Skip to main content
Log in

A study on the growth and structure of titania nanotubes

  • Rapid Communications
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

Titania nanotubes synthesized by a soft chemical process are described, having diameters of 8 nm to 10 nm and lengths ranging from approximately 0.1 μm to 1 μm. X-ray diffraction studies show the structure of the as-prepared nanotubes is the same as that of the starting anatase TiO2 nanoparticles. Energy-dispersive x-ray analysis and electron energy loss spectroscopy studies further indicate that the as-prepared nanotubes are composed of titania. Studies using transmission electron microscopy verified that the nanotubes are formed during alkali treatment, with subsequent acidic treatments having no effect on nanotube structure and shape.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. O.K. Varghese, D. Gong, M. Paulose, K.G. Ong, E.C. Dickey, and C.A. Grimes, Adv. Mater. 15, 624 (2003).

    Article  CAS  Google Scholar 

  2. O.K. Varghese, D. Gong, M. Paulose, C.A. Grimes, and E.C. Dickey, J. Mater. Res. 17, 1162 (2002).

    Article  CAS  Google Scholar 

  3. J. Zou, L. Pu, X. Bao, and D. Feng, Appl. Phys. Lett. 80, 1079 (2002).

    Article  CAS  Google Scholar 

  4. L. Pu, X. Bao, J. Zou, and D. Feng, Angewante Chemie 113, 1538 (2001).

    Article  Google Scholar 

  5. D.W. Gong, C.A. Grimes, O.K. Varghese, Z. Chen, W.C. Hu, and E.C. Dickey, J. Mater. Res. 16, 3331 (2001).

    Article  CAS  Google Scholar 

  6. H-J. Muhr, F. Krumeich, U.P. Schonholzer, F. Bieri, M. Niederberger, L.J. Gauckler, and R. Nesper, Adv. Mater. 12, 231 (2000).

    Article  CAS  Google Scholar 

  7. C.N.R. Rao, B.C. Satishkumar, and A. Govindaraj, Chem. Commun. 16, 1581 (1997).

    Article  Google Scholar 

  8. P. Hoyer, Langmuir 12, 1411 (1996).

    Article  CAS  Google Scholar 

  9. T. Kasuga, M. Hiramatsu, A. Hoson, T. Sekino, and K. Niihara, Langmuir 14, 3160 (1998).

    Article  CAS  Google Scholar 

  10. Q.H. Zhang, L. Gao, J. Sun, and S. Zheng, Chem. Lett. 31, 226 (2002).

    Article  Google Scholar 

  11. M. Adachi, Y. Murata, M. Harada, and S. Yoshikawa, Chem. Lett. 29, 942 (2000).

    Article  Google Scholar 

  12. Y. Zhu, H. Li, Y. Koltypin, Y.R. Hacohen, and A. Gedanken, Chem. Commun. 24, 2616 (2001).

    Article  Google Scholar 

  13. H. Imai, Y. Takei, K. Shimizu, M. Matsuda, and H. Hirashima, J. Mater. Chem. 9, 2971 (1999).

    Article  CAS  Google Scholar 

  14. S.L. Zhang, J.F. Zhou, Z.J. Zhang, Z.L. Du, and A.V. Vorontsov, Chinese Sci. Bull. 45, 1104 (2000).

    Article  Google Scholar 

  15. G.H. Du, Q. Chen, R.C. Che, Z.Y. Yuan, and L.M. Peng, Appl. Phys. Lett. 79, 3702 (2001).

    Article  CAS  Google Scholar 

  16. T. Kasuga, M. Hiramatsu, A. Hoson, T. Sekino, and K. Niihara, Adv. Mater. 11, 1307 (1999).

    Article  CAS  Google Scholar 

  17. O.K. Varghese, M. Paulouse, D. Gong, C.A. Grimes, and E.C. Dickey, J. Mater. Res. 18, 156 (2003).

    Article  CAS  Google Scholar 

  18. X. Sun and Y. Li, Chem. Eur. J. 9, 2229 (2003).

    Article  CAS  Google Scholar 

  19. B.D. Yao, Y.F. Chan, X.Y. Zhang, W.F. Zhang, Z.Y. Yang, and N. Wang, Appl. Phys. Lett. 82, 281 (2003).

    Article  CAS  Google Scholar 

  20. T. Feist and P. Davies, J. Solid State Chem. 101, 275 (1992).

    Article  CAS  Google Scholar 

  21. Q. Chen, G.G. Du, S. Zhang, and L.M. Peng, Acta Cryst. B 58, 587 (2002).

    Article  CAS  Google Scholar 

  22. A. Chemseddine and T. Moritz, Eur. J. Inorg. Chem. 1999, 235 (1999).

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Wang, W., Varghese, O.K., Paulose, M. et al. A study on the growth and structure of titania nanotubes. Journal of Materials Research 19, 417–422 (2004). https://doi.org/10.1557/jmr.2004.19.2.417

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/jmr.2004.19.2.417

Navigation