Skip to main content
SpringerLink
Log in

Preparation and characterization of nanosized zirconium (hydrous) oxide particles

  • Articles
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

A method for the preparation of nanosized zirconium (hydrous) oxide particles of narrow size distribution is described. The procedure yields stable dispersions at low temperatures and short reaction times in the absence of surfactants, using inorganic zirconium salts. Crystal structure, particle size distribution, electrokinetic properties, stability, and thermal behavior of the prepared particles were investigated. Colloidal dispersions were treated with ultrasound to study their effect on the crystal structure of the calcined samples.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. D. J. Clough, Ceram. Eng. Sci. Proc. 6, 1244 (1995).

    Article  Google Scholar 

  2. P. Hafenmuller and W. Van Gool, Solid Electrolytes (Academic Press, New York, 1978).

    Google Scholar 

  3. M. A. Blesa, A. J.G. Maroto, S. I. Passaggio, N. E. Figliolia, and G. Rigotti, J. Mater. Sci. 20, 4601 (1985).

    Article  CAS  Google Scholar 

  4. L. Lerot, F. Legrand, and P. Bruycker, J. Mater. Sci. 26, 2353 (1991).

    Article  CAS  Google Scholar 

  5. B. E. Yoldas, J. Mater. Sci. 21, 1080 (1986).

    Article  CAS  Google Scholar 

  6. M. Ocaña, V. Fornes, and C. J. Serna, Ceram. Int. 18, 99 (1992).

    Article  Google Scholar 

  7. T. Yoshioka, K. Dosaka, T. Sato, A. Okuwaki, S. Tanno, and T. Miura, J. Mater. Sci. Lett. 11, 51 (1992).

    Article  CAS  Google Scholar 

  8. H. Yue-Xiang and G. Cun-Ji, Powder Technol. 72, 101 (1992).

    Article  Google Scholar 

  9. B. Aiken, W. P. Hsu, and E. Matijević, J. Mater. Sci. 25, 1886 (1990).

    Article  CAS  Google Scholar 

  10. S. Ardizzone, M. G. Cattania, P. Lazzari, and P. Lugo, Colloids Surf. 90, 45 (1994).

    Article  CAS  Google Scholar 

  11. S. Komarneni, R. Roy, E. Breval, M. Ollinen, and Y. Suwa, Adv. Ceram. Mater. 1, 87 (1986).

    CAS  Google Scholar 

  12. P. E. D. Morgan, J. Am. Ceram. Soc. 69, C204 (1984).

    Google Scholar 

  13. E. Tani, M. Yoshimura, and S. Sōmiya, J. Am. Ceram. Soc. 66, 11 (1983).

    Article  CAS  Google Scholar 

  14. A. W. L. Dudeney, M. Abdel-Ghani, G. H. Kelsall, A. J. Monhemius, and L. Zhang, Powder Technol. 65, 207 (1991).

    Article  CAS  Google Scholar 

  15. Y. T. Moon, D.K. Kim, and C.H. Kim, J. Am. Ceram. Soc. 78, 1103 (1995).

    Article  CAS  Google Scholar 

  16. S. W. Provencher, Comput. Phys. Commun. 27, 215 (1982).

    Google Scholar 

  17. P. Scherrer, Gött. Nachr. 2, 98 (1918).

    Google Scholar 

  18. M. D. Rasmussen, G. W. Jordan, M. Akinc. O. Hunter, Jr., and M. F. Berard, Ceram. Int. 9, 59 (1983).

    Article  CAS  Google Scholar 

  19. D. M. Avila and E. N. S. Muccillo, Thermochim. Acta 256, 391 (1995).

    Article  CAS  Google Scholar 

  20. P. H. Tewari and W. Lee, J. Colloid Interface Sci. 52, 77 (1975).

    Article  CAS  Google Scholar 

  21. S. Ardizzone, G. Bassi, and G. Liborio, Colloids Surf. 51, 207 (1990).

    Article  CAS  Google Scholar 

  22. G. Ajay and E. Matijević, J. Colloid. Interface Sci. 126, 243 (1988).

    Article  Google Scholar 

  23. A. E. Regazzoni, M. A. Blesa, and A. J. G. Maroto, J. Colloid Interface Sci. 91, 560 (1983).

    Article  CAS  Google Scholar 

  24. G. W. Smith and T. Salmon, Can. Metall. Q. 5, 93 (1966).

    Article  CAS  Google Scholar 

  25. G. B. Amphlett, L. A. McDonald, and M. J. Redman, J. Inorg. Nucl. Chem. 6, 263 (1958).

    Article  Google Scholar 

  26. M. Schultz, St. Grimm, and Buckhardt, Solid State Ionics 63–65, 18 (1993).

    Article  Google Scholar 

  27. G. Parks, Chem. Rev. 65, 177 (1965).

    Article  CAS  Google Scholar 

  28. E. Matijević and M. Kerker, J. Phys. Chem. 62, 62 (1958).

    Article  Google Scholar 

  29. A. Koliadima, L. A. Pérez-Maqueda, and E. Matijević, Langmuir 13, 3733 (1997).

    Article  CAS  Google Scholar 

  30. G. Gimblett, A. A. Rahman, and K. S. W. Sing, J. Chem. Tech. Biotech. 30, 51 (1980).

    Article  CAS  Google Scholar 

  31. E. Crucean and B. Rand, Trans. J. Brit. Ceram. Soc. 78, 58 (1979).

    CAS  Google Scholar 

  32. A. Benedetti, G. Fagherazzi, F. Pinna, and S. Polizzi, J. Mater. Sci. 25, 1473 (1990).

    Article  CAS  Google Scholar 

  33. G. Štefanić, S. Popović, and S. Musić, Thermochim. Acta 259, 225 (1995).

    Article  Google Scholar 

  34. C. M. Phillipy and K. S. Mazdiyasni, J. Am. Ceram. Soc. 54, 254 (1971).

    Article  Google Scholar 

  35. K. S. Suslick, MRS Bull. 74, 29 (1995).

    Article  Google Scholar 

  36. A. Delgado and E. Matijević, Part. Part. Syst. Charact. 8, 128 (1991).

    Article  CAS  Google Scholar 

  37. R. Srinivasan, I. Z. Shirgaonkar, and A. B. Pandit, Sep. Sci. Technol. 30, 2239 (1995).

    Article  Google Scholar 

  38. T. Mitsuhashi, M. Ichihara, and U. Tatsuke, J. Am. Ceram. Soc. 57, 97 (1974).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Center for Advanced Materials Processing, Clarkson University, Potsdam, New York, 13699-5814, USA

    Luis A. Pérez-Maqueda & Egon Matijević

  2. On leave from Instituto de Ciencia de Materiales de Sevilla, Centro Mixto C.S.I.C., Universidad de Sevilla, Apdo. 1115, 41080, Sevilla, Spain

    Luis A. Pérez-Maqueda

Authors
  1. Luis A. Pérez-Maqueda
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Egon Matijević
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Pérez-Maqueda, L.A., Matijević, E. Preparation and characterization of nanosized zirconium (hydrous) oxide particles. Journal of Materials Research 12, 3286–3292 (1997). https://doi.org/10.1557/JMR.1997.0432

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/JMR.1997.0432

Search

Navigation