The evolution of TEOS to silica gel and glass by vibrational spectroscopy
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Ethyl silicate–nanolime treatment for the consolidation of calcareous building materials
2024, Construction and Building MaterialsUnveiling the elusive role of tetraethyl orthosilicate hydrolysis in ionic-liquid-templated zeolite synthesis
2022, Materials Today ChemistryCitation Excerpt :Various characterization methods, for example, electrospray ionization mass spectrometry [34–37]. Raman spectroscopy [38–40], infrared spectroscopy [41–48], and nuclear magnetic resonance [49–53] have been used to investigate the hydrolysis process of TEOS during the preparation of the synthesis solution and to account for the mechanism of zeolite crystallization. Despite substantial efforts, a clear correlation between TEOS hydrolysis and zeolite formation remains elusive.
Study on the structure change and devitrification of high silica glass particles with B<inf>2</inf>O<inf>3</inf> modification by Raman, IR and MAS NMR spectroscopies
2021, Journal of Non-Crystalline SolidsCitation Excerpt :The Raman spectra of high silica glass were shown in Fig. 2. There were a number of bands associated with organic functional groups in Raman spectra of xerogel that could be identified as follow according to references [17,18]. The band ∼874 cm−1 was assigned to CH3 or CH2 deformation (EtOH).