electrospinning process and photocatalytic degradation performances

Original Paper

Novel bulk synthesis of magnesium oxide nanobelts networks by microwave hydrothermal route

Premium Partner

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen. 

    Zur Marktübersicht
    Bildnachweise