Abstract
In this paper, we report the compositional variation-dependent phase stability of hydroxyapatite (Ca10(PO4)6(OH)2) on doping with silver. The transformation of hydroxyapatite to (β/α) tricalcium phosphate phases during sintering has been explored using Raman spectroscopy and X-ray diffraction techniques. The optical absorption spectroscopy analysis reveals the presence of Ag+ ions at low doping levels. As the doping increases, abundance of Ag particles is enhanced.
Similar content being viewed by others
References
Osborn J F and Newesely H 1980 Biomaterials 1 108
Lee I S, Kim D H, Kim H E, Jung Y C and Han C H 2002 Biomaterials 23 609
Dorozhkin S V 2012 Acta Biomater. 8 963
Nath S, Biswas K and Basu B 2008 Scripta Mater. 58 1054
Li M, Wang Y, Liu Q, Li Q, Cheng Y, Zheng Y, Xi T and Wei S 2013 J. Mater. Chem. B 1 475
Aza PNde, Guitin F, Santos C, Aza Sde, Cusc R and Arts L 1997 Chem. Mater. 9 916
Kannan S, Rocha J H G, Ventura J M G, Lemos A F and Ferreira J M F 2005 Scripta Mater. 53 1259
Bezzi G, Celotti G, Landi E, Torretta T M G, Sopyan I and Tampieri A 2003 Mater. Chem. Phys. 78 816
Webster T J, Ergun C, Doremus R H, Siegel R W and Bizios R 2000a Biomaterials 21 1803
Webster T J, Ergun C, Doremus R H, Siegel R W and Bizios R 2000b J. Biomed. Mater. Res. 51 475
Kay M I, Young R A and Posner A S 1964 Nature 204 1050
LeGeros R Z, Taheri M H, Quirolgico G B and LeGeros J P 1980 Proc. 2nd. Int. Congr. Phosphorus Comp. Boston, Imphos, Paris 89
Williams R L, Doherty P J, Vince D G, Grashoff G J and Williams D F 1989 Crit. Rev. Biocompat. 5 221
Chena W, Liua Y, Courtney H S, Betteng M, Agrawal C M, Bumgardnere J D and Ong J L 2006 Biomaterials 27 5512
Singh B, Kumar S, Basu B and Gupta R 2013 Mater. Lett. 95 100
Han I H, Lee I S, Song J H, Lee M H, Park J C, Lee G H, Sun X D and Chung S M 2007 Biomed. Mater. 2 S91
Lee I S, Whang C N, Oh K S, Park J C, Lee K Y, Lee G H, Chung S M and Sun X D 2006 Nucl. Instr. Meth. Phys. Res. B 242 45
Singh B, Dubey A K, Kumar S, Saha N, Basu B and Gupta R 2011 Mater. Sci. Eng. C 31 1320
Singh B, Kumar S, Basu B and Gupta R 2013 Int. J. Appl. Ceram. Technol. doi: 10.1111/ijac.12167
Yashima M, Sakai A, Kamiyama T and Hoshikawab A 2003 J. Solid State Chem. 175 272
Costa A M, Soares G A, Calixto R and Rossi A M 2004 Key Eng. Mater. 254–256 119
Geoffrey I N, Graham A B and James B, Metson 2001 Phys. Chem. Chem. Phys. 17 3838
Pettinger B, Bao X, Wilcock I, Muhler M, Schlogl R and Ertl G 1994 Angew. Chem. Inf. Ed. End. 33 85
Bohren C F and Huffman D R, New York: Wiley 1983
Hansen W N and Prostak A 1968 Phase Rev. 174 500
Wang D S, Kerker M and Chew H 1990 Appl. Opt. 19 2135
Morones J R, Elechiguerra J L, Camacho A, Holt K, Kouri J B, Ramírez J T and Yacaman M J 2005 Nanotechnology 16 2346
Jiménez J A, Lysenko S and Liu H 2008 J. Appl. Phys. 104 054313
Acknowledgements
We acknowledge the financial support from the CSIR and DST, India. BS thanks Dr N P Lalla, IUC-DAEF, Indore, for assistance in TEM analysis.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
SINGH, B., KUMAR, S., SAHA, N. et al. Phase stability of silver particles embedded calcium phosphate bioceramics. Bull Mater Sci 38, 525–529 (2015). https://doi.org/10.1007/s12034-014-0839-y
Published:
Issue Date:
DOI: https://doi.org/10.1007/s12034-014-0839-y