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Transmission electron microscopy and differential scanning calorimetry studies on the precipitation sequence in an Al-Mg-Si alloy: AA6022

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Abstract

The precipitate sequence in a 6022 aluminum alloy was investigated by means of differential scanning calorimetry (DSC), transmission electron microscopy, and Vickers hardness measurements. The solution-treated samples were quenched and then immediately subjected to DSC and isothermal aging experiments. It was observed that in the early stages of aging there are some unknown small precipitates that form prior to the formation of ß? precipitates. Studies on isothermally aged and DSC heated samples suggest that some of the ß? needles transform during growth to lath-shaped precipitates. An alternative precipitation sequence for AA6022 is proposed.

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References

  1. W.F. Miao and D.E. Laughlin: Effects of Cu content and pre-aging on precipitation characteristics in aluminum alloys 6022. Metall. Mater. Trans. A 31, 361 (2000).

    Article  Google Scholar 

  2. W.F. Miao and D.E. Laughlin: Precipitation hardening in aluminum alloy 6022. Scripta Mater. 40, 873 (1999).

    Article  CAS  Google Scholar 

  3. G.A. Edwards, K. Stiller, G.L. Dunlop and M.J. Couper: The precipitation sequence in Al-Mg-Si alloys. Acta Mater. 46, 3893 (1998).

    Article  CAS  Google Scholar 

  4. M. Murayama and K. Hono: Pre-precipitate clusters and precipitation processes in Al-Mg-Si alloys. Acta Mater. 47, 1537 (1999).

    Article  CAS  Google Scholar 

  5. I. Dutta and S.M. Allen: J. Mater. Sci. Lett. 10, 323 (1991).

    Article  CAS  Google Scholar 

  6. S.J. Andersen, H.W. Zandbergen, J. Jansen, C. TrÆholt, U. Tundal and O. Reiso: Crystal structure of the ß’ phase in Al-Mg-Si alloys. Acta Mater. 46, 3283 (1998).

    Article  CAS  Google Scholar 

  7. K. Matsuda, T. Naoi, Y. Uetani, T. Sato, A. Kamio and S. Ikeno: High resolution energy-filtering transmission electron microscopy for equilibrium ß-phase in an Al-Mg-Si alloy. Scripta Mater. 41, 379 (1999).

    Article  CAS  Google Scholar 

  8. D.J. Chakrabarti and E. Laughlin: Phase relations and precipitation in Al-Mg-Si alloys with Cu additions. Prog. Mater. Sci. 49, 389 (2004).

    Article  CAS  Google Scholar 

  9. C. Wolverton: Crystal structure and stability of complex precipitate phases in Al-Cu-Mg-(Si) and Al-Mg-Si alloys. Acta Mater. 49, 3129 (2001).

    Article  CAS  Google Scholar 

  10. J.D. Bryant: The effect of preageing treatments on ageing kinetics and mechanical properties in AA6111 aluminum autobody sheet. Metall. Mater. Trans. A 30, 1999 (1999).

    Article  Google Scholar 

  11. L. Zhen and S.B. Kang: DSC analyses of the precipitation behavior of two Al-Mg-Si alloys naturally aged for different times. Mater. Lett. 37, 349 (1998).

    Article  CAS  Google Scholar 

  12. M.H. Jacobs: The structure of the metastable precipitates formed during ageing of an Al-Mg-Si alloy. Philos. Mag. 26, 1 (1972).

    Article  CAS  Google Scholar 

  13. L. Sagalowicz, G. Hug, D. Bechet, P. Sainfort and G. Lapasset: Study of the structural precipitation in the Al-Mg-Si-Cu system, in Intl. Conf. of Al Alloys 4 (Trans Tech, Switzerland, 1994), p. 636.

    Google Scholar 

  14. C. Cayron, L. Sagalowicz, O. Beffort and P.A. Buffat: Structural phase transition in Al-Cu-Mg-Si alloys by transmission-electron-microscopy study on an Al-4 wt% Cu-1 wt% Mg-Ag alloy reinforced by SiC particles. Philos. Mag. 79, 2833 (1999).

    Article  CAS  Google Scholar 

  15. H. Westengen and N. Ryum: Precipitation reactions in an aluminium 1 wt% Mg2Si alloy. Z. Metallkde. 70, 528 (1979).

    CAS  Google Scholar 

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Correspondence to Reza S. Yassar.

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Yassar, R.S., Field, D.P. & Weiland, H. Transmission electron microscopy and differential scanning calorimetry studies on the precipitation sequence in an Al-Mg-Si alloy: AA6022. Journal of Materials Research 20, 2705–2711 (2005). https://doi.org/10.1557/JMR.2005.0330

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  • DOI: https://doi.org/10.1557/JMR.2005.0330

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