Skip to main content

2013 | OriginalPaper | Buchkapitel

2. Separation Techniques

verfasst von : Catherine Vieillescazes, Isabel Sierra, Sonia Morante-Zarcero

Erschienen in: Conservation Science for the Cultural Heritage

Verlag: Springer Berlin Heidelberg

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

This chapter deals with the importance of analytical chemistry and more particularly the separation techniques in the field of conservation science. High performance liquid chromatography (HPLC) and gas chromatography (GC) are mainly developed. The principles of the methods, some information about the methodology and their evaluation are discussed.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat Burgot G, Burgot JL (2002) Méthodes Instrumentales d’Analyse Chimique. Tec et Doc, Paris Burgot G, Burgot JL (2002) Méthodes Instrumentales d’Analyse Chimique. Tec et Doc, Paris
2.
Zurück zum Zitat Poole CF (2003) The essence of chromatography. Elsevier, Bristol Poole CF (2003) The essence of chromatography. Elsevier, Bristol
3.
Zurück zum Zitat Chavanne M, Beaudoin GJ, Jullien A, Flamand E (1999) Chimie organique expérimentale. Belin, Paris Chavanne M, Beaudoin GJ, Jullien A, Flamand E (1999) Chimie organique expérimentale. Belin, Paris
4.
Zurück zum Zitat Defranceschi M (1990) 144 manipulations de chimie générale et minérale. Ellipses, Paris Defranceschi M (1990) 144 manipulations de chimie générale et minérale. Ellipses, Paris
5.
Zurück zum Zitat Douglas A, Skoog F, Holler J, Timothy A, Nieman T (2003) Principes d’Analyse Instrumentales De Boeck. Paris et, Bruxelles Douglas A, Skoog F, Holler J, Timothy A, Nieman T (2003) Principes d’Analyse Instrumentales De Boeck. Paris et, Bruxelles
6.
Zurück zum Zitat Rouessac F (2004) Analyse chimique (méthodes et techniques instrumentales modernes). Masson, Paris Rouessac F (2004) Analyse chimique (méthodes et techniques instrumentales modernes). Masson, Paris
7.
Zurück zum Zitat Arpino P, Prevôt A, Serpinet J, Tranchant J, Vergnol A, Wittier P (1995) Manuel pratique de chromatographie en phase gazeuse. Masson, Paris Arpino P, Prevôt A, Serpinet J, Tranchant J, Vergnol A, Wittier P (1995) Manuel pratique de chromatographie en phase gazeuse. Masson, Paris
8.
Zurück zum Zitat Rosset R, Caude M, Jardy A (1991) Chromatographies en phase liquide et supercritique. Masson, Paris Rosset R, Caude M, Jardy A (1991) Chromatographies en phase liquide et supercritique. Masson, Paris
9.
Zurück zum Zitat Martin AJP, Synge RLM (1941) A new form of chromatogram employing two liquid phases. 1. A theory of chromatography. 2. Application of the microdetermination of the higher monoaminoacids in proteins. Biochem J 35:1358–1368 Martin AJP, Synge RLM (1941) A new form of chromatogram employing two liquid phases. 1. A theory of chromatography. 2. Application of the microdetermination of the higher monoaminoacids in proteins. Biochem J 35:1358–1368
10.
Zurück zum Zitat Mills JS, White R (1994) The organic chemistry of museum objects. Butterworth Heinemann, London Mills JS, White R (1994) The organic chemistry of museum objects. Butterworth Heinemann, London
11.
Zurück zum Zitat Shedrinsky AM, Wampler TP, Indictor N, Baer NS (1989) Application of analytical pyrolysis to problems in art and archaeology: a review. J Anal Appl Pyrol 15:393–412CrossRef Shedrinsky AM, Wampler TP, Indictor N, Baer NS (1989) Application of analytical pyrolysis to problems in art and archaeology: a review. J Anal Appl Pyrol 15:393–412CrossRef
12.
Zurück zum Zitat Hovaneissian M, Archier P, Mathe C, Vieillescazes C (2006) Contribution de la chimie analytique à l’étude des exsudats végétaux styrax, storax et benjoin. C R Chim 9(9):1192–1202CrossRef Hovaneissian M, Archier P, Mathe C, Vieillescazes C (2006) Contribution de la chimie analytique à l’étude des exsudats végétaux styrax, storax et benjoin. C R Chim 9(9):1192–1202CrossRef
13.
