Abstract
Pb(Zr0·52Ti0·48)O3 (PZT) powders were prepared by hydrothermal method. The effects of experimental parameters, including Pb/(Zr, Ti) ratio, alkaline concentration, reaction temperature and time on the product powders were studied in detail. Pure PZT powders were synthesized at suitable experimental conditions and Raman spectra confirmed the PZT with a perovskite-type structure. The homogeneous PZT powders with cubic-shaped morphology were formed at alkaline concentration of 1·2 M after reacting at 230°C for 2 h. The pure PZT powders obtained at low temperature and low alkaline concentration were attributed to precursors, TiCl4, with high activity and mineralizer NaOH with small cation radius.
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Qiu, ZC., Zhou, JP., Zhu, G. et al. Hydrothermal synthesis of Pb(Zr0·52Ti0·48)O3 powders at low temperature and low alkaline concentration. Bull Mater Sci 32, 193–197 (2009). https://doi.org/10.1007/s12034-009-0030-z
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DOI: https://doi.org/10.1007/s12034-009-0030-z