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Erschienen in: Physics of Metals and Metallography 2/2021

01.02.2021 | STRUCTURE, PHASE TRANSFORMATIONS, AND DIFFUSION

The Effect of Electron Beam Welding on the Microstructure and Microhardness of 3D-Printed Products from Titanium Alloy Ti–6Al–4V

verfasst von: E. N. Boyangin, O. B. Perevalova, A. V. Panin, S. A. Martynov

Erschienen in: Physics of Metals and Metallography | Ausgabe 2/2021

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Abstract

The microstructure of double-sided welded joints of 3D-printed items made of titanium alloy Ti‒6Al–4V by the electron-beam freeform fabrication (EBF3) method has been investigated using the methods of X-ray diffraction analysis, optical metallography, and scanning and transmission electron microscopy. It is found that columnar epitaxial growth of primary β grains with transverse dimensions close to the sizes of primary β grains in the base material occurs in the process of electron-beam welding with a double-sided welded joint. Inside the primary β grains, there are grains of the α-phase with a lamellar shape inherited from the α' martensite, which is formed in the course of transformation β → α'. As in the printed samples, there is a nanocrystalline α"-phase in the metal of the welded joint inside grains of the α-phase and in interlayers of the β-phase. However, the density of particles of this phase in the metal of the welded joint is higher than in the base material. In the metal of the welded joint, tensile macrostresses and elastic residual microstrains also increase. The microhardness of the metal of the welded joint is greater than the microhardness of the base material.