Zurück zum Zitat Regert M, Rolando C (1996) Archéologie des résidus organiques: De la chimie analytique à l’archéologie : un état de la question. Techné 3:118–128 Regert M, Rolando C (1996) Archéologie des résidus organiques: De la chimie analytique à l’archéologie : un état de la question. Techné 3:118–128
14.
Zurück zum Zitat Mejanelle P, Bleton J, Goursaud S, Tchapla A (1996) Analyse de baumes de momification d’Egypte ancienne par chromatographie gazeuse capillaire: spectrométrie de masse. Analusis Magazine 24(7):16–20 Mejanelle P, Bleton J, Goursaud S, Tchapla A (1996) Analyse de baumes de momification d’Egypte ancienne par chromatographie gazeuse capillaire: spectrométrie de masse. Analusis Magazine 24(7):16–20
15.
Zurück zum Zitat Bleton J, Coupry C, Sansoulet J (1996) Approche d’étude des encres anciennes. Stud Conserv 41:95–108CrossRef Bleton J, Coupry C, Sansoulet J (1996) Approche d’étude des encres anciennes. Stud Conserv 41:95–108CrossRef
16.
Zurück zum Zitat Connan J, Deschene O (1996) Le bitume à Suse: Collection du Musée du Louvre Réunion des Musées Nationaux et Elf Aquitaine Production. Paris et Pau, Paris Connan J, Deschene O (1996) Le bitume à Suse: Collection du Musée du Louvre Réunion des Musées Nationaux et Elf Aquitaine Production. Paris et Pau, Paris
17.
Zurück zum Zitat Colinart S (1987) Chapter IV: Matériaux constitutifs. In: Sculptures en cire de l’ancienne Egypte à l’art abstrait, Ministère de la Culture et de la Communication. Editions de la réunion des musées nationaux, Paris PP 29–57 Colinart S (1987) Chapter IV: Matériaux constitutifs. In: Sculptures en cire de l’ancienne Egypte à l’art abstrait, Ministère de la Culture et de la Communication. Editions de la réunion des musées nationaux, Paris PP 29–57
18.
Zurück zum Zitat Ploeger R, Scalaron O, Chiantore O (2008) The characterization of commercial artists’ alkyd paints. J Cult Herit 9(4):412–419CrossRef Ploeger R, Scalaron O, Chiantore O (2008) The characterization of commercial artists’ alkyd paints. J Cult Herit 9(4):412–419CrossRef
19.
Zurück zum Zitat Quye A, Wouters J, Boon JJ (1996) A preliminary study of light-ageing effect on the analysis of natural flavanoid-dye wools by photodiode array HPLC and by direct temperature mass spectrometry. In: Commitee for Conservation. ICOM, Edimbourg 2:704–713 Quye A, Wouters J, Boon JJ (1996) A preliminary study of light-ageing effect on the analysis of natural flavanoid-dye wools by photodiode array HPLC and by direct temperature mass spectrometry. In: Commitee for Conservation. ICOM, Edimbourg 2:704–713
20.
Zurück zum Zitat Szostek B, Orska-Gawrys J, Surowiec I (1012) Trojanowicz M (2003) Investigation of natural dyes occurring in historical Coptic textiles by high-performance liquid chromatography with UV–Vis and mass spectrometric detection. J Chromatogr 2:179–192 Szostek B, Orska-Gawrys J, Surowiec I (1012) Trojanowicz M (2003) Investigation of natural dyes occurring in historical Coptic textiles by high-performance liquid chromatography with UV–Vis and mass spectrometric detection. J Chromatogr 2:179–192
21.
Zurück zum Zitat Wallert A (1996) Tannins of the parchment of the Dead Sea scrolls. In: committee for conservation ICOM. Edimbourg, 2:560–564 Wallert A (1996) Tannins of the parchment of the Dead Sea scrolls. In: committee for conservation ICOM. Edimbourg, 2:560–564
22.
Zurück zum Zitat Richardin P, Copy S, Chahine C, Saltron F, Bonnassies TS (1996) GC and GC/MS characterization of degradation amino acids in naturally and artificially aged leathers. J Am Leather Chem Assoc 91(1):2–17 Richardin P, Copy S, Chahine C, Saltron F, Bonnassies TS (1996) GC and GC/MS characterization of degradation amino acids in naturally and artificially aged leathers. J Am Leather Chem Assoc 91(1):2–17
23.
Zurück zum Zitat Pastore P, Magno F, Volpin S, Biscontin G (1991) Chromatographic determination of oxalate ion in patinas covering ancient materials. Ann Chim (Rome) 81(5–6):233–241 Pastore P, Magno F, Volpin S, Biscontin G (1991) Chromatographic determination of oxalate ion in patinas covering ancient materials. Ann Chim (Rome) 81(5–6):233–241
