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Erschienen in: Microsystem Technologies 10/2016

09.09.2015 | Technical Paper

Practice of diclofenac sodium for the hydrothermal growth of NiO nanostructures and their application for enzyme free glucose biosensor

verfasst von: Razium Ali Soomro, Zafar Hussain Ibupoto, Sirajuddin, Syed Tufail Hussain Sherazi, Muhammad Ishaq Abro, Magnus Willander

Erschienen in: Microsystem Technologies | Ausgabe 10/2016

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Abstract

In this study diclofenac sodium (DFS), an analgesic drug has been employed as an effective template for the synthesis of NiO nanostructures. The NiO nanostructures were synthesised using low temperature hydrothermal growth method,  both in the presence and absence of the DFS drug. The synthesised nanostructures were studied for their structural, compositional and electrochemical properties using scanning electron microscopy, X-ray diffraction and cyclic voltammetry. The synthesised nanostructures were then utilised for the modification of glassy carbon electrode which were then utilised for the electro-catalytic enzyme free glucose sensing in alkaline media. The competitive experiments suggested that although, both nanostructures possess excellent capability of glucose sensing, the NiO nanoflakes modified electrode was found to be twice as much as sensitive (2584 µA mM−1 cm−2) as nanoflowers based electrode (1154 µA mM−1 cm−2). The NiO nanoflakes based sensor further demonstrated excellent anti-interference potential in the presence of common interferents like uric acid, ascorbic acid and dopamine. In addition, the successful application NiO nanoflakes based sensor to determine real blood glucose concentration further suggest its feasibility for real sample analysis.

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Metadaten
Titel
Practice of diclofenac sodium for the hydrothermal growth of NiO nanostructures and their application for enzyme free glucose biosensor
verfasst von
Razium Ali Soomro
Zafar Hussain Ibupoto
Sirajuddin
Syed Tufail Hussain Sherazi
Muhammad Ishaq Abro
Magnus Willander
Publikationsdatum
09.09.2015
Verlag
Springer Berlin Heidelberg
Erschienen in
Microsystem Technologies / Ausgabe 10/2016
Print ISSN: 0946-7076
Elektronische ISSN: 1432-1858
DOI
https://doi.org/10.1007/s00542-015-2669-2

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