Introduction
Experimental
The STIP Irradiation Parameters
Tensile Testing of the STIP Samples
Small Scale Sample Preparation
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Initially foil production began with a 1 μm × 1 μm × 10 μm slice cut from the foil and transported to the LEAP sample holder stubs [14‐16] using the micro manipulator. The sample setup was shaped in a key and slot shape to ensure a good connection. Carbon was deposited on the connection using the gas injector systems (GIS) to ensure a good and stable joint. It was found that carbon gives a similar joint as Pt. While time consuming, this technique was determined to result in a stable connection and safe sample transport. The principle steps of this method are shown in Fig. 2(a–d).×
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The second technique instead transported the entire foil to the sample holder stub once it was removed from the sample. Then the end of the foil was mounted on the stub by depositing carbon on the sample-stub joint after which the foil was cut so the LEAP needle was attached to the holder. This is a quicker way of mounting the sample but the joint between the actual sample and the Si holder might not be as stable as the initially described method above. The unique steps of Method 2 are illustrated in Fig. 2(e–f).
Small Scale Mechanical Testing
Local Electrode Atom Probe Measurements
Results and Discussion
Dose Rate and Isotope Estimations on the STIP Samples
Isotope | Total activity measured [Bq] | Activity/LEAP needle [Bq] |
---|---|---|
Na-22 | 6.56 105
| 1.68 10−5
|
Mn-54 | 5.05 107
| 1.29 10−3
|
Co-57 | 7.04 105
| 1.8 10−5
|
Co-58 | M. to low | M. to low |
Co-60 | 2.19 107
| 5.6 10−4
|
Tc-95 | M. to low | M. to low |
Hf-172 | 4.57 105
| 1.17 10−5
|
Lu-172 | 7.36 105
| 1.88 10−5
|
Lu-173 | 1.06 106
| 2.79 10−5
|
Re-186 | M. to low | M. to low |
Total activity [Bq] | 7.6 107
| 1.95 10−3
|
Total dpm # LEAP needles until 200 dpm | 4.56 109
| 1.71 10−1
|
171 103
| ||
mSv/h | 3.6 | 9.28 10−11
|