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Journal of Materials Science
Erschienen in: Journal of Materials Science 5/2015

01.03.2015 | Original Paper

On ball-milled ODS ferritic steel recrystallization: From as-milled powder particles to consolidated state

verfasst von: Nicolas Sallez, Patricia Donnadieu, Eglantine Courtois-Manara, Delphine Chassaing, Christian Kübel, Frederic Delabrouille, Martine Blat-Yrieix, Yann de Carlan, Yves Bréchet

Erschienen in: Journal of Materials Science | Ausgabe 5/2015

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Abstract

Recrystallization of a ball-milled ferritic ODS steel is studied towards its evolution from as-milled powder to consolidated state. This characterization has been made possible by using a combination of X-ray Diffraction (XRD) and an innovative method based on an Automated Crystallographic Orientation Mapping (ACOM) tool attached to a Transmission Electron Microscope (TEM). Focus Ion Beam preparation has been essential to obtain a thin section of the ODS steel powder particle and perform the ACOM-TEM study. Relevant temperatures regarding recovery and recrystallization during the heat treatment had first been identified with XRD profile analysis. Selected states were further characterized using ACOM-TEM that provides key information on microstructure, i.e. grain size and morphology, crystallite size, local texture and distortion. ACOM-TEM cartographies have revealed for the first time that the microstructure of as-milled ODS ferritic steel particles consists in very anisotropic grains containing undistorted domains and dislocation walls. This is in agreement with the nanosized crystallites measured by XRD results. The mutual benefits of XRD and ACOM-TEM methods to analyse and describe the microstructure are discussed as well as the reliability of dislocation density measurements provided by ACOM-TEM misorientation measurements. In addition, of the ACOM-TEM results, the microstructural evolution during the processing route is interpreted in terms of a competition between recovery, recrystallization, grain growth and precipitation.
Vorheriger Artikel Fabrication and characterization of poly(octanediol citrate)/gallium-containing bioglass microcomposite scaffolds
Nächster Artikel Structural features, properties, and relaxations of PMMA-ZnO nanocomposite

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Metadaten
Titel
On ball-milled ODS ferritic steel recrystallization: From as-milled powder particles to consolidated state
verfasst von
Nicolas Sallez
Patricia Donnadieu
Eglantine Courtois-Manara
Delphine Chassaing
Christian Kübel
Frederic Delabrouille
Martine Blat-Yrieix
Yann de Carlan
Yves Bréchet
Publikationsdatum
01.03.2015
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 5/2015
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-014-8783-1

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