Abstract
The behavior of N-2-pyridyl(maleic acid monoamide) in various hydrolyzing media has been studied. It is found that the substance is instantly hydrolyzed by 6 M CH3COOH under normal conditions to form 2-aminopyridine. The molar absorptivity of the hydrolyzate is several times higher than that of N-2-pyridyl(maleic acid monoamide) in various media, which can be used for the sensitive determination of the substance. A procedure for the spectrophotometric determination of N-2-pyridyl(maleic acid monoamide) has been developed.
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REFERENCES
Mikhailin, Yu.A. andMiichenko, I.P., Plast. Massy, 1992, no. 5, p. 56.
US Patent 4525536, 1986.
Japan Patent 61-1693 4, 1986.
Entsiklopediya polimerov (Encyclopedia of Polymers), Moscow: Sovetskaya Entsiklopediya, 1972, vol. 1.
Melent'eva, G.A. andAntonova, L.A., Farmatsevticheskaya khimiya (Pharmaceutical Chemistry), Moscow: Meditsina, 1993.
Korenman, I.M., Fotometricheskii analiz. Metody opredeleniya organicheskikh soedinenii (Photometric Analysis. Methods for Determination of Organic Compounds), Moscow: Khimiya, 1975.
Isaev, R.N.,Ishkov, A.V., andLobanova, T.V., Zh. Anal. Khim., 1999, vol. 54, no. 6, p. 608.
RF Patent 2106616, 1998, Byull. Izobret., 1998, no 7.
Fieser, L. andFieser, M., Reagents for Organic Synthesis, New York: Wiley, 1968-1975, 7 vols. Translated under the title Reagenty dlya organicheskogo sinteza, Moscow: Mir, 1970-1978.
US Patent 4626573, 1986.
Kazitsyna, L.A. andKupletskaya, N.B., Primenenie UF-, IK-, i YaMR-spektroskopii v organicheskoi khimii (Applications of UV, IR, and NMR Spectroscopy in Organic Chemistry), Moscow: Mosk. Gos. Univ., 1979, p. 86.
RF Patent 214 1646, 1999, Byull. Izobret., 1999, no. 32, p. 251.
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Isaev, R.N., Ishkov, A.V. & Lobanova, T.V. Spectrophotometric Determination of N-2-Pyridyl(maleic acid monoamide). Journal of Analytical Chemistry 56, 249–252 (2001). https://doi.org/10.1023/A:1009454522940
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DOI: https://doi.org/10.1023/A:1009454522940