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Journal of Sol-Gel Science and Technology
Erschienen in: Journal of Sol-Gel Science and Technology 1/2015

01.01.2015 | Original Paper

Optimizing sol–gel synthesis of magnesia-stabilized zirconia (MSZ) nanoparticles using Taguchi robust design for thermal barrier coatings (TBCs) applications

verfasst von: Morteza Hajizadeh-Oghaz, Reza Shoja Razavi, Mohammad Khajelakzay

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 1/2015

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Abstract

Nanocrystalline magnesia-stabilized zirconia powders have been synthesized using Pechini method and Taguchi experiment design. In the present research work, Taguchi method was applied to investigate the effect of citric acid to ethylene glycol mole ratio (CA/EG), citric acid to transition metal mole ratio (CA/TM), calcination temperature and time on particle size. CA/EG and CA/TM were determined to be the main parameters controlling particle size of magnesia-stabilized zirconia powders. Under optimum conditions, a verification experiment was carried out, and the average primary particle size of magnesia-stabilized zirconia powders was found to be 5.6 nm with homogeneous particle size distribution. Contribution percentage of each manageable factor was also determined. Furthermore, characterization of optimum sample was accomplished by means of thermogravimetric analysis, differential thermal analysis, X-ray diffraction, transmission electron microscopy, field emission scanning electron microscope and Raman spectroscopy.
Vorheriger Artikel Effect of initial sol concentration on the microstructure and morphology of carbon aerogels
Nächster Artikel Study on the crack mechanism of SiO2 anti-reflective layer prepared by sol–gel method

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Metadaten
Titel
Optimizing sol–gel synthesis of magnesia-stabilized zirconia (MSZ) nanoparticles using Taguchi robust design for thermal barrier coatings (TBCs) applications
verfasst von
Morteza Hajizadeh-Oghaz
Reza Shoja Razavi
Mohammad Khajelakzay
Publikationsdatum
01.01.2015
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 1/2015
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-014-3521-3

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