Issue 6, 1997

Synthesis of PbS nanocrystallites using a novel single molecule precursors approach: X-ray single-crystal structure of Pb(S2CNEtPri)2

Abstract

The synthesis and characterisation of some lead(ii) dithiocarbamato complexes Pb(S 2 CNRR′) 2 is reported. These compounds were used as single molecule precursors to produce nanocrystalline PbS by their thermolysis in trioctylphosphine oxide. The optical and morphological properties of the resulting PbS nanocrystallites were investigated; the influence of experimental parameters, such as precursor, growth time and temperature, on the final nanodispersed materials is also reported.

Article information

Article type
Paper

J. Mater. Chem., 1997,7, 1011-1016

Synthesis of PbS nanocrystallites using a novel single molecule precursors approach: X-ray single-crystal structure of Pb(S2CNEtPri)2

T. Trindade, P. O’Brien, X. Zhang and M. Motevalli, J. Mater. Chem., 1997, 7, 1011 DOI: 10.1039/A608579B

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