RESEARCH PAPERDetermination of Thirteen Antibiotics Residues in Manure by Solid Phase Extraction and High Performance Liquid Chromatography
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Vertical distribution of antibiotics and antibiotic resistance genes in a representative municipal solid waste landfill, China
2022, Ecotoxicology and Environmental SafetyCitation Excerpt :Five SAs (sulfadiazine, SDZ; sulfamerazine, SM1; sulfadimidine, SM2; sulfamethoxazole, SMZ; sulfadimethoxine, SMT), three TCs (oxytetracycline, OTC; tetracycline, TC; chlortetracycline, CTC), and two MLs (erythromycin, ETM; roxithromycin, RTM), were measured, due to the extensive use in medicine, agriculture and animal husbandry (Zhang et al., 2015). Antibiotics were extracted from 10 g (dry weight) refuse samples with 50 mL 0.1 M Na2EDTA-Mcllvaine buffer (Hu et al., 2008). The samples were vortex-mixed for 10 min and sonicated for 30 min.
Assessment of veterinary antibiotics from animal manure-amended soil to growing alfalfa, alfalfa silage, and milk
2021, Ecotoxicology and Environmental SafetySimultaneous extraction and determination of 45 veterinary antibiotics in swine manure by liquid chromatography-tandem mass spectrometry
2020, Journal of Chromatography B: Analytical Technologies in the Biomedical and Life SciencesCitation Excerpt :The reason may be that TCs are widely used in the animal breeding industry due to their low price. In addition, the three farms had different antibiotic residual levels, which may be due to the different drug application habits, and different fodder sources etc. [14]. A sensitive and reliable UHPLC-MS/MS method was developed and validated for the determination of 45 VAs in swine manure samples.
This work was supported by the grants from the National Science Foundation of China (No. 20777041) and Tianjin Municipal Science and Technology Commission of China (Grants 06TXTJJC14000).