Issue 21, 2011
From the journal:

CrystEngComm

Hydrothermal synthesis of rutile TiO2 with hierarchical microspheres and their characterization

Sawanta S. Mali,a   Chirayath A. Betty,b   Popatrao N. Bhosalec  and  Pramod S. Patil*a  

* Corresponding authors

a Thin Film Materials Laboratory, Department of Physics, Shivaji University, Kolhapur, India
E-mail: psp_phy@unishivaji.ac.in, malisawantasubhash@gmail.com, sawantamali@yahoo.co.in
Fax: +91-0231-2691533
Tel: +91-231-2609229

b Chemistry Division, Bhabha Atomic Research Center (BARC), Trombay-Mumbai, India

c Materials Research Laboratory, Department of Chemistry, Shivaji University, Kolhapur, M. S. India

Abstract

Novel rutile TiO2 films with primary microspheres and secondary nanospheres have been deposited on glass substrates via a hydrothermal process by using titanium(IV) butoxide in the presence of toluene and HCl at 160 °C and time period varying from 4 to 8 h. The TiO2 films were characterized using XRD, SEM, FT-Raman, etc. techniques.

Graphical abstract: Hydrothermal synthesis of rutile TiO2 with hierarchical microspheres and their characterization

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Article information

DOI
https://doi.org/10.1039/C1CE05928A
Article type
Communication
Submitted
21 Jul 2011
Accepted
24 Aug 2011
First published
20 Sep 2011

CrystEngComm, 2011,13, 6349-6351

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Hydrothermal synthesis of rutile TiO2 with hierarchical microspheres and their characterization

S. S. Mali, C. A. Betty, P. N. Bhosale and P. S. Patil, CrystEngComm, 2011, 13, 6349 DOI: 10.1039/C1CE05928A

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