Abstract
The Fe3O4–Fe2O3 nanocomposites were prepared by the co-precipitation method and followed by calcination process. The products were synthesized and characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and energy-dispersive X-ray analysis. The obtained Fe3O4–Fe2O3 nanocomposites were then applied to study the electrocatalytic reduction of hydrogen peroxide (H2O2) in 0.01 M pH 7.0 phosphate buffer medium. Then the Fe3O4–Fe2O3 nanocomposites were used as active electrode material of electrochemical sensors for H2O2 detection The detection sensitivity of the sensor was 20.325 μA mM −1, and the detection limit was estimated to be about 0.2 mM.
Similar content being viewed by others
References
Klassen N V, Marchington D and Mcgowan H C E 1994 Anal. Chem. 66 2921
Salimi A, Hallaj R, Soltanian S and Mamkhezri H 2007 Anal. Chim. Acta 594 24
Yang Y J and Hu S 2010 Electrochim. Acta 55 3471
Song X C, Wang X, Zheng Y F, Ma R and Yin H Y 2011a J. Nanopart. Res. 13 1319
Diaz A N, Peinado M C R and Minguez M C T 1998 Anal. Chim. Acta 363 221
Tanner P A and Wong A Y S 1998 Anal. Chim. Acta 370 279
Cui K, Song Y H, Yao Y, Huang Z Z and Wang L 2008 Electrochem. Commun. 10 663
Miao X, Yuan R, Chai Y, Shi Y and Yuan Y 2008 J. Electroanal. Chem. 612 157
Jia W, Guo M, Zheng Z, Yu T, Rodriguez E G, Wang Y and Lei Y 2009 J. Electroanal. Chem. 625 27
Gu A, Wang G, Gua J, Zhang X and Fang B 2010 Electrochim. Acta 55 7182
Song X C, Wang X, Zheng Y F, Ma R and Yin H Y 2011b J. Nanopart. Res. 13 5449
Song M, Hwang S W and Whang D 2010 Talanta 80 1648
Tural B, Ozkan N and Volkan M 2009 J. Phys. Chem. Solids 70 860
Wang N, Zhu L, Wang M, Wang D and Tang H 2010 Ultrasonics Sonochem. 17 78
Song X C, Zheng Y F and Yin H Y 2013 J. Nanopart. Res. 15 1856
Wang Y, Cao J, Yu M, Sun G, Wang X, Bala H and Zhang Z 2013 Mater. Lett. 100 102
Yu C, Gou L, Zhou X, Bao N and Gu H 2011 Electrochim. Acta 56 9056
Hu Y, Li J, Zhang Z, Zhang H, Luo L and Yao S 2011 Anal. Chim. Acta 698 61
Shan H, Liu C, Liu L, Li S, Wang L, Zhang X, Bo X and Chi X 2013 Sens. Actuators B 184 243
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
CAO, G.S., WANG, P., LI, X. et al. A sensitive nonenzymatic hydrogen peroxide sensor based on Fe3O4–Fe2O3 nanocomposites. Bull Mater Sci 38, 163–167 (2015). https://doi.org/10.1007/s12034-014-0803-x
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s12034-014-0803-x