Abstract
The technology for beneficiation of banded iron ores containing low iron value is a challenging task due to increasing demand of quality iron ore in India. A flotation process has been developed to treat one such ore, namely banded hematite quartzite (BHQ) containing 41.8wt% Fe and 41.5wt% SiO2, by using oleic acid, methyl isobutyl carbinol (MIBC), and sodium silicate as the collector, frother, and dispersant, respectively. The relative effects of these variables have been evaluated in half-normal plots and Pareto charts using central composite rotatable design. A quadratic response model has been developed for both Fe grade and recovery and optimized within the experimental range. The optimum reagent dosages are found to be as follows: collector concentration of 243.58 g/t, dispersant concentration of 195.67 g/t, pH 8.69, and conditioning time of 4.8 min to achieve the maximum Fe grade of 64.25% with 67.33% recovery. The predictions of the model with regard to iron grade and recovery are in good agreement with the experimental results.
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X. Ma., M. Marques, and C. Gontijo, Comparative studies of reverse cationic/anionic flotation of Vale iron ore, Int. J. Miner. Process., 100(2011), p. 179.
L. Rocha, R.Z.L. Cançado, and A.E.C. Peres, Iron ore slimes flotation, Miner. Eng., 23(2010), p. 842.
K. Quast, Flotation of hematite using C6-C18 saturated fatty acids, Miner. Eng., 19(2006), p. 582.
S. Montes-Sotomayor, R. Houot, and M. Kongolo, Flotation of silicated gangue iron ores: mechanism and effect of starch, Miner. Eng., 11(1998), p. 71.
H.D.G. Turrer and A.E.C. Peres, Investigation on alternative depressants for iron ore flotation, Miner. Eng. 23(2010), p.1066.
A.C. Araujo, P.R.M. Viana, and A.E.C. Peres, Reagents in iron ores flotation, Miner. Eng., 18(2005), p. 219.
L. Li, J.T. Liu, Y.T. Wang, Y.J. Cao, H.J. Zhang, and H.S. Yu, Experimental research on anionic reverse flotation of hematite with a flotation column, Procedia Earth Planet. Sci., 1(2009), p. 791.
H.T. Shen and X.Y. Huang, A review of technical progress in iron ore processing (2000–2004), Min. Metall. Eng. 25(2005), p. 26.
G.Q. Zhang, W.B. Li, and X.M. Bai, Research and practice of technological flowsheet of Qidashan iron mine, Met. Mine, 2006, No. 3, p. 37.
Y.H. Wang and J. W. Ren, The flotation of quartz from iron minerals with a combined quaternary ammonium salt, Int. J. Miner. Process., 77(2005), p. 116.
M. Pradip, Processing of alumina-rich Indian iron ore slimes, Int. J. Miner. Met. Mater. Eng., 59(2006), p. 551.
B. Das, B.K. Mishra, S. Prakash, S.K. Das, P.S.R. Reddy, and S.I. Angadi, Magnetic and flotation studies of banded hematite quartzite (BHQ) ore for the production of pellet grade concentrate, Int. J. Miner. Metall. Mater., 17(2010), p. 675.
B. Raj, B.S.S. Rao, and S. Chandra, Development of a process flow sheet for beneficiation of Indian banded hematite quartz (BHQ) iron ore, [in] Proceedings of Iron Ore Conference, Perth, 2007, p. 375.
Z.R. Lazic, Design of Experiments in Chemical Engineering, Wiley-VCH, Weinheim, 2004.
G.E.P. Box and K.B. Wilson, On the experimental attainment of optimum conditions, J. R. Stat. Soc. Ser. B, 13(1951), p. 1.
G.E.P. Box and J.S Hunter, Multi-factor experimental designs for exploring response surfaces, Ann. Math. Stat., 28(1957), p. 195.
J.S. Kwak, Application of Taguchi and response surface methodologies for geometric error in surface grinding process, Int. J. Mach. Tools Manuf., 45(2005), p. 327.
V. Gunaraj and N. Murugan, Application of response surface methodology for predicting weld bead quality in submerged arc welding of pipes, J. Mater. Process. Technol., 88(1999), p. 266.
N. Aslan, Application of response surface methodology and central composite rotatable design for modeling and optimization of a multi-gravity separator for chromite concentration, Powder Technol., 185(2008), p. 80.
P.K. Naik, P.S.R. Reddy, and V.N. Mishra, Optimization of coal flotation using statistical technique, Fuel Process. Technol., 85(2004), p. 1473.
A. Martínez-L, A. Uribe S, F.R. Carrillo P, J. Coreño A, and J.C. Ortiz, Study of celestite flotation efficiency using sodium dodecyl sulfonate collector: factorial experiment and statistical analysis of data, Int. J. Miner. Process., 70(2003), p. 83.
S. Kelebek, A. Khan, B. Wall, and J. Pettingil, Statistical evaluation of the effect of polyamine type in flotation of a Ni-Cu complex sulphide ore, [in] Proceedings of XXIII International Mineral Process Congress, 2006, p. 1830.
M.S. Sheridan, D.R. Nagaraj, D. Fornasiero, and J. Ralston, The use of a factorial experimental design to study collector properties of N-allyl-O-alkyl thionocarbamate collector in the flotation of a copper ore, Miner. Eng., 15(2002), p. 333.
J.V. Mehrabani, M. Noaparast, S.M. Mousavi, R. Dehghan, and A. Ghorbani, Process optimization and modelling of sphalerite flotation from a low-grade Zn-Pb ore using response surface methodology, Sep. Purif. Technol., 72(2010), p. 242.
R.D. Kulkarni and P. Somasundaran, Kinetics of oleate adsorption at the liquid/air interface and its role in hematite flotation, AIChE Symp. Ser., 71(1975), No. 150, p. 124.
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Rath, S.S., Sahoo, H. & Das, B. Optimization of flotation variables for the recovery of hematite particles from BHQ ore. Int J Miner Metall Mater 20, 605–611 (2013). https://doi.org/10.1007/s12613-013-0773-9
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DOI: https://doi.org/10.1007/s12613-013-0773-9