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Literatur
1.
Zurück zum Zitat H. K. Rafi, N. V. Karthik, H. Gong, T. L. Starr, and B. E. Stucker, “Microstructures and mechanical properties of Ti6Al4V parts fabricated by selective laser melting and electron beam melting,” J. Mater. Eng. Perform. 22, No. 12, 3872–3883 (2013).CrossRef H. K. Rafi, N. V. Karthik, H. Gong, T. L. Starr, and B. E. Stucker, “Microstructures and mechanical properties of Ti6Al4V parts fabricated by selective laser melting and electron beam melting,” J. Mater. Eng. Perform. 22, No. 12, 3872–3883 (2013).CrossRef
2.
Zurück zum Zitat D. Zhang, S. Sun, D. Qiu, M. A. Gibson, M. S. Dargusch, M. Brandt, M. Qian, and M. Easton, “Metal alloys for fusion-based additive manufacturing,” Adv. Eng. Mater. 20, 1700952 (2018).CrossRef D. Zhang, S. Sun, D. Qiu, M. A. Gibson, M. S. Dargusch, M. Brandt, M. Qian, and M. Easton, “Metal alloys for fusion-based additive manufacturing,” Adv. Eng. Mater. 20, 1700952 (2018).CrossRef
3.
Zurück zum Zitat S. F. Hasan, R. S. Casey, and H. Kazunori, “Metal additive manufacturing for microelectromechanical systems: titanium alloy (Ti–6Al–4V)-based nanopositioning flexure fabricated by electron beam melting,” Sens. Actuators, A 249, 284–293 (2016).CrossRef S. F. Hasan, R. S. Casey, and H. Kazunori, “Metal additive manufacturing for microelectromechanical systems: titanium alloy (Ti–6Al–4V)-based nanopositioning flexure fabricated by electron beam melting,” Sens. Actuators, A 249, 284–293 (2016).CrossRef
4.
Zurück zum Zitat A. K. Petrov, “Main directions in the development of additive technologies for micron-resolution printing,” Inorg. Mater. 53, No. 12, 1349–1359 (2017).CrossRef A. K. Petrov, “Main directions in the development of additive technologies for micron-resolution printing,” Inorg. Mater. 53, No. 12, 1349–1359 (2017).CrossRef
5.
Zurück zum Zitat V. V. Bashenko, Electron Beam Installations (Mashinostroenie, Moscow, 1972) [in Russian]. V. V. Bashenko, Electron Beam Installations (Mashinostroenie, Moscow, 1972) [in Russian].
6.
Zurück zum Zitat A. G. Illarionov and A. A. Popov, Technological and Operational Properties of Titanium Alloys (Izd-vo Ural. un-ta, Yekaterinburg, 2014) [in Russian]. A. G. Illarionov and A. A. Popov, Technological and Operational Properties of Titanium Alloys (Izd-vo Ural. un-ta, Yekaterinburg, 2014) [in Russian].
7.
Zurück zum Zitat Q. Wang, J. H. Liu, Z. X. Lu, and D. L. Chen, “Cyclic deformation of dissimilar welded joints between Ti–6Al–4V and Ti17 alloys: Effect of strain ratio,” Mater. Sci. Eng., A 598, 122–134 (2014).CrossRef Q. Wang, J. H. Liu, Z. X. Lu, and D. L. Chen, “Cyclic deformation of dissimilar welded joints between Ti–6Al–4V and Ti17 alloys: Effect of strain ratio,” Mater. Sci. Eng., A 598, 122–134 (2014).CrossRef
8.
Zurück zum Zitat J. Liu, X. Gao, L. Zhang, and J. Zhang, “Effects of the heterogeneity in the electron beam welded joint on mechanical properties of Ti6Al4V alloy,” J. Mater. Eng. Perform. 24, 319–328 (2015).CrossRef J. Liu, X. Gao, L. Zhang, and J. Zhang, “Effects of the heterogeneity in the electron beam welded joint on mechanical properties of Ti6Al4V alloy,” J. Mater. Eng. Perform. 24, 319–328 (2015).CrossRef
9.
Zurück zum Zitat X. Chen, J. Zhang, X. Chen, X. Cheng, and Z. Huang, “Electron beam welding of laser additive manufacturing Ti–6.5Al–3.5Mo–1.5Zr–0.3Si titanium alloy thick plate,” Vacuum 151, 116–121 (2018).CrossRef X. Chen, J. Zhang, X. Chen, X. Cheng, and Z. Huang, “Electron beam welding of laser additive manufacturing Ti–6.5Al–3.5Mo–1.5Zr–0.3Si titanium alloy thick plate,” Vacuum 151, 116–121 (2018).CrossRef
10.
Zurück zum Zitat H. Yu, F. Li, J. Yang, J. Shao, Z. Wang, and X. Zeng, “Investigation on laser welding of selective laser melted Ti–6Al–4V parts: Weldability, microstructure and mechanical properties,” Mater. Sci. Eng., A 712, 20–27 (2018).CrossRef H. Yu, F. Li, J. Yang, J. Shao, Z. Wang, and X. Zeng, “Investigation on laser welding of selective laser melted Ti–6Al–4V parts: Weldability, microstructure and mechanical properties,” Mater. Sci. Eng., A 712, 20–27 (2018).CrossRef
11.
Zurück zum Zitat A. Panin, M. Kazachenok, O. Perevalova, S. Martynov, A. Panina, and E. Sklyarova, “Continuous electron beam post-treatment of EBF3-fabricated Ti–6Al–4V parts,” Metals 9, No. 6, 699 (2019).CrossRef A. Panin, M. Kazachenok, O. Perevalova, S. Martynov, A. Panina, and E. Sklyarova, “Continuous electron beam post-treatment of EBF3-fabricated Ti–6Al–4V parts,” Metals 9, No. 6, 699 (2019).CrossRef
12.
Zurück zum Zitat S. S. Gorelik, L. N. Rastorguev, and Yu. A. Skakov, X‑ray and Electron-Optical Analysis (Metallurgiya, Moscow, 1970). S. S. Gorelik, L. N. Rastorguev, and Yu. A. Skakov, X‑ray and Electron-Optical Analysis (Metallurgiya, Moscow, 1970).
13.
