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Effect of mineral additives on the setting of blended cement by the maturity method

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Abstract

The addition of a mineral additive to Portland cement involves an increase of the setting time allotted to the dilution effect (dilution of the most active ingredient) and to the increase in the necessary water to prepare a normal consistency paste. In this study, ordinary cement was substituted by 5, 15 and 25% of limestone powder, 10, 20 and 30% of natural pozzolan and 10, 30 and 50% of slag. The tests of penetration are carried out every 10 min in order to determine initial and final setting time. The mortar is prepared and preserved at curing temperature of 20, 40 and 60°C. The results are analyzed and quantified by using the maturity method where the effect of each addition appears more explicit. The value of the activation energy calculated at the very early age reveals the state of activity of these mineral additives and their temperature sensitivity. For replacement amounts lower than 15%, the activation energy of the three additives increases at the initial setting and beyond this content a clear difference is observed. At the final setting time, the activation energy remains constant for limestone, increases regularly for slag and increases highly for natural pozzolan with replacement amounts above than 20%.

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References

  1. Alshamsi M, Sabouni AR, Bashlaibi AH (1993) Influence of set-retarding superplasticizer and microsilica on setting time of pastes at various temperatures. Cem Concr Res 23(3):592–598. doi:10.1016/0008-8846(93)90009-X

    Article  Google Scholar 

  2. Baron J, Ollivier JP (1996) Les bétons: bases et données pour leurs formulation. Edition Eyrolles, France, 522 p

  3. Bougara A, Ezziane K, Kadri A (2001) Prédiction de la résistance du ciment au laitier durcissant sous une température variable. Can J Civ Eng 28(4):555–561. doi:10.1139/cjce-28-4-555

    Article  Google Scholar 

  4. Brooks JJ, Megat Johari MA, Mazloom M (2000) Effect of admixtures on the setting times of high-strength concrete. Cem Concr Compos 22(4):293–301. doi:10.1016/S0958-9465(00)00025-1

    Article  Google Scholar 

  5. Carino NJ (1994) The maturity method: theory and application. Cem Concr Aggreg 6(2):61–73

    Google Scholar 

  6. Chanvillard G, D’Aloia L (1997) Concrete strength estimation at early age: modification of the method of equivalent age. ACI Mater J 94(6):520–530

    Google Scholar 

  7. Elkhadiri I, Diouri A, Boukhari A, Aride J, Puertas F (2002) Mechanical behaviour of various mortars made by combined fly ash and limestone in Moroccan Portland cement. Cem Concr Res 32(10):1597–1603. doi:10.1016/S0008-8846(02)00834-7

    Article  Google Scholar 

  8. Gesoglu M, Erdogan Ozbay E (2007) Effects of mineral admixtures on fresh and hardened properties of self-compacting concretes: binary, ternary and quaternary systems. Mater Struct 40:923–937. doi:10.1617/s11527-007-9242-0

    Article  Google Scholar 

  9. Ezziane K, Bougara A, Kadri A, Khelafi H, Kadri E (2007) Compressive strength of mortar containing natural pozzolan under various curing temperature. Cem Concr Compos 29(8):587–593. doi:10.1016/j.cemconcomp.2007.03.002

    Article  Google Scholar 

  10. Kanstad T, Hammer TA, Bjantegaard IO, Sellevold EJ (2003) Mechanical properties of young concrete: Part I. Experimental results related to test methods and temperature effects. Mater Struct 36:218–225

    Google Scholar 

  11. Konsta-Gdoutos MS, Shah SP (2003) Hydration and properties of novel blended cements based on cement kiln dust and blast furnace slag. Cem Concr Res 33(8):1269–1276. doi:10.1016/S0008-8846(03)00061-9

    Article  Google Scholar 

  12. Malhotra VM (ed) (1987) Supplementary cementing materials for concrete. CANMET Publ, SP 86-8E, CANADA, 428p

  13. Moulin E, Blanc P (2001) Properties of artificial pozzolan blended cements as a function of clay precursor mineralogy and cement chemical parameters. In: Proceedings of the 7th CANMET/ACI international conference on fly ash, silica fume, slag and natural pozzolans in concrete, Chennai (Madras), India, pp 361–377

  14. Naik TR, Singh SS (1997) Influence of fly ash on setting and hardening characteristics of concrete systems. ACI Mater J 94(5):355–360

    Google Scholar 

  15. Naik TR, Singh SS, Ramme BW (2001) Time of setting influenced by inclusion of ash and chemical admixtures. In: Proceedings of the 7th CANMET/ACI international conference on fly ash, silica fume, slag and natural pozzolans in concrete, Chennai (Madras), India, pp 393–413

  16. Neville M (2000) Propriétés des bétons. Edition Eyrolles, France, 805p

  17. NF EN 196-3 (1990) Méthodes d’essais de ciment, Détermination du temps de prise et du de la stabilité, Mars, 10 p

  18. Pinto CA, Hover KC (1999) Application of maturity approach to setting time. ACI Mater J 96(6):686–691

    Google Scholar 

  19. Ravindrarajah R, Tam CT (1989) Properties of concrete containing low calcium fly ash under hot and humid climate. In: Proceedings of the 3th CANMET/ACI international conference on fly ash, silica fume, slag and natural pozzolans in concrete, Trondheim, Norway, pp 139–155

  20. Targana S, Olgun A, Erdogan Y, Sevinc V (2003) Influence of natural pozzolan, colemanite ore waste, bottom ash, and fly ash on the properties of Portland cement. Cem Concr Res 33(8):1175–1182. doi:10.1016/S0008-8846(03)00025-5

    Article  Google Scholar 

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Ezziane, K., Kadri, E.H., Hallal, A. et al. Effect of mineral additives on the setting of blended cement by the maturity method. Mater Struct 43, 393–401 (2010). https://doi.org/10.1617/s11527-009-9498-7

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  • DOI: https://doi.org/10.1617/s11527-009-9498-7

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