An N.M.R. study of the interactions between cadoxen and saccharides
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How alkaline solvents in viscosity measurements affect data for oxidatively damaged celluloses. Cuoxam and Cadoxen
2020, Carbohydrate PolymersCitation Excerpt :In contrast to cuen and cuoxam, no evidence has been provided of a carbohydrate-solvent complexes being formed upon dissolution. NMR investigations suggested that in this solvent rather an acid-base mechanism is involved in cellulose dissolution (Bain, Eaton, Hux, & Tong, 1980). Various natural and/or artificial processes (e.g. pulping, bleaching, natural aging, exposure to atmospheric contaminants and other chemicals) lead to the oxidation of cellulosic hydroxyl groups to carbonyls (and at C-6 subsequently also to carboxyls).
1D and 2D NMR of nanocellulose in aqueous colloidal suspensions
2014, Carbohydrate PolymersCitation Excerpt :The projection of 13C spectrum correlated with the proton nuclei was shown on the vertical axis and the projection of 1H spectrum correlated with the carbon nuclei was shown on the horizontal axis. The well resolved 13C NMR spectrum of cellulose had shown the most deshielded anomeric carbon at δ 102.00, followed by a less deshielded carbon C4 at δ 79.00–80.00 and the most shielded methylene carbon C6 at δ 60.00, with other C2, C3, and C5 signals at around δ 74.00 (Bain, Eaton, Hux, & Tong, 1980; Elkafrawy, 1982; Nehls, Wagenknecht, Philipp, & Stscherbina, 1994). The H1 at δ 4.45 was coupled with anomeric C1 at δ 102.1.
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