Porous TiO2-Al2O3 Photocatalyst: The Effects of Calcination Time

Article Preview

Abstract:

Porous TiO2-Al2O3 composite materials were prepared through sol-gel method after calcination at 500 oC for different time. FT-IR spectra of porous TiO2-Al2O3 composite materials revealed that the samples are composed of Al2O3 and TiO2. The sample calcinated for 2.5 h had the maximum specific area of 128.9 m2•g-1. High pore volume and average pore size were possessed by the samples calcinated for 1 h and 3 h. While being calcinated at 500 oC, photocatalytic activities of the materials increased at first and then dropped down with the increasing calcination time. The sample calcinated for 3 h showed the maximum activity of 35%.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

165-168

Citation:

Online since:

March 2012

Export:

Price:

[1] M.F. Vanesa, L.S. Ergardo, N.B. Mirta, and R.P. Luis: J. Colloid. Interface. Sci. Vol. 327 (2008), p.403.

Google Scholar

[2] X.B. Li, L.L. Wang, and X.H. Lu: J. Hazard. Mater. Vol. 177 (2010), p.639.

Google Scholar

[3] Q.Y. Li, K. Wang, S.L. Zhang, M. Zhang, J.J. Yang, and Z.S. Jin: J. Mol. Catal. A Vol. 258 (2006), p.83.

Google Scholar

[4] H.M. Sung-Suh, J.R. Choi, H.J. Hah, S.M. Koo, and Y.C. Bae: J. Photochem. Photobiol. A Vol. 163 (2004), p.37.

Google Scholar

[5] W.C. Hung, Y.C. Chen, H. Chu, and T.K. Tseng: Appl. Surf. Sci. Vol. 255 (2008), p.2205.

Google Scholar

[6] R. Khan, and T.J. Kim: J. Hazard. Mater. Vol. 163 (2009), p.1179.

Google Scholar

[7] Y.N. Huo, J. Zhu, J.X. Li, G.S. Li, and H.X. Li: J. Mol. Catal. A Vol. 27 (2007), p.237.

Google Scholar

[8] M.T.S. Adrián, G.S. Cláudia, D. Goran, and L.F. Joaquim: Catal. Today Vol. 44 (2009), p.13.

Google Scholar

[9] S. Qourzal, N. Barka, M. Tamimi, A. Assabbane, A. Nounah, A. Ihlal, and A. Ait-Ichou: Mater. Sci. Eng. C Vol. 29 (2009), p.1616.

DOI: 10.1016/j.msec.2008.12.024

Google Scholar

[10] S.F. Chen, L. Chen, S. Gao, and G.Y. Cao: Mater. Chem. Phy. Vol. 98 (2006), p.116.

Google Scholar