Influence of loading rate on the delamination response of untufted and tufted carbon epoxy non-crimp fabric composites/Mode II
Graphical abstract
Highlights
► Dynamic delamination of NCF and tufted NCF in Mode II. ► Novel dynamic apparatus. ► Full dynamic optical analyses. ► Characterisation of rate effect detection during delamination.
Introduction
Composite shell structures reinforced by spars and ribs are in use in the aerospace, motorsport and marine industry. The structures can reach high speed and can sometimes collide with unexpected objects. Out of plane impact response is dictated by the resistance to delamination in Mode II for low speed impacts. Loading rate effects on the crack propagation in Mode II would therefore influence the response to impact of the laminate and the damage produced. It is consequently of particular interest to predict and understand the dynamic delamination in Mode II of composite laminates.
Textile composites offer reduced manufacturing time over pre-impregnated techniques by the use of resin infusion methods. The use of non-crimp fabrics consisting of two unidirectional (UD) plies stitched together increases the speed of draping and reduces the manufacturing time while maintaining an excellent in-plane response due to the reduced crimp compared to woven materials. However, the response to out of plane loading can be poor as the material is likely to delaminate, which can reduce the structural strength dramatically. Through the thickness reinforcement enhances the resistance to delamination considerably and is under investigation in this work.
Different experimental set ups can provide delamination Mode II measurements but none of them has been standardised. End notch flexural (ENF) specimen [1], end loaded split (ELS) [2] or short length specimens are possible test configurations to quantify delamination in Mode II. Dynamic experiments can be carried out via hydraulic test machines, drop towers or Hopkinson pressure bars. Smiley and Pipes [1] investigated the dependence of Mode II fracture toughness on strain rate via a screw-driven and a hydraulic testing machine (up to 0.092 m/s) with ENF type specimens. It was found that crack growth was changing from ductile to brittle mode as the rate of loading increased. This change resulted in a considerable drop in GIIC. Nwosu et al. [3] investigated Mode II delamination in graphite fibre epoxy specimens at high strain rate with a Split Hopkinson pressure bar and ENF and centre notch flexure CNF specimen configurations. Results showed that delamination resistance and energy absorbed in fracture increased with impact energy. Wu and Dzenis [4] used a three-point-bending and compact shearing set ups with a Hopkinson pressure bar and found no significant rate effects in Mode II. Cairn [5] used a modified ENF set up in a drop tower and registered superior fracture initiation and higher resistance to propagation under dynamic conditions. Tsai et al. [6] used a modified ENF tests in a drop weight tower in conjunction with a special insert film that delayed crack initiation allowing high crack speed to be reached. Using finite element analysis and experimental results it was concluded that no significant rate effects were achieved for crack speeds up to 1100 m/s. Using a similar set up Cantwell [7] detected positive rate sensitivity. It was also noticed that offsetting the interface by a few degrees would increase the rate sensitivity during testing. Using CNF and FE analysis Maikuma et al. [8] and Caimmi et al. [9] observed decreasing fracture energy for increasing loading rate on carbon composites with screw-driven or drop tower test devices. Caimmi et al. [9] utilised a new specimen set up called CENF (compact edge-notched shear specimen) and found increasing fracture energy with loading rates. With the use of ENF and drop weight loading on glass-fibre/vinyl-ester specimen Compston et al. [10] showed no significant rate effects. In general the results reported in the literature indicate some discrepancy due to the difference of delamination test set up, loading apparatus, and materials tested.
Through the thickness reinforcements by means of stitches were investigated in Mode II, static delamination in carbon epoxy laminates by Wood et al. [11]. It was found that the stitch effects could be measured but did not significantly improved the delamination resistance.
This research investigates the dynamic delamination behaviour of standard and tufted carbon NCF composites in Mode II. Results based on load cell readings and image recordings are presented and compared. The optical technique is utilised to investigate strain rate effects and to understand better the crack loading.
Section snippets
Specimen preparation
Tufted and untufted carbon non-crimp fabric textiles reinforced with high temperature RTM6 resin are investigated in this study. The tufts are prepared using 1 K carbon thread (Tenax HTA 5241 67 Tex F100 S15). The textile fabric is a 540 g/m2 NCF from Saertex. The textile fabric is infused with the resin at 120 °C, which is then post cured at 160 °C for 2 h. The specimen consists of a beam of dimensions 200 × 20 × 4.4 mm in which a pre-crack was introduced via the placement of a 63 mm long and 10 μm thin
Quasi static behaviour
The response of the tufted and untufted NCF composites is shown in Fig. 3a. The response of both materials was characterised by similar loading behaviour until crack initiation due to similar bending stiffness. In the case of the tufted NCF composites the specimen retained higher strength during crack initiation and propagation as the tufts failed at a higher shear force and at greater specimen bending than the resin interface. Also, when tufts failed they acted as a carbon sharp nail
Discussion
Unlike Mode I testing [Ref to part I] the use of an optical technique, for monitoring and capturing the crack propagation in Mode II at high speed is challenging. The Photron 1024PCI camera prove to be limited with low resolution (256 × 256) for frame rates ranging between 6000 and 10,000 images/s which made accurate crack tracking difficult. But the chance to use an alternative camera with advanced feature (Photron The SA1 camera with 1024 × 896 at 6250 frame per second) allows improved crack
Conclusion
Overall the presence of tufts are very beneficial on the dynamic Mode II response as it increased the energy absorption considerably, reduced crack speed significantly and bear a slight positive rate effect. The modified ELS apparatus and the optical analysis prove to provide interesting results for which load acquisition is not necessary. Further work could use similar setups but more emphasis should be given to the determination of the correction factor and to larger test programs to attempt
Acknowledgements
EU financial support through ITOOL/(ITOOL-FP6/516146) is acknowledged as well as support from J.P. Chubb, A.K. Pickett and D.D.R. Cartié.
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