Skip to main content
Log in

Advanced characterization of pores and fractures in coals by nuclear magnetic resonance and X-ray computed tomography

  • Research Paper
  • Published:
Science China Earth Sciences Aims and scope Submit manuscript

Abstract

This paper demonstrates capabilities of low-field nuclear magnetic resonance (NMR) and microfocus X-ray computed tomography (μCT) in advanced, nondestructive, and quantitative characterization of pore types, producible porosity, pore structure, and spatial disposition of pore-fractures in coals. Results show that the NMR transverse relaxation time (T 2) at 0.5–2.5, 20—50, and >100 ms correspond to pores of <0.1 μm, >0.1 μm, and fractures, respectively. A much higher T 2 spectrum peak reflects a much better development of pores (or fractures) corresponding to the T 2, and vice versa. Three basic components in coals, i.e., the pores (or fractures), coal matrix, and minerals have their distinctive range of CT numbers. Among these, the CT number of pores is commonly less than 600 HU. The producible porosity, which is a determination of permeability, can be calculated by T 2 cutoff value (T 2C) of coal NMR. The coal pore structure can be efficiently estimated by the newly proposed “T 2C based model”. Finally, μCT scan was proven capable of modeling and spatial visualization of pores and fractures.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Yao Y B, Liu D M, Tang D Z, et al. Reserving and recovering characteristics of coalbed methane in coal reservoirs in North China (in Chinese). Petro Exp Dev, 2007, 34: 664–668

    Google Scholar 

  2. Sing K S W. Characterization of porous materials: Past, present and future. Colloid Surface A, 2004, 241: 3–7

    Article  Google Scholar 

  3. Yao Y B, Liu D M, Huang W H, et al. Research on the pore-fractures system properties of coalbed methane reservoirs and recovery of coalbed methane in Huainan and Huaibei coal-fields (in Chinese). J China Coal Soc, 2006, 31: 163–168

    Google Scholar 

  4. Yao Y B, Liu D M, Tang D Z, et al. Fractal characterization of adsorption-pores of coals from North China: An investigation on CH4 adsorption capacity of coals. Int J Coal Geol, 2008, 73: 27–42

    Article  Google Scholar 

  5. Yao Y B, Liu D M, Tang D Z, et al. Fractal characterization of seep-age-pores of coals from China: An investigation on permeability of coals. Comput Geosci, 2009, 35:1159–1166

    Article  Google Scholar 

  6. Suuberg E M, Deevi S C, Yun Y. Elastic behaviour of coals studied by mercury porosimetry. Fuel, 1995, 74: 1522–1530

    Article  Google Scholar 

  7. Gane P A C, Ridgway C J, Lehtinen E, et al. Comparison of NMR cryoporometry, mercury intrusion porosimetry, and DSC thermoporosimetry in characterizing pore size distributions of compressed finely ground calcium carbonate structures. Ind Eng Chem Res, 2004, 43: 7920–7927

    Article  Google Scholar 

  8. Yao Y B, Liu D M, Che Y, et al. Petrophysical characterization of coals by low-field nuclear magnetic resonance (NMR). Fuel, 2009, doi: 10.1016/j.fuel.2009.11.005

  9. Yao Y B, Liu D M, Che Y, et al. Non-destructive characterization of coal samples from China using microfocus X-ray computed tomography. Int J Coal Geol, 2009, 80: 113–123

    Article  Google Scholar 

  10. Coates G R, Xiao L Z, Prammer M G. NMR Logging Principles and Applications. Houston (Texas): Gulf Publishing Company, 1999. 1–76

    Google Scholar 

  11. Kevin M, Douglas M, Smith A. NMR technique for the analysis of pore structure: numerical inversion of relaxation measurements. J Colloid Interface Sci, 1987, 19: 117–126

    Google Scholar 

  12. Hodgkins M A, Howard J J. Application of NMR logging to reservoir characterization of low-resistivity sands in the gulf of Mexico. AAPG Bull, 1999, 83: 114–127

    Google Scholar 

  13. Wang W M, Sun D Q, Miao S, et al. The fundamental study on NMR logging (in Chinese). Well Log Tech, 1997, 21: 385–392

    Google Scholar 

  14. Wang X W, Xiao L Z, Xie R H, et al. Study of NMR porosity for terrestrial formation in China. Sci China Ser G-Phys, Mech Astron, 2006, 49: 313–320

    Article  Google Scholar 

  15. Kenyon W E. Nuclear magnetic resonance as a petrophysical measurement. Nucl Geophys, 1992, 6:153–171

    Google Scholar 

  16. Karacan C Ö, Okandan E. Fracture/cleat analysis of coals from Zonguldak Basin (northwestern Turkey) relative to the potential of coalbed methane production. Int J Coal Geol, 2000, 44: 109–125

    Article  Google Scholar 

  17. Van Geet M, Swennen R. Quantitative 3D-fracture analysis by means of microfocus X-ray computer tomography (μCT): An example from coal. Geophys Res Lett, 2001, 28: 3333–3336

    Article  Google Scholar 

  18. Mazumder S, Wolf K H A A, Elewaut K, et al. Application of X-ray computed tomography for analyzing cleat spacing and cleat aperture in coal samples. Int J Coal Geol, 2006, 68: 205–222

    Article  Google Scholar 

  19. Yakov V. A practical approach to obtain primary drainage capillary pressure curves from NMR core and log data. Petrophysics, 2001, 42: 334–343

    Google Scholar 

  20. Liu T Y, Xiao L Z, Fu R S, et al. Applications and characterization of NMR relation derived from sphere capillary model (in Chinese). Chin J Geophys, 2004, 47:663–671

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to YanBin Yao.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Yao, Y., Liu, D., Cai, Y. et al. Advanced characterization of pores and fractures in coals by nuclear magnetic resonance and X-ray computed tomography. Sci. China Earth Sci. 53, 854–862 (2010). https://doi.org/10.1007/s11430-010-0057-4

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11430-010-0057-4

Keywords

Navigation