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Characterization of the mechanical behavior of wear surfaces on single crystal nickel by nanomechanical techniques

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Abstract

In ductile metals, sliding contact induces plastic deformation resulting in subsurfaces, the mechanical properties of which are different from those of the bulk. This article describes a novel combination of nanomechanical test methods and analysis techniques to evaluate the mechanical behavior of the subsurfaces generated underneath a wear surface. In this methodology, nanoscratch techniques were first used to generate wear patterns as a function of load and number of cycles using a Hysitron TriboIndenter. Measurements were made on a (001) single crystal plane along two crystallographic directions, <001> and <011>. Nanoindentation was then used to measure mechanical properties in each wear pattern. The results on the (001) single crystal nickel plane showed that there was a strong increase in hardness with increasing applied load that was accompanied by a change in surface deformation. The amount of deformation underneath the wear patterns was examined from focused ion beam cross-sections of the wear patterns.

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References

  1. P. Heilmann, W.A.T. Clark, and D.A. Rigney: Orientation determination of subsurface cells generated by sliding. Acta Metall. 31, 1293 (1983).

    Article  CAS  Google Scholar 

  2. S.V. Prasad, J.K. Michael, and T.R. Christenson: EBSD studies on wear-induced subsurface regions in LIGA nickel. Scr. Mater. 48, 255 (2003).

    Article  CAS  Google Scholar 

  3. D.A. Rigney: The roles of hardness in the sliding behavior of materials. Wear 175, 63 (1994).

    Article  Google Scholar 

  4. D.A. Rigney: Transfer, mixing and associated chemical and mechanical processes during the sliding of ductile materials. Wear 245, 1 (2000).

    Article  CAS  Google Scholar 

  5. A. Emge, S. Karthikeyan, H.J. Kim, and D.A. Rigney: The effect of sliding velocity on the tribological behavior of copper. Wear 263, 614 (2007).

    Article  CAS  Google Scholar 

  6. P. Heilmann, J. Don, T.C. Sun, D.A. Rigney, and W.A. Glaeser: Sliding wear and transfer. Wear 91, 171 (1983).

    Article  Google Scholar 

  7. D.A. Rigney: Large strains associated with sliding contact of metals. Mater. Res. Innov. 1, 231 (1998).

    Article  CAS  Google Scholar 

  8. D.A. Rigney, R. Divakar, and S.M. Kuo: Deformation substructures associated with very large plastic strains. Scr. Metall. 27, 975 (1992).

    Article  CAS  Google Scholar 

  9. D.A. Rigney and W.A. Glaeser: The significance of near surface microstructure in the wear process. Wear 46, 241 (1978).

    Article  CAS  Google Scholar 

  10. K.F. Dufrane and W.A. Glaeser: Rolling-contact deformation of MgO single crystals. Wear 37, 21 (1976).

    Article  Google Scholar 

  11. W.A. Glaeser: High strain wear mechanisms in ferrous alloys. Wear 123, 155 (1988).

    Article  CAS  Google Scholar 

  12. D. Tabor: The Hardness of Metals (Oxford University Press, NY, 1951).

    Google Scholar 

  13. W.C. Oliver and G.M. Pharr: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 (1992).

    Article  CAS  Google Scholar 

  14. M.J. Cordill, N.R. Moody, and W.W. Gerberich: Effects of dynamic indentation on the mechanical response of materials. J. Mater. Res. 23, 1604 (2008).

    Article  CAS  Google Scholar 

  15. K. Durst, O. Franke, A. Bohner, and M. Goken: Indentation size effect in Ni-Fe solid solutions. Acta Mater. 55, 6825 (2007).

    Article  CAS  Google Scholar 

  16. T.E. Buchheit, D.A. LaVan, J.R. Michael, T.R. Christensen, and S.D. Leith: Microstructural and mechanical properties investigation of electrodeposited and annealed LIGA nickel structures. Metall. Mater. Trans. A 33, 539 (2002).

    Article  Google Scholar 

  17. W.H. Safranek: The Properties of Electrodeposited Metals and Alloys, a Handbook (American Electroplaters Society, Orlando, FL, 1986).

    Google Scholar 

  18. J.W. Dini: Electrodeposition (Noyes Publications, Park Ridge, NJ, 1993).

    Google Scholar 

  19. A. Romanowski: Impact of the heat generation of the primary scanning beam on the sem-ebic characteristics. Phys. Status Solidi 88, 663 (1985).

    Article  CAS  Google Scholar 

  20. I. Ishitani and H. Kaga: Calculation of local temperature rise in focused-ion-beam sample preparation. J. Electron Microsc. 44, 331 (1995).

    CAS  Google Scholar 

  21. L.A. Giannuzzi and F.A. Stevie: Introduction to Focused Ion Beams: Instrumentation, Theory, Techniques and Practice (Springer, NY, 2005).

    Book  Google Scholar 

  22. M.S. Bobji and S.K. Biswas: Deconvolution of hardness from data obtained from nanoindentation of rough surfaces. J. Mater. Res. 14, 2259 (1999).

    Article  CAS  Google Scholar 

  23. D.L. Joslin and W.C. Oliver: A new method for analyzing data from continuous depth-sensing microindentation tests. J. Mater. Res. 5, 123 (1990).

    Article  CAS  Google Scholar 

  24. T.F. Page, G.M. Pharr, J.C. Hay, W.C. Oliver, B.N. Lucas, E. Herbert, and L. Riester: Nanoindentation characterization of coated systems: P/S2. A new approach using the continuous stiffness technique, in Fundamentals of Nanoindentation and Nano-tribology, edited by N.R. Moody, W.W. Gerberich, N. Burnham, and S.P. Baker (Mater. Res. Soc. Symp. Proc. 522, Warrendale, PA, 1998), pp. 53–64.

    CAS  Google Scholar 

  25. K. Hokkirigawa and K. Kato: An experimental and theoretical investigation of ploughing, cutting and wedge formation during abrasive wear. Tribol. Int. 21, 51 (1988).

    Article  CAS  Google Scholar 

  26. K.L. Johnson: Contact Mechanics (Cambridge University Press, Cambridge, 1985).

    Book  Google Scholar 

  27. D. Kramer, H. Huang, M. Kriese, J. Robach, J. Nelson, A. Wright, D.F. Bahr, and W.W. Gerberich: Yield strength predictions from the plastic zone around nanocontacts. Acta Mater. 47, 333 (1999).

    Article  CAS  Google Scholar 

  28. N.I. Tymiak, D.E. Kramer, D.F. Bahr, T.J. Wyrobek, and W.W. Gerberich: Plastic strain and strain gradients at very small indentation depths. Acta Mater. 49, 1021 (2001).

    Article  CAS  Google Scholar 

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Correspondence to M. J. Cordill.

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This author was an editor of this focus issue during the review and decision stage. For the JMR policy on review and publication of manuscripts authored by editors, please refer to http://www.mrs.org/jmr_policy

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Cordill, M.J., Moody, N.R., Prasad, S.V. et al. Characterization of the mechanical behavior of wear surfaces on single crystal nickel by nanomechanical techniques. Journal of Materials Research 24, 844–852 (2009). https://doi.org/10.1557/jmr.2009.0075

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  • DOI: https://doi.org/10.1557/jmr.2009.0075

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