Abstract
The class of low-carbon, high-alloy CrMnNi steels exhibits outstanding mechanical properties with respect to high strength and ductility due to either transformation-induced plasticity (TRIP) or twinning-induced plasticity (TWIP) effect depending on chemical composition and deformation temperature. However, the ongoing deformation mechanisms like the formation of stacking faults, martensitic phase transformation or deformation-induced twinning are overlapping and the kinetics of the microstructure evolution are quite complex. Therefore, in addition to macroscopic deformation tests and microstructural investigations by scanning electron microscopy, a combination of several in situ characterization techniques with either high lateral and/or temporal resolution as well as providing integral volume information were chosen in order to give a thoroughly and comprehensive description of the deformation behavior of CrMnNi TRIP/TWIP steels. In addition, the complementary in situ techniques like in situ nanoindentation, micro-digital image correlation, and acoustic emission measurements provide excellent possibility for description of materials behavior on a multiscale level from the submicrometer scale up to the macroscopic range. The results obtained by the complementary techniques can support the future modeling of the deformation behavior of TRIP/TWIP steels dependent on chemical composition, temperature, grain size and grain orientation.
Similar content being viewed by others
References
W.B. Lee, S.G. Hong, C.G. Park, and S.H. Park, Met. Mater. Trans. A 33, 1689 (2002).
M. Calcagnotto, D. Ponge, and D. Raabe, Mater. Sci. Eng. A 527, 7832 (2010).
J. Speer, D.K. Matlock, B.C. De Cooman, and J.G. Schroth, Acta Mater. 51, 2611 (2003).
B.C. De Cooman, Curr. Opin. Sol. State Mater. Sci. 8, 285 (2004).
J.H. Shin, J.S. Jeong, and J.W. Lee, Mater. Charac. 99, 230 (2015).
O. Grässel, L. Krüger, G. Formmeyer, and L.W. Meyer, Int. J. Plast 16, 1391 (2000).
G. Frommeyer, U. Brüx, and P. Neumann, ISIJ Inter. 43, 438 (2003).
C. Herrera, D. Ponge, and D. Raabe, Acta Mater. 59, 4653 (2011).
G.B. Olson and M. Cohen, Met. Mat. Trans. A 6, 791 (1975).
G.B. Olson, Transformation plasticity and stability of plastic flow, in Deformation, Processing and Structure, ed. by G. Krauss (Metals park, OH: ASM, 1984), pp. 391–424.
V.I. Levistas, A.V. Idesman, and G.B. Olson, Acta Mater. 47, 219 (1999).
B.C. de Cooman, O. Kwon, and K.G. Chin, Mater. Sci. Technol. 28, 513 (2012).
O. Bouaziz, S. Allain, and C. Scott, Scripta Mater. 58, 484 (2008).
K. Renard, S. Ryelandt, and P.J. Jacques, Mater. Sci. Eng. A 527, 2969 (2010).
A. Weiß, H. Gutte, M. Radke, and P.R. Scheller, patent specification WO 0020 08009722A1.
A. Jahn, A. Kovalev, A. Weiss, S. Wolf, L. Krüger, and P.R. Scheller, Steel Res. Int. 82, 39 (2011).
A. Glage, A. Weidner, and H. Biermann, Steel Res. Int. 82, 1040 (2011).
S. Ackermann, D. Kulawinski, S. Henkel, and H. Biermann, Int. J. Fatig. 67, 123 (2014).
D. Ehinger, L. Krüger, U. Martin, C. Weigelt, and C.G. Aneziris, Steel Res. Int. 82, 1048 (2011).
S. Ackermann, S. Martin, M.R. Schwarz, C. Schimpf, D. Kulawinski, C. Lathe, S. Henkel, D. Rafaja, H. Biermann, and A. Weidner, Met. Mat. Trans. A (2015, in press).
