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Licensed Unlicensed Requires Authentication Published by De Gruyter May 16, 2012

Analysis of DCM extractable components from hot-pressed hybrid poplar

  • Noridah B. Osman , Armando G. McDonald EMAIL logo and Marie-Pierre G. Laborie
From the journal Holzforschung

Abstract

The effects of thermal compression on the organic-soluble material of a uniform wood substrate, hybrid poplar (clone OP-367), has been studied. Poplar veneers were preconditioned to 0% or 8% moisture content and subsequently hot pressed at 150°C, 200°C, and 250°C. The dichloromethane (DCM) extracts were characterized by various hyphenated analyses [gas chromatography-mass spectrometry (GC-MS), analytical pyrolysis (Py-GC-MS), electrospray ionization-mass spectrometry (ESI-MS), and gel permeation chromatography (GPC)]. The yields and composition of extractable compounds were markedly influenced by treatment at 250°C compared to those obtained at lower temperatures. Most importantly, the organic extracts contained a significant portion of lignin-derived compounds after treatment at 250°C.


Corresponding author. Renewable Materials Program, Department of Forest, Rangeland, and Fire Science, University of Idaho, Moscow, ID 83844-1132, USA

Received: 2012-1-24
Accepted: 2012-4-4
Published Online: 2012-05-16
Published in Print: 2012-12-01

©2012 by Walter de Gruyter Berlin Boston

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