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High-pressure studies with nuclear scattering of synchrotron radiation

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Abstract

The nuclear forward scattering (NFS) of synchrotron radiation is especially suited for probing magnetism at high pressure (h.p.), here in the Mbar range, by the nuclear resonances of 57Fe and 151Eu. We report on high-pressure NFS studies with the 14.4 keV transition of 57Fe, presenting at first the pressure induced α–ε transformation in iron. Then a systematic study of magnetic RFe2 Laves phases of cubic C15 structure (YFe2, GdFe2) and hexagonal C14 structure (ScFe2, TiFe2) at pressures up to 100 GPa (= 1 Mbar) is given. First, high-pressure NFS studies performed with the 21.5 keV resonance of 151Eu are also presented, probing valence transitions in EuNi2Ge2 and the magnetism in the CsCl-type h.p. phase of EuTe. Finally, we discuss future applications, such as high-pressure studies of phonon densities of states, using the inelastic channel of nuclear scattering of synchrotron radiation.

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References

  1. S.L. Ruby, J. Phys. C 6 (1974) 209.

    Google Scholar 

  2. E. Gerdau et al., Phys. Rev. Lett. 54 (1985) 835.

    Google Scholar 

  3. J.B. Hastings et al., Phys. Rev. Lett. 66 (1991) 770; U. van Bürck et al., Phys. Rev. B46 (1992) 6207; 558 R. Lübbers et al. / High-pressure studies with NFS IV-2.3 E. Gerdau and U. van Bürck, in: Resonant Anomalous X-Ray Scattering, Theory and Applications (Elsevier, Amsterdam, 1994) p. 589.

    Google Scholar 

  4. G. Faigel et al., Phys. Rev. Lett. 58 (1987) 2699; T. Ishikawa et al., Rev. Sci. Instrum. 63 (1992) 1015; T. Toellner et al., Proc. SPIE 1740 (1992) 218.

    Google Scholar 

  5. S. Kishimoto, Nucl. Instrum. Methods A 309 (1991) 603; A.Q.R. Baron et al., Nucl. Instrum. Methods A 343 (1994) 517 and ibid. 352 (1995) 665.

    Google Scholar 

  6. R.V. Pound and G.A. Rebka, Phys. Rev. Lett. 4 (1961) 337.

    Google Scholar 

  7. S. Nasu, Hyp. Interact. 90 (1994) 54.

    Google Scholar 

  8. R. Rüffer and A.I. Chumakov, Hyp. Interact. 97/98 (1996) 589; R. Rüffer et al., ESRF Newsletter 22 (1994) 12, and ESRF Highlights 1994/95, p. 36.

    Google Scholar 

  9. W. Sturhahn and E. Gerdau, Phys. Rev. B 49 (14) (1994) 9285.

    Google Scholar 

  10. A.Q.R. Baron et al., Phys. Rev. Lett. 77 (1996) 4808; see also this issue, section IV-3.1.

    Google Scholar 

  11. G. Cort, R.D. Taylor and J.O. Willis, J. Appl. Phys. 53 (1982) 2064 and 8199.

    Google Scholar 

  12. M.P. Pasternak et al., Phys. Rev. Lett. 79 (1997) 5046.

    Google Scholar 

  13. D.L. Williamson, in: Müssbauer Isomer Shifts (North-Holland, Amsterdam, 1978) p. 317.

    Google Scholar 

  14. M.P. Pasternak and R.D. Taylor, in: Müssbauer Spectroscopy Applied to Magnetism and Materials Science, Vol. 2 (Plenum Press, New York, 1996) p. 167.

    Google Scholar 

  15. R.A. Forman, G.J. Piermarini, J.D. Barnett and S. Block, Science 176 (1972) 284.

    Google Scholar 

  16. R. Lübbers, Diplom thesis, Paderborn (1994), unpublished.

  17. M. Seto et al., Phys. Rev. Lett. 74 (1995) 3828; W. Sturhahn et al., Phys. Rev. Lett. 74 (1995) 3832; A.I. Chumakov et al., Europhys. Lett. 30 (1995) 427.