A. Weidner, S. Martin, V. Klemm, U. Martin, and H. Biermann, Scripta Mater. 64, 513 (2011).
S. Martin, S. Wolf, U. Martin, and L. Krüger, Solid State Phenom. 172–174, 172 (2011).
D. Rafaja, C. Krbetschek, D. Borisova, H. Schreiber, and V. Klemm, Thin Solid Films 530, 105 (2013).
D. Borisova, V. Klemm, S. Martin, S. Wolf, and D. Rafaja, Adv. Eng. Mater. 15, 571 (2013).
A. Jahn, A. Kovalev, A. Weiss, and P.R. Scheller, Steel Res. Int. 82, 1108 (2011).
H. Biermann, A. Glage, and M. Droste, Met. Mater. Trans. A (2015). doi:10.1007/s11661-014-2723-1.
A. Weidner, A. Müller, A. Weiss, and H. Biermann, Mater. Sci. Eng. A 571, 68 (2013).
A. Vinogradov, J. Acoust. Emission 17, 1 (1998).
C.U. Grosse and M. Ohtsu, Acoustic Emission Testing: Basics for Research—Applications in Civil Engineering (Berlin: Springer, 2010), p. 3.
H. Hatano, J. Appl. Phys. 48, 4397 (1977).
W. Schaarwachter and H. Ebener, Acta Metall. Mater. 38, 195 (1990).
D. Rouby, P. Fleischmann, and C. Duvergier, Phys. Stat. solid. A 48, 439 (1978).
A. Vinogradov, S. Hashimoto, and S. Miura, Acta Mater. 44, 2883 (1996).
K. Kitagawa, Y. Kaneko, and A. Vinogradov, Mater. Trans. 38, 607 (1997).
C. Scruby, H. Wadley, and J.E. Sinclair, Phil. Mag. A 44, 249 (1981).
J. Baram and M. Rosen, Mater. Sci. Eng. 47, 243 (1981).
J. Baram, Y. Geren, and M. Rosen, Scripta Metal. 15, 835 (1981).
A. Vinogradov, V. Patlan, S. Hashimoto, and K. Kitagawa, Phil. Mag. A 82, 317 (2002).
K. Darowicki, A. Mirakowski, and S. Krakowiak, Corr. Sci. 45, 1747 (2003).
A. Danyuk, D. Merson, and A. Vinogradov, Proceedings 12th International Conference of the Slovenian Society of Non-Destructive testing, Portoroz, Slovenia, 567 (2013) pp. 567–574.
J.A. Simmons and H.N.G. Wadley, J. Research Nat. Bureau Stand. 89, 55 (1984).
R. Pascual, M. Ahlers, and R. Ra Dacioli, Scripta Metall. 9, 79 (1975).
S. Mintzer and R. Pascual, Scripta Metall. 12, 531 (1978).
C.H. Caceres, W. Arneodo, R. Pascual, and H.R. Bertorello, Scripta Metall. 14, 293 (1980).
K. Takashima, Y. Higo, and S. Nunomura, Scripta Metall. 14, 489 (1980).
K.Takashima, Y.Higo, and S. Nunomura, Phil. Mag. A 49, 221 (1984).
L. Manosa, A. Planes, D. Rouby, and J.L. Macqueron, Acta Metall. Mater. 38, 1635 (1990).
K. Barat, H.N. Bar, D. Mandal, H. Royc, S. Sivaprasad, and S. Tarafder, Mater. Sci. Eng. A 597, 37 (2014).
S.M.C. van Bohemen, J. Sietsma, M.J.M. Hermans, and I.M. Richardson, Acta Mater. 51, 4183 (2003).
S.M.C. van Bohemen, Phil. Mag. A 95, 210 (2015).
E. Pomponi and A. Vinogradov, Mech. Syst. Signal Proc. 40, 791 (2013).
A. Vinogradov, A. Lazarev, M. Linderov, A. Weidner, and H. Biermann, Acta Mater. 61, 2434 (2013).
VEDDAC 5.0—Digitale Image Correlation Software, Chemnitzer, Werkstoffmechnik GmbH, Technologiecampus 1, 09126 Chemnitz, Germany.
C.A. Walker, Exp. Mech. 34, 281 (1994).
G. Hartmann and T. Nicholas, Exp. Techn. 11, 24 (1987).
J. Fang and F.H. Dai, Exp. Mech. 31, 163 (1991).
N. Biery, M. De Graef, and T.M. Pollock, Metall. Mater. Trans. A 34, 2301 (2003).
M. Eskandari, M.R. Yadegari-Dehnavi, A. Zarei-Hanzaki, M.A. Mohtadi-Bonab, R. Basu, and J.A. Szpunar, Opt. Las. Eng. 67, 1 (2015).
C. Efstathiou, H. Sehitoglu, and J. Lambros, Int. J. Plast 26, 93 (2010).
W. Abuzaid, H. Sehitoglu, and J. Lambros, Mater. Sci. Eng. A 561, 507 (2013).
H.A. Crostack, G. Fischer, E. Soppa, S. Schmauder, and Y.L. Liu, J. Microsc. 201, 171 (2001).
