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Journal of Materials Science
Erschienen in: Journal of Materials Science 28/2020

25.06.2020 | Chemical routes to materials

Microwave synthesis of phosphorus-doped graphitic carbon nitride nanosheets with enhanced electrochemiluminescence signals

verfasst von: Jingye Zou, Yongzhi Yu, Kun Qiao, Shan Wu, Wenjun Yan, Si Cheng, Nan Jiang, Jigang Wang

Erschienen in: Journal of Materials Science | Ausgabe 28/2020

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Abstract

Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irradiation. When the melamine precursor is modified with a 5 wt% diammonium hydrogen phosphate, the as-synthesized PCNNs display a very thin thickness (about 2 nm), good dispersibility in water (still stable after 2 weeks), low electron-transfer resistance (7499 Ω) and suitable band gap (2.7 eV). More importantly, the ECL intensity of the optimal PCNNs at low potential (− 1.2 to 0 V) is 26.7 times stronger than that of pure graphitic carbon nitride. The key to the excellent ECL property primarily lies in the more satisfactory sheet-like structure, faster electron transfer and better water affinity.
Vorheriger Artikel The spent FCC catalyst loaded with Sb-doped SnO2 and its application in electrocatalytic degradation of methylene blue
Nächster Artikel Atmospheric pressure atomic layer deposition of iron oxide nanolayer on the Al2O3/SiO2/Si substrate for mm-tall vertically aligned CNTs growth

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Metadaten
Titel
Microwave synthesis of phosphorus-doped graphitic carbon nitride nanosheets with enhanced electrochemiluminescence signals
verfasst von
Jingye Zou
Yongzhi Yu
Kun Qiao
Shan Wu
Wenjun Yan
Si Cheng
Nan Jiang
Jigang Wang
Publikationsdatum
25.06.2020
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 28/2020
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-020-04862-6

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