Zurück zum Zitat O. B. Perevalova, A. V. Panin, and M. S. Kazachenok, “Effect of substrate cooling on the microstructure and phase composition of Ti–6Al–4V titanium based alloy products obtained using additive technologies”, Tech. Phys. 65, No. 3, 392–399 (2020).CrossRef O. B. Perevalova, A. V. Panin, and M. S. Kazachenok, “Effect of substrate cooling on the microstructure and phase composition of Ti–6Al–4V titanium based alloy products obtained using additive technologies”, Tech. Phys. 65, No. 3, 392–399 (2020).CrossRef
14.
Zurück zum Zitat A. A. Bondar, T. Ya. Velikanova, V. M. Danilenko, V. M. Dement’ev, E. V. Kozlov, G. M. Lukashenko, V. R. Sidorko, and D. M. Shtern, Stability of Phases and Phase Equilibria in Alloys of Transition Metals (Naukova Dumka, Kiev, 1991) [in Russian]. A. A. Bondar, T. Ya. Velikanova, V. M. Danilenko, V. M. Dement’ev, E. V. Kozlov, G. M. Lukashenko, V. R. Sidorko, and D. M. Shtern, Stability of Phases and Phase Equilibria in Alloys of Transition Metals (Naukova Dumka, Kiev, 1991) [in Russian].
15.
Zurück zum Zitat T. V. Pryadko, “Features of hydrogenation of Ti–V alloys,” Metallofiz. Nov. Tekhnol. 37, No. 2, 243–255 (2015).CrossRef T. V. Pryadko, “Features of hydrogenation of Ti–V alloys,” Metallofiz. Nov. Tekhnol. 37, No. 2, 243–255 (2015).CrossRef
16.
Zurück zum Zitat N. V. Kazantseva, I. V. Ezhov, N. I. Vinogradova, M. V. Il’inykh, A. S. Fefelov, D. I. Davydov, O. A. Oleneva, and M. S. Karabanalov,”Effect of built geometry on the microstructure and strength characteristics of the TI–6Al–4V alloy prepared by the selective laser melting,” Phys. Met. Metallogr. 119, No. 11, 1079–1086 (2018).CrossRef N. V. Kazantseva, I. V. Ezhov, N. I. Vinogradova, M. V. Il’inykh, A. S. Fefelov, D. I. Davydov, O. A. Oleneva, and M. S. Karabanalov,”Effect of built geometry on the microstructure and strength characteristics of the TI–6Al–4V alloy prepared by the selective laser melting,” Phys. Met. Metallogr. 119, No. 11, 1079–1086 (2018).CrossRef
17.
Zurück zum Zitat M. A. Murzinova, S. V. Zherebtsov, and G. A. Salishchev, “Dependence of the specific energy of the β/α interface in the VT6 titanium alloy on the heating temperature in the interval 600–975°C,” J. Exp. Theor. Phys. 122, 705–715 (2016).CrossRef M. A. Murzinova, S. V. Zherebtsov, and G. A. Salishchev, “Dependence of the specific energy of the β/α interface in the VT6 titanium alloy on the heating temperature in the interval 600–975°C,” J. Exp. Theor. Phys. 122, 705–715 (2016).CrossRef
18.
Zurück zum Zitat T. W. Duerig, J. Albrecht, D. Richter, and P. Fischer, “Formation and reversion of stress induced martensite in Ti–10V–2Fe–3Al,” Acta Metall. 30, 2161–2172 (1982).CrossRef T. W. Duerig, J. Albrecht, D. Richter, and P. Fischer, “Formation and reversion of stress induced martensite in Ti–10V–2Fe–3Al,” Acta Metall. 30, 2161–2172 (1982).CrossRef
19.
Zurück zum Zitat N. Kazantseva, P. Krakhmalev, M. Thuvander, I. Yadroitsev, N. Vinogradova, and I. Ezhov, “Martensitic transformations in Ti–6Al–4V (ELI) alloy manufactured by 3D printing,” Mater. Charact. 146, 101–112 (2018).CrossRef N. Kazantseva, P. Krakhmalev, M. Thuvander, I. Yadroitsev, N. Vinogradova, and I. Ezhov, “Martensitic transformations in Ti–6Al–4V (ELI) alloy manufactured by 3D printing,” Mater. Charact. 146, 101–112 (2018).CrossRef
20.
Zurück zum Zitat P. B. Hirsch, A. Howie, R. B. Nicholson, D. W. Pashley and M. J. Whelan, Electron Microscopy of Thin Crystals (Krieger Pub Co., 1977). P. B. Hirsch, A. Howie, R. B. Nicholson, D. W. Pashley and M. J. Whelan, Electron Microscopy of Thin Crystals (Krieger Pub Co., 1977).
21.
Zurück zum Zitat E. V. Kozlov, L. I. Trishkina, N. A. Popova, and N. A. Koneva, “Dislocation physics in the multilevel approach to plastic deformation,” Phys. Mesomech. 14, Nos. 5–6, 283–296 (2011).CrossRef E. V. Kozlov, L. I. Trishkina, N. A. Popova, and N. A. Koneva, “Dislocation physics in the multilevel approach to plastic deformation,” Phys. Mesomech. 14, Nos. 5–6, 283–296 (2011).CrossRef
22.
Zurück zum Zitat V. I. Trefilov, V. F. Moiseev, E. P. Pechkovskii, I. D. Gornaya, and A. D. Vasil’ev, Strain Hardening and Fracture of Polycrystalline Metals (Naukova dumka, Kiev, 1989) [in Russian]. V. I. Trefilov, V. F. Moiseev, E. P. Pechkovskii, I. D. Gornaya, and A. D. Vasil’ev, Strain Hardening and Fracture of Polycrystalline Metals (Naukova dumka, Kiev, 1989) [in Russian].
23.
Zurück zum Zitat Z. Yacen, L. Huiqun, Y. Danging, W. Bin, J. Yong, H. Tao, X. Yu, and Y. Qi. “Stress-induced α” phase in a beta Ti–19Nb–1/5Mo–4Zr–8Sn alloy,” Mater. Charact. 140, 247–258 (2018).CrossRef Z. Yacen, L. Huiqun, Y. Danging, W. Bin, J. Yong, H. Tao, X. Yu, and Y. Qi. “Stress-induced α” phase in a beta Ti–19Nb–1/5Mo–4Zr–8Sn alloy,” Mater. Charact. 140, 247–258 (2018).CrossRef
Metadaten
Titel
The Effect of Electron Beam Welding on the Microstructure and Microhardness of 3D-Printed Products from Titanium Alloy Ti–6Al–4V
verfasst von
E. N. Boyangin
O. B. Perevalova
A. V. Panin
S. A. Martynov
Publikationsdatum
01.02.2021
Verlag
Pleiades Publishing
Erschienen in
Physics of Metals and Metallography / Ausgabe 2/2021
Print ISSN: 0031-918X
Elektronische ISSN: 1555-6190
DOI
https://doi.org/10.1134/S0031918X21020034

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