    Google Scholar 

  18. A.I. Chumakov et al., Phys. Rev. B 54 (1996) 9596.

    Google Scholar 

  19. D. Bancroft, E.L. Peterson and S. Minshall, J. Appl. Phys. 27 (1956) 291.

    Google Scholar 

  20. D.N. Pipkorn et al., Phys. Rev. A 135(6) (1964) 1604.

    Google Scholar 

  21. D.L. Williamson, S. Bukshpan and R. Ingalls, Phys. Rev. B 6(11) (1972) 6126.

    Google Scholar 

  22. R.D. Taylor, M.P. Pasternak and R. Jeanloz, J. Appl. Phys. 69(8) (1991) 6126.

    Google Scholar 

  23. N. von Bargen and R. Boehler, High Pressure Res. 6 (1990) 133.

    Google Scholar 

  24. H.F. Grünsteudel et al., Hyp. Interact. C 1 (1996) 509.

    Google Scholar 

  25. H.F. Grünsteudel et al., Austral. J. Phys. 51 (1998) 453.

    Google Scholar 

  26. E. Burzo, A. Chelkowski and H. Kirchmayr, in: Landolt-Bürnstein New Series III, Vol. 19d2 (Springer, Berlin, 1990).

    Google Scholar 

  27. K. Mori et al., J. Alloys Compounds 270 (1998) 35.

    Google Scholar 

  28. Y. Nishihara and Y. Yamaguchi, J. Phys. Soc. Japan 54 (1985) 1122 and ibid 55 (1986) 920.

    Google Scholar 

  29. J. Lu, Dissertation, Universität Paderborn (1999).

  30. J. Lu et al., in: Conf. Proc., Vol. 50 (SIF, Bologna, 1996) p. 243.

    Google Scholar 

  31. G. Reiß et al., unpublished results; G. Reiß, Dissertation, Paderborn (1999).

  32. M. Strecker and G. Wortmann, Hyp. Interact. 120/121 (1999) 187.

    Google Scholar 

  33. D.J. Keavey et al., Phys. Rev. Lett. 74 (1995) 4531 and references therein.

    Google Scholar 

  34. M. Brouha and K.H.J. Buschow, J. Appl. Phys. 44 (1973) 1813.

    Google Scholar 

  35. J.M.G. Armitage et al., J. Phys. F., Metal. Phys. 16 (1986) L141.

    Google Scholar 

  36. E.P. Wohlfahrt, in: Physics of Solids under High Pressure (North-Holland, Amsterdam, 1981) p. 175.

    Google Scholar 

  37. O. Leupold et al., Europhys. Lett. 35 (1996) 671; see also this issue, section IV-2.7.

    Google Scholar 

  38. I. Koyama et al., Japan J. Appl. Phys. 35 (1996) 6297.

    Google Scholar 

  39. E.R. Bauminger, G.M. Kalvius and I. Nowik, in: Müssbauer Isomer Shifts (North-Holland, Amsterdam, 1978) p. 661.

    Google Scholar 

  40. I. Nowik, Hyp. Interact. 13 (1983) 89.

    Google Scholar 

  41. G. Wortmann et al., Phys. Rev. B 43 (1991) 5261.

    Google Scholar 

  42. H.-J. Hesse et al., J. Alloys Compounds 246 (1997) 220.

    Google Scholar 

  43. J. Moser, G. Wortmann and G.M. Kalvius, unpublished results.

  44. I.N. Goncharenko and I. Mirebeau, Europhys. Lett. 37 (1997) 633, and Phys. Rev. Lett. 80 (1998) 1082.

    Google Scholar 

  45. M. Pleines, Diplom thesis, University of Paderborn (1998), unpublished.

  46. M. Pleines et al., Hyp. Interact. 120/121 (1999) 181.

    Google Scholar 

  47. U.F. Klein et al., J. Magn. Magn. Mater. 3 (1976) 50.

    Google Scholar 

  48. J. Moser et al., J. Magn. Magn. Mater. 12 (1979) 77.

    Google Scholar 

  49. Ch. Sauer, A.M. Zaker and W. Zinn, J. Magn. Magn. Mater. 38 (1983) 225.

    Google Scholar 

  50. M.M. Abd-Elmeguid and R.D. Taylor, Phys. Rev. B 42 (1990) 11048.

    Google Scholar 

  51. A. Jayaraman et al., Phys. Rev. B 9 (1974) 2513.

    Google Scholar 

  52. L. Zhang et al., American Mineralogist 84 (1999) 447.

    Google Scholar 

  53. S. Kikuta, Hyp. Interact. 90 (1994) 335; E.E. Alp et al., Phys. Rev. Lett. 70 (1993) 3351; A.I. Chumakov et al., Phys. Rev. B 58 (1998) 254.

    Google Scholar 

  54. A. Barla et al., to be published.

  55. R. Lübbers et al., ESRF Report on experiment HS-583 (1998), and to be published.

  56. R. Lübbers et al., to be published.

  57. A. K. Freund et al., Proc. SPIE 3448 (1998) 1 and references therein.

  58. Di Fabrizio et al., J. Vac. Sci. Tech. B 11 (1998) 3855 and references therein.

  59. A. Snigirev et al., Nature 384 (1996) 49.

    Google Scholar 

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Lübbers, R., Wortmann, G. & Grünsteudel, H.F. High-pressure studies with nuclear scattering of synchrotron radiation. Hyperfine Interactions 123, 529–559 (1999). https://doi.org/10.1023/A:1017032125551

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