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Erschienen in: Journal of Nanoparticle Research 4/2014

01.04.2014 | Research Paper

Synthesis of flexible free-standing silver nanoparticles-graphene films and their surface-enhanced Raman scattering activity

verfasst von: Nan Zhao, Xiaonong Cheng, Yazhou Zhou, Mingxin Yang, Juan Yang, Tao Zhong, Sihui Zheng

Erschienen in: Journal of Nanoparticle Research | Ausgabe 4/2014

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Abstract

A free-standing and flexible silver nanoparticles-graphene (Ag NPs–GE) film with high surface-enhanced Raman scattering (SERS) sensitivity has been developed. First, the high stable and dispersive Ag NPs–GE composite was fabricated by in situ reduction using graphene oxide sheets as substrates and the hydrazine hydrate as a reducing agent in the solvothermal environment. Second, the Ag NPs–GE films can be fabricated through vacuum filtration of the Ag NPs–GE suspension. Transmission electron microscope (TEM) images show that the Ag NPs with an average size of 22 nm and a narrow particle size distribution are uniformly distributed on GE sheets. The coverage density of Ag NPs onto the surface of GE sheets can be successfully controlled by tuning the concentration of silver ion precursor. As-prepared Ag NPs–GE substrates have good SERS sensitivity due to the high SERS-active of Ag NPs. The enhancement factor for 1 × 10−6 M of rhodamine 6G molecules adsorbed onto the surface of substrate is about 2.7 × 105. The SERS activity toward crystal violet and Escherichia coli was also investigated.

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Metadaten
Titel
Synthesis of flexible free-standing silver nanoparticles-graphene films and their surface-enhanced Raman scattering activity
verfasst von
Nan Zhao
Xiaonong Cheng
Yazhou Zhou
Mingxin Yang
Juan Yang
Tao Zhong
Sihui Zheng
Publikationsdatum
01.04.2014
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 4/2014
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-014-2335-0

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