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Erschienen in: Journal of Materials Engineering and Performance 11/2020

14.10.2020

Microstructure of Electrodeposited Nickel: Role of Additives

verfasst von: Mark K. King Jr., Manoj K. Mahapatra

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 11/2020

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Abstract

Micro–nanoscale surface microstructure of electrodeposited nickel on AISI 430 substrate from sulfamate bath with ionic and nonionic additives was investigated. 0.69 × 10−4-2.08 × 10−4 M sodium dodecyl sulfate (SDS) and 0.5-4.0 M sodium chloride (NaCl) were used as ionic additives. 0.5-4.0 M ethanol and 1-propanol were used as nonionic additives. Ethanol, propanol, and NaCl promote evolution of nickel micro–nanocones/pyramids. Concentration of these additives, especially NaCl, plays a significant role to modify nickel microstructure. Adhesion of deposited nickel with the substrate, determined by crosscut tape test, is excellent for SDS, ethanol, and propanol additive regardless of their concentration. NaCl degrades the adhesion resulting 100% removal of deposited nickel for 4.0M additive in sulfamate bath. Nickel coating without additive and 1.39 × 10−4 M SDS additive corrode at the same rate (1.08 × 10−2 mm/year), while the other additives increase the corrosion rate.

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Metadaten
Titel
Microstructure of Electrodeposited Nickel: Role of Additives
verfasst von
Mark K. King Jr.
Manoj K. Mahapatra
Publikationsdatum
14.10.2020
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 11/2020
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-020-05173-2

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