Skip to main content
Log in

Fabrication of porous NiTi alloy via powder metallurgy and its mechanical characterization by shear punch method

  • Powder Materials and Coatings
  • Published:
Russian Journal of Non-Ferrous Metals Aims and scope Submit manuscript

Abstract

In this study, Porous NiTi shape memory alloy has been produced by mechanical alloying of the elemental Ni and Ti powders. The compacting process was done at two temperatures (warm and cold press) and then sintering at 980 and 1050°C was performed on the specimens. Microstructure and mechanical prop-erties of the samples were investigated by optical microscopy, scanning electron microscopy (SEM) and X-ray diffraction. Moreover, shear punch test (SPT) employed to investigate the effect of compaction pressure and sintering temperature on the mechanical properties of the fabricated samples. It was revealed that warm compaction/sintering resulted in 15% yield stress improvement and 20% ultimate tensile strength (UTS) enhancement with respect to conventionally produced specimens. The proposed approach in this paper seems a step forward towards fulfillment of the demand for heavy load-bearing artificial bone.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Bram, M., Ahmad-Khanlou, A., Heckmann, A., Fuchs, B., Buchkremer, H.P., and Stover, D., Powder Metallurgical Fabrication Processes for NiTi Shape Memory Alloy Parts, Mater. Sci. Eng. A, 2002, vol. 337, pp. 254–263.

    Article  Google Scholar 

  2. Otsuka, K. and Ren, X., Physical Metallurgy of Ti-Ni-Based Shape Memory Alloys, Prog. Mater Sci., 2005, vol. 50, pp. 511–678.

    Article  CAS  Google Scholar 

  3. Prymak, O., Bogdanski, D., Koller, M., Esenwein, S.A., Muhr, G., Beckmann, F., Donath, T., Assad, M., and Epple, M., Morphological Characterization and in vitro Biocompatibility of a Porous Nickel-Titanium Alloy, Biomaterials, 2005, vol. 26, pp. 5801–5807.

    Article  CAS  Google Scholar 

  4. Greiner, C., Oppenheimer, S.M., and Dunand, D.C., High Strength, Low Stiffness, Porous NiTi with Superelastic Properties, Acta Biomater., 2005, vol. 1, pp. 705–716.

    Article  Google Scholar 

  5. Chu, C.L., Chung, C.Y., Lin, P.H., and Wang, S.D., Fabrication and Properties of Porous NiTi Shape Memory Alloys for Heavy Load-Bearing Medical Applications Journal of Materials Processing Technology, J. Mater. Process. Technol., 2005, vol. 169, pp. 103–107.

    Article  CAS  Google Scholar 

  6. Li, Y.H., Rong, L.J., and Li, Y.Y., Pore Characteristics of Porous NiTi Alloy Fabricated by Combustion Synthesis, Journal of Alloys and Compounds, J. Alloys Compd., 2001, vol. 325, pp. 259–262.

    Article  CAS  Google Scholar 

  7. Yuan, B., Chung, C.Y., and Zhu, M., Microstructure and Martensitic Transformation Behavior of Porous NiTi Shape Memory Alloy Prepared by Hot Isostatic Pressing Processing, Mater. Sci. Eng. A, 2004, vol. 181, p. 382.

    Google Scholar 

  8. Schüller, E., Bram, M., Buchkremer, H.P., and Stöver, D., Phase Transformation Temperatures for NiTi Alloys Prepared by Powder Metallurgical Processes, Mater. Sci. Eng. A, 2004, vol. 378, pp. 165–169.

    Article  Google Scholar 

  9. Monastyrsky, G.E., Odnosum, V., Humbeeck, J.V., Kolomytsev, V.I., and Koval, Y.N., Powder Metallurgical Processing of Ni-Ti-Zr Alloys Undergoing Martensitic Transformation: Part I, Intermetallics, 2002, vol. 10, pp. 95–103.

    Article  CAS  Google Scholar 

  10. Chu, C.L., Chung, C.Y., Lin, P.H., Wang, S.D., Fabrication of Porous NiTi Shape Memory Alloy for Hard Tissue Implants by Combustion Synthesis, Mater. Sci. Eng. A, 2004, vol. 366, pp. 114–119.

    Article  Google Scholar 

  11. Sadrnezhaad, S.K. and Hosseini, S.A., Fabrication of Porous NiTi-shape Memory Alloy Objects by Partially Hydrided Titanium Powder for Biomedical Applications, Mater. Des., 2009, vol. 30, pp. 4483–4487.

    Article  CAS  Google Scholar 

  12. Crone, W.C., Yahya, A.N., and Perepezko, J.H., Bulk Shape Memory NiTi with Refined Grain Size Synthesized by Mechanical Alloying, Mater. Sci. Forum, 2002, vol. 386, pp. 597–602.

    Article  Google Scholar 

  13. Morris, D.G. and Morris, M.A., NiTi Intermetallic by Mixing, Milling and Interdiffusing Elemental Components, Materials Science and Engineering A, Mater. Sci. Eng. A, 1989, vol. 110, pp. 139–149.

    Article  Google Scholar 

  14. Green, S.M., Grant, D.M., and Kelly, N.R., Powder Metallurgical Processing of Ni-Ti Shape-Memory Alloy, Powder Metallurgy, Powder Metall., 1997, vol. 10, pp. 43–47.

    Google Scholar 

  15. Green, S.M., Grant, D.M., and Wood, J.V., Shape Memory Transformation in Mechanically Alloyed Ni-5O at % Ti, J. Phys. IV france 7, 1997, vol. C5, p. 351.

    Google Scholar 

  16. Gharacheh, M.A., Kokabi, A.H., Daneshi, G.H., Shalchi, B., and Sarrafi, R., The Influence of the Ratio of “Rotational Speed/Traverse Speed” (ω/v) on Mechanical Properties of AZ31 Friction Stir Welds, Int. J. Mach. Tools Manuf., 2006, vol. 48, pp. 1983–1987.

    Article  Google Scholar 

  17. Zhu, S.L., Yang, X.J., Hu, F., Deng, S.H., and Cui, Z.D., Processing of Porous TiNi Shape Memory Alloy from Elemental Powders by Ar-Sintering, Mater. Lett., 2004, vol. 58, pp. 2369–2373.

    Article  CAS  Google Scholar 

  18. Bronzino, J.D., The Biomedical Engineering Handbook, 2nd ed., vol. 1, Boca Raton: CRC Press, 2000.

    Google Scholar 

  19. Hey, J.C. and Jardine, A.P., Shape Memory TiNi Synthesis from Elemental Powders, Mater. Sci. Eng. A, 1994, vol. 188, pp. 291–300.

    Article  Google Scholar 

  20. Li, B.Y., Rong, L.J., Li, Y.Y., and Gjunter, V.E., A Recent Development in Producing Porous Ni-Ti Shape Memory Alloys, Intermetallics, 2000, vol. 8, pp. 881–884.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Sayed Khatiboleslam Sadrnezhaad.

Additional information

The article is published in the original.

About this article

Cite this article

Parvizi, S., Hasannaeimi, V., Saebnoori, E. et al. Fabrication of porous NiTi alloy via powder metallurgy and its mechanical characterization by shear punch method. Russ. J. Non-ferrous Metals 53, 169–175 (2012). https://doi.org/10.3103/S1067821212020113

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3103/S1067821212020113

Keywords

Navigation