M.A. Sutton, N. Li, D.C. Joy, A.P. Reynolds, and X. Li, Exp. Mech. 47, 775 (2007).
E. Heripre, M. Dexet, J. Crepin, L. Gelebart, A. Ross, M. Bornet, and D. Caldemaison, Int. J. Plast 23, 1512 (2007).
A. Tatschl and O. Kolednik, Mater. Sci. Eng. A 339, 265 (2003).
C.C. Tasan, J.P.M. Hoefnagels, M. Diehl, D. Yan, F. Roters, and D. Raabe, Int. J. Plast 63, 198 (2014).
M. Krottenthaler, C. Schmid, J. Schaufler, K. Durst, and M. Göken, Surf. Coat. Technol. 215, 247 (2013).
B. Winiarski, G.S. Schajer, and P.J. Withers, Exp. Mech. 52, 793 (2012).
H. Na, S. Nambu, M. Ojima, J. Inoue, and T. Koseki, Scripta Mater. 69, 793 (2013).
H. Ghadbeigi, C. Pinna, S. Celotto, and J.R. Yates, Mater. Sci. Eng. A 527, 5026 (2010).
H. Ghadbeigi, C. Pinna, and S. Celotto, Mater. Sci. Eng. A 588, 420 (2013).
A. Ramazani, Z. Ebrahimi, and U. Prahl, Comput. Mater. Sci. 87, 241 (2014).
M. Kimiecik, J.W. Jones, and S. Daly, Mater. Lett. 95, 25 (2013).
A.C. Fischer-Cripps, Nanoindentation, 2nd ed. (New York: Springer, 2004).
A.C. Fischer-Cripps, Surf. Coat. Technol. 200, 4153 (2006).
Q. Furnemont, M. Kempf, P.J. Jacques, M. Göken, and F. Delannay, Mater. Sci. Eng. A 328, 26 (2002).
B.B. He and M.X. Huang, Met. Mater. Trans. A 46, 688 (2015).
B.B. He, M.X. Huang, Z.Y. Liang, A.H.W. Ngan, H.W. Luo, J. Shi, W.Q. Cao, and H. Dong, Scripta Mater. 69, 215 (2013).
H. Nili, K. Kalantar-zadeh, M. Bhaskaran, and S. Sriram, Prog. Mater Sci. 58, 1 (2013).
R. Rabe, J.M. Breguet, P. Schwaller, S. Stauss, F.J. Huang, J. Patscheider, and J. Michler, Thin Solid Films 469–470, 206 (2004).
R. Ghisleni, K. Rzepiejewska-Malyska, L. Philippe, P. Schwaller, and J. Michler, Micros. Res. Technol. 72, 242 (2009).
J.D. Nowak, K.A. Rzepiejewska-Malyska, R.C. Major, O.L. Warren, and J. Michler, Mater Today Electron Microsc. Spec. Issue 12, 44–45 (2010).
B. Moser, J. Kuebler, H. Meinhard, W. Muster, and J. Michler, Adv. Eng. Mater. 7, 388 (2005).
K. Rzepiejewska-Malyska, M. Parlinska-Wojtan, K. Wasmer, K. Hejduk, and J. Michler, Micron 40, 22 (2009).
K.A. Rzepiejewska-Malyska, G. Buerki, J. Michler, R.C. Major, E. Cyrankowski, S.A.S. Asif, and O.L. Warren, J. Mater. Res. 23, 1973 (2008).
C. Niederberger, W.M. Mook, X. Maeder, and J. Michler, Mater. Sci. Eng. A 527, 4306 (2010).
Q.X. Dai, A.D. Wang, X.N. Cheng, and X.M. Luo, Chin. Phys. 11, 596 (2002).
D. Rafaja, C. Krbetschek, C. Ullrich, and S. Martin, J. Appl. Cryst. 47, 947 (2014).
S. Martin, S. Wolf, U. Martin, L. Krüger, and D. Rafaja, Metall. Mater. Trans. A (2014). doi:10.1007/s11661-014-2684-4.
H. Biermann, S. Solarek, and A. Weidner, Steel Res. Int. 83, 512 (2012).
L. Remy, A. Pineau, and B. Thomas, Mater. Sci. Eng. 36, 47 (1978).
L. Krüger, S. Wolf, U. Martin, S. Martin, P.R. Scheller, A. Jahn, and A. Weiss, J. Phys. Conf. Ser. 240, 12098 (2010).
A. Kovalev, A. Jahn, A. Weiß, S. Wolf, and P.R. Scheller, Steel Res. Int. 82, 1108 (2011).
Hysitron, http://www.hysitron.com/Portals/0/Updated%20Address/SEMSS_SAM-0072-A.pdf. Accessed 24 March 2015.
