Abstract
We have studied the effect of titanium glycerolate precursor heat treatment on the morphology, structure, and photocatalytic properties of titanium dioxide nanopowders.
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Hu, X., Li, G., and Yu, J.C., Design, fabrication, and modification of nanostructured semiconductor materials for environmental and energy applications, Langmuir, 2010, vol. 26, no. 5, pp. 3031–3039.
Chen, X. and Mao, S.S., Titanium dioxide nanomaterials: Synthesis, properties, modifications, and applications, Chem. Rev., 2007, vol. 107, no. 7, pp. 2891–2959.
Ismagilov, Z.R., Tsikoza, L.T., Shikina, N.V., et al., Synthesis and stabilization of nanoparticulate titania, Usp. Khim., 2009, vol. 78, no. 9, pp. 942–955.
Priya, S., Robichaud, J., Méthot, M.-C., et al., Transformation of microporous titanium glycolate nanorods into mesoporous anatase titania nanorods by hot water treatment, J. Mater. Sci., 2009, vol. 44, no. 24, pp. 6470–6483.
Wang, D., Yu, R., Chen, Y., et al., Photocatalysis property of needle-like TiO2 prepared from a novel titanium glycolate precursor, Solid State Ionics, 2004, vol. 172, nos. 1–4, pp. 101–104.
Shankar, K., Basham, J.I., Allam, N.K., et al., Recent advances in the use of TiO2 nanotube and nanowire arrays for oxidative photoelectrochemistry, J. Phys. Chem. C, 2009, vol. 113, no. 16, pp. 6327–6359.
Zhou, W., Liu, H., Boughton, R.I., et al., One-dimensional single-crystalline Ti-O based nanostructures: Properties, synthesis, modifications and applications, J. Mater. Chem., 2010, vol. 20, no. 29, pp. 5993–6008.
Das, J., Freitas, F.S., Evans, I.R., et al., A facile nonaqueous route for fabricating titania nanorods and their viability in quasi-solid-state dye-sensitized solar cells, J. Mater. Chem., 2010, vol. 20, no. 21, pp. 4425–4431.
Wang, P., Xie, T., Peng, L., et al., Water-assisted synthesis of anatase TiO2 nanocrystals: Mechanism and sensing properties to oxygen at room temperature, J. Phys. Chem. C, 2008, vol. 112, no. 17, pp. 6648–6652.
Tian, G., Chen, Y., Bao, H.-L., et al., Controlled synthesis of thorny anatase TiO2 tubes for construction of Ag-AgBr/TiO2 composites as highly efficient simulated solar-light photocatalyst, J. Mater. Chem., 2012, vol. 22, no. 5, pp. 2081–2088.
Zakharova, G.S., Jähne, C., Popa, A., et al., Anatase nanotubes as an electrode material for lithium-ion batteries, J. Phys. Chem. C, 2012, vol. 116, no. 15, pp. 8714–8720.
Zakharova, G.S. and Andreikov, E.I., Effect of the precursor heat treatment procedure on the properties of titania photocatalysts, Inorg. Mater., 2012, vol. 48, no. 7, pp. 727–731.
Inoue, M., Glycothermal synthesis of metaloxides, J. Phys.: Condens. Matter, 2004, vol. 16, no. 14, pp. S1291–S1303.
Wang, D., Yu, R., Kumada, N., and Kinomura, N., Hydrothermal synthesis and characterization of a novel one-dimensional titanium glycolate complex single crystal: Ti(OCH2CH2O)2, Chem. Mater., 1999, vol. 11, no. 8, pp. 2008–2012.
Jiang, X., Wang, Y., Herricks, T., and Xia, Y., Ethylene glycol-mediated synthesis of metal oxide nanowires, J. Mater. Chem., 2004, vol. 14, no. 4, pp. 695–703.
Václav., Bakardjieva, S. Murafa, N., et al., Preparation and characterization of titania based nanowires, J. Nanopart. Res., 2007, vol. 9, no. 3, pp. 455–470.
Yu, H.K., Yi, G.-R., Kang, J.-H., et al., Surfactantassisted synthesis of uniform titania microspheres and their clusters, Chem. Mater., 2008, vol. 20, no. 8, pp. 2704–2710.
Krasil’nikov, V.N., Shtin, A.P., Gyrdasova, O.I., et al., Synthesis and properties of titanium glycolate Ti(OCH2CH2O)2, Russ. J. Inorg. Chem., 2008, vol. 53, no. 7, pp. 1065–1069.
Jiang, J., Gu, F., Shao, W., and Li, C., Fabrication of spherical multi-hollow TiO2 nanostructures for photoanode film with enhanced light-scattering performance, Ind. Eng. Chem. Res., 2012, vol. 51, no. 7, pp. 2838–2845.
Dou, B., Dupont, V., Williams, P.T., et al., Thermogravimetric kinetics of crude glycerol, Bioresour. Technol., 2009, vol. 100, no. 9, pp. 2613–2620.
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Original Russian Text © G.S. Zakharova, E.I. Andreikov, V.A. Osipova, Yu.G. Yatluk, I.S. Puzyrev, 2013, published in Neorganicheskie Materialy, 2013, Vol. 49, No. 11, pp. 1216–1221.
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Zakharova, G.S., Andreikov, E.I., Osipova, V.A. et al. Effect of the titanium glycerolate precursor heat treatment procedure on the morphology and photocatalytic properties of TiO2 nanopowder. Inorg Mater 49, 1127–1132 (2013). https://doi.org/10.1134/S0020168513100154
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DOI: https://doi.org/10.1134/S0020168513100154