Skip to main content

Advertisement

Log in

Microstructure, Texture Evolution, and Mechanical Properties of ECAP-Processed ZAT522 Magnesium Alloy

  • Published:
Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

In this work, the high-strength Mg–5Zn–2Al–2Sn (ZAT522, in wt%) Mg alloys was obtained at 220 °C and 130 °C by a two-step equal channel angular pressing (ECAP). For each stage, two passes were used. The results showed a remarkable grain refinement after the first stage of ECAP (A2 samples), leading to a fine-grained structure with average size of 1.40 μm. The additional stage (A4 samples) caused further grain refinement to 1.18 μm, and an ultra-fine grain structure (700 nm) appeared in the precipitate-rich region. The grain refinement mechanism for both samples was discussed in detail. To this end, the original extrusion fiber texture evolved into a new strong texture characterized by the base planes tilted toward the ECAP shear plane, with a higher Schmid factor value of 0.34. Compared with the as-extruded alloy, the yield strength of the A2 samples increased from 180 to 245 MPa, which was mainly attributed to the combined effects of grain boundary strengthening and precipitation strengthening. In the case of A4 samples, the dislocation strengthening resulted in a net increase in yield strength to 335 MPa, while the ductility was significantly reduced.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

Similar content being viewed by others

References

  1. Z. Yang, J.P. Li, J.X. Zhang, G.W. Lorimer, J. Robson, Acta Metall. Sin. (Engl. Lett.) 21, 328 (2008)

    Google Scholar 

  2. J. Bai, Y.S. Sun, S. Xun, F. Xue, T.B. Zhu, Mater. Sci. Eng. A 419, 1 (2006)

    Article  CAS  Google Scholar 

  3. Y. Zhang, X.F. Huang, Z.D. Ma, Y. Li, F. Guo, J.C. Yang, Y. Ma, Y. Hao, Mater. Sci. Eng. A 686, 93 (2017)

    Article  CAS  Google Scholar 

  4. S.J. Meng, H. Yu, S.D. Fan, Q.Z. Li, S.H. Park, J.S. Suh, Y.M. Kim, X.L. Nan, M.Z. Bian, F.X. Yin, W.M. Zhao, B.S. You, K.S. Shin, Acta Metall. Sin. (Engl. Lett.) 32, 145 (2019)

    Article  CAS  Google Scholar 

  5. P. Cao, M.L. Zhang, W. Han, Y.D. Yan, L.J. Chen, Acta Metall. Sin. (Engl. Lett.) 25, 265 (2012)

    CAS  Google Scholar 

  6. B. Wang, X.H. Chen, F.S. Pan, J.J. Mao, Prog. Nat. Sci. 27, 695 (2017)

    Article  CAS  Google Scholar 

  7. Y. Wang, H.J. Wu, X.T. Liu, Y.L. Jiao, J.F. Sun, R.Z. Wu, L.G. Hou, J.H. Zhang, X.L. Li, M.L. Zhang, Mater. Sci. Eng. A 761, 138049 (2019)

    Article  CAS  Google Scholar 

  8. H.J. Wu, T.Z. Wang, R.Z. Wu, L.G. Hou, J.H. Zhang, X.L. Li, M.L. Zhang, J. Mater. Process. Tech. 254, 265 (2018)

    Article  CAS  Google Scholar 

  9. L.G. Hou, T.Z. Wang, R.Z. Wu, J.H. Zhang, M.L. Zhang, A.P. Dong, B.D. Sun, S. Betsofen, B. Krit, J. Mater. Sci. Technol. 34, 317 (2018)

    Article  Google Scholar 

  10. H. Liu, H. Huang, C. Wang, J.P. Sun, J. Bai, F. Xue, A.B. Ma, X.B. Cheng, Recent advances in LPSO-containing wrought magnesium alloys: relationships between processing, microstructure, and mechanical properties. JOM (2019). https://doi.org/10.1007/s11837-019-03610-9