A. Weidner, U. Hangen, and H. Biermann, Phil. Mag. Lett. 94, 522 (2014).
A. Weidner, C. Segel, and H. Biermann, Mater. Lett. 143, 155 (2015).
Ferritscope© FMP30—Helmut Fischer GmbH, Industriestarße 21, 7106 9 Sindelfingen-Maichingen.
J. Talonen, PhD thesis, Helsinki (2007).
A. Weiß, H. Gutte, and P.R. Scheller; Proceedings of the Fifth Stainless Steel Science and Market Congress, (2005).
A. Weidner, A. Glage, and H. Biermann, Proc. Eng. 2, 1961 (2010).
S. Martin, C. Ullrich, D. Simek, U. Martin, and D. Rafaja, J. Appl. Cryst. 44, 779 (2011).
S. Martin, C. Ullrich, and D. Rafaja, Proceedings ICOMAT 2014, Materials Today (2015).
J.-B. Seol, J.E. Jung, Y.W. Jang, and C.G. Park, Acta Mater. 61, 558 (2013).
M. Linderov, C. Segel, A. Weidner, H. Biermann, and A. Vinogradov, Mater. Sci. Eng. A 597, 183 (2014).
S. Zaefferer and N.N. Elhami, Acta Mater. 75, 20 (2014).
H. Mansour, J. Guyon, M.A. Crimp, N. Gey, B. Beausir, and N. Maloufi, Scripta Mater. 84–85, 11 (2014).
A. Weidner and H. Biermann, Phil. Mag. A 95, 759 (2015).
D.G. Coates, Phil. Mag. 16, 1179 (1967).
G.R. Booker, M.B. Shawa, M.J. Whelan, and P.B. Hirsch, Phil. Mag. 16, 1185 (1967).
J. Talonen and H. Hänninen, Acta Mater. 55, 6108 (2007).
J. Thomas and T. Gemming, Analytical Transmission Electron Microscopy (Wien: Springer, 2014), p. 135.
H. Idrissi, K. Renard, L. Ryelandt, D. Schryvers, and P.J. Jaqcues, Acta Mater. 58, 2464 (2010).
W.C. Oliver and G.M. Pharr, J. Mater. Res. 7, 1564 (1992).
J.G. Sevillano, Scripta Mater. 60, 336 (2009).
S. Martin, S. Wolf, S. Decker, L. Krüger, and U. Martin; Steel Res. Int. (2015, in press).
G.V. Kurdjumov and G. Sachs, Z. Phys. 32, 325 (1930).
H. Schumann, Krist. Tech. 1, 663 (1976).
H. Schumann, Krist. Tech. 12, 363 (1977).
J. Kim, Y. Estrin, H. Beladi, I. Timokhina, K. Chin, S. Kim, and B.C. De Cooman, Met. Mat. Trans. A 43, 479 (2012).
Acknowledgement
The authors thank the German Research Foundation (DFG) for the financial support of the Collaborative Research Centre “TRIP-Matrix Composite” (CRC 799), subproject B5. PhD M. Linderov and Prof. A. Vinogradov are acknowledged for their assistance with the AE data analysis. Dipl.-Ing. J. Solarek and Dipl.-Ing. C. Segel are acknowledged for performing the in situ tests and the µDIC, respectively. Dr. S. Martin is acknowledged for providing the TEM foil for the t-SEM investigations. Dr. U. Hangen is acknowledged for the assistance with the in situ nanoindentation experiments. Furthermore, the authors would kindly express their thanks to all colleagues of the CRC contributing to the comprehensive results reported in this paper.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Weidner, A., Biermann, H. Combination of Different In Situ Characterization Techniques and Scanning Electron Microscopy Investigations for a Comprehensive Description of the Tensile Deformation Behavior of a CrMnNi TRIP/TWIP Steel. JOM 67, 1729–1747 (2015). https://doi.org/10.1007/s11837-015-1456-y
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11837-015-1456-y