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Synthesis of nanosized iron(III) oxide and study of its formation features

  • Synthesis and Properties of Inorganic Compounds
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Abstract

Nanosized iron(III) oxide has been obtained by thermolysis of iron(III) acetylacetonate using diphenyl ether as a dispersion medium. It has been shown that increase in thermolysis temperature from 180 to 250°C allows one to half the average size of Fe2O3 nanoparticles. The introduction of surfactant into dispersion medium also leads to decrease of the average size of particles down to 4 nm. The phase composition of the prepared nano-Fe2O3 has been established, the possibility to reduce nano-Fe2O3 into iron metal has been shown by temperature-programmed reduction

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Authors and Affiliations

  1. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia

    A. S. Lyadov, A. A. Kochubeev, L. D. Koleva, O. P. Parenago & S. N. Khadzhiev

Authors
  1. A. S. Lyadov
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  2. A. A. Kochubeev
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  3. L. D. Koleva
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  4. O. P. Parenago
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  5. S. N. Khadzhiev
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Correspondence to A. S. Lyadov.

Additional information

Original Russian Text © A.S. Lyadov, A.A. Kochubeev, L.D. Koleva, O.P. Parenago, S.N. Khadzhiev, 2016, published in Zhurnal Neorganicheskoi Khimii, 2016, Vol. 61, No. 11, pp. 1440–1444.

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Lyadov, A.S., Kochubeev, A.A., Koleva, L.D. et al. Synthesis of nanosized iron(III) oxide and study of its formation features. Russ. J. Inorg. Chem. 61, 1387–1391 (2016). https://doi.org/10.1134/S0036023616110127

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  • DOI: https://doi.org/10.1134/S0036023616110127

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