    Article  Google Scholar 

  11. H. Liu, J. Ju, X.W. Yang, J.L. Yan, D. Song, J.H. Jiang, A.B. Ma, J. Alloys Compd. 704, 509 (2017)

    Article  CAS  Google Scholar 

  12. B. Srinivasarao, N.V. Dudamell, M.T. Pérez-Prado, Mater. Charact. 75, 101 (2013)

    Article  CAS  Google Scholar 

  13. B. Kima, C.H. Park, H.S. Kim, B.S. You, S.S. Park, Scr. Mater. 76, 21 (2014)

    Article  CAS  Google Scholar 

  14. Y.C. Yuan, A.B. Ma, X.F. Gou, J.H. Jiang, G. Arhin, D. Song, H. Liu, Mater. Sci. Eng. A 677, 216 (2016)

    Google Scholar 

  15. M. Gzyl, A. Rosochowski, S. Boczkal, L. Olejnik, Mater. Sci. Eng. A 638, 20 (2015)

    Article  CAS  Google Scholar 

  16. E. Mostaed, A. Fabrizi, D. Dellasega, F. Bonollo, M. Vedani, J. Alloys Compd. 638, 267 (2015)

    Article  CAS  Google Scholar 

  17. D.H. Shin, J.J. Pak, Y.K. Kim, K.T. Park, Y.S. Kim, Mater. Sci. Eng. A 323, 409 (2002)

    Article  Google Scholar 

  18. K. Huang, R.E. Logé, Mater. Des. 111, 548 (2016)

    Article  CAS  Google Scholar 

  19. K. Sheng, L.W. Lu, Y. Xiang, M. Ma, Z.C. Wang, Acta Metall. Sin. (Engl. Lett.) 32, 235 (2019)

    Article  CAS  Google Scholar 

  20. W.L. Cheng, L. Tian, S.C. Ma, Y. Bai, H.X. Wang, Materials 10, 708 (2017)

    Article  CAS  Google Scholar 

  21. F.-D. Dumitru, O.F. Higuera-Cobos, J.M. Cabrera, Mater. Sci. Eng. A 594, 32 (2014)

    Article  CAS  Google Scholar 

  22. R. Jahadi, M. Sedighi, H. Jahed, Mater. Sci. Eng. A 593, 178 (2014)

    Article  CAS  Google Scholar 

  23. T. Liu, W. Zhang, S.D. Wu, C.B. Jiang, S.X. Li, Y.B. Xu, Mater. Sci. Eng. A 360, 345 (2003)

    Article  CAS  Google Scholar 

  24. Y. Bai, W.L. Cheng, S.C. Ma, J. Zhang, C. Guo, Y. Zhang, Acta Metall. Sin. (Engl. Lett.) 31, 41 (2018)

    Google Scholar 

  25. Y.B. He, Q.L. Pan, Y.J. Qin, X.Y. Liu, W.B. Li, Y.L. Chiu, J. Chen, Chin. J. Nonferr. Metal. 20, 2274 (2010)

    CAS  Google Scholar 

  26. C.J. Wang, K.K. Deng, S.S. Zhou, W. Liang, Acta Metall. Sin. (Engl. Lett.) 29, 527 (2016)

    Article  CAS  Google Scholar 

  27. E. Mostaed, M. Hashempour, A. Fabrizi, D. Dellasega, M. Bestetti, F. Bonollo, M. Vedani, J. Mech. Behav. Biomed. 37, 307 (2014)

    Article  CAS  Google Scholar 

  28. A. Gholinia, P.B. Prangnell, M.V. Markushev, Acta Mater. 48, 1115 (2000)

    Article  CAS  Google Scholar 

  29. J. Koike, T. Kobayashi, T. Mukai, H. Watanabe, M. Suzuki, K. Maruyama, K. Higash, Acta Mater. 51, 2055 (2003)

    Article  CAS  Google Scholar 

  30. P. Yang, L.N. Wang, X. Li, L. Meng, Acta Metall. Sin. (Engl. Lett.) 23, 63 (2010)

    CAS  Google Scholar 

  31. N. Afrin, D.L. Chen, X. Cao, M. Jahazi, Scr. Mater. 57, 1004 (2007)

    Article  CAS  Google Scholar 

  32. J.L. Wang, Y.C. Guo, J.L. Li, Z. Yang, S. Kamado, L.M. Wang, J. Alloys Compd. 653, 100 (2015)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This study was supported by the National Natural Science Foundation of China (Grant Nos. 51874209 and 51771129).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Fu-Yin Han.

Additional information

Available online at http://link.springer.com/journal/40195

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ma, Y., Han, FY., Liu, C. et al. Microstructure, Texture Evolution, and Mechanical Properties of ECAP-Processed ZAT522 Magnesium Alloy. Acta Metall. Sin. (Engl. Lett.) 33, 233–242 (2020). https://doi.org/10.1007/s40195-019-00969-1

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s40195-019-00969-1

Keywords

Navigation