24.
Zurück zum Zitat Vieillescazes C, Coen S (1993) Charactérisation de quelques résines utilisées en Egypte ancienne. Stud Conserv 38:255–264CrossRef Vieillescazes C, Coen S (1993) Charactérisation de quelques résines utilisées en Egypte ancienne. Stud Conserv 38:255–264CrossRef
25.
Zurück zum Zitat Casoli A, Mirti P, Palla G (1995) Characterization of medieval proteinaceous painting media using gas chromatography and gas chromatography- mass spectrometry. Fresenius’ J Anal Chem 352(3–4):372–379CrossRef Casoli A, Mirti P, Palla G (1995) Characterization of medieval proteinaceous painting media using gas chromatography and gas chromatography- mass spectrometry. Fresenius’ J Anal Chem 352(3–4):372–379CrossRef
26.
Zurück zum Zitat Halpine SM (1992) Amino acid analysis of proteinaceous media from Cosimo Tura’s The Annunciation with Saint Francis and Saint Louis of Toulouse. Stud Conserv 37(1):22–38CrossRef Halpine SM (1992) Amino acid analysis of proteinaceous media from Cosimo Tura’s The Annunciation with Saint Francis and Saint Louis of Toulouse. Stud Conserv 37(1):22–38CrossRef
27.
Zurück zum Zitat Bouchonnet S (2009) La spectrométrie de masse en couplage avec chromatographie en phase gazeuse. Tec and Doc Lavoisier, Paris Bouchonnet S (2009) La spectrométrie de masse en couplage avec chromatographie en phase gazeuse. Tec and Doc Lavoisier, Paris
28.
Zurück zum Zitat Cuoco G, Mathe C, Archier P, Vieillescazes C (2009) A multivariate study of the performance of an ultrasound-assisted madder dyes extraction and characterization by liquid chromatography-photodiode array detection. Ultrason sonochem 16:75–82CrossRef Cuoco G, Mathe C, Archier P, Vieillescazes C (2009) A multivariate study of the performance of an ultrasound-assisted madder dyes extraction and characterization by liquid chromatography-photodiode array detection. Ultrason sonochem 16:75–82CrossRef
29.
Zurück zum Zitat Bleton J, Tchapla A (2009) SPME/GC-MS in the caracterisation of terpenic resins. In: Organic mass spectrometry in art and archeology. J Wiley 10:261–302 Bleton J, Tchapla A (2009) SPME/GC-MS in the caracterisation of terpenic resins. In: Organic mass spectrometry in art and archeology. J Wiley 10:261–302
30.
Zurück zum Zitat Colombini MP, Modugno F, Giannarelli S, Fuoco R, Matteini M (2000) GC-MS characterization of paint varnishes. Microchem J 67:385–396CrossRef Colombini MP, Modugno F, Giannarelli S, Fuoco R, Matteini M (2000) GC-MS characterization of paint varnishes. Microchem J 67:385–396CrossRef
31.
Zurück zum Zitat Colombini MP, Andreotti A, Bonaduce I, Modugno F, Ribechini E (2009) Analytical strategies for characterizing organic paint media using gas chromatography/mass spectrometry. Acc Chem Res 43(6):715–727CrossRef Colombini MP, Andreotti A, Bonaduce I, Modugno F, Ribechini E (2009) Analytical strategies for characterizing organic paint media using gas chromatography/mass spectrometry. Acc Chem Res 43(6):715–727CrossRef
32.
Zurück zum Zitat Gröβl M, Harrison S, Kaml I, Kenndler E (2005) Characterisation of natural polysaccharides (plant gums) used as binding media for artistic and historic works by capillary zone electrophoresis. J Chromatogr 1077:80–89CrossRef Gröβl M, Harrison S, Kaml I, Kenndler E (2005) Characterisation of natural polysaccharides (plant gums) used as binding media for artistic and historic works by capillary zone electrophoresis. J Chromatogr 1077:80–89CrossRef
33.
Zurück zum Zitat Kaml I, Vcelakova K, Kenndler E (2004) Characterisation and identification of proteinaceous binding media (animal glues) from their amino acid profile by capillary zone electrophoresis. J Sep Sci 27:161–166CrossRef Kaml I, Vcelakova K, Kenndler E (2004) Characterisation and identification of proteinaceous binding media (animal glues) from their amino acid profile by capillary zone electrophoresis. J Sep Sci 27:161–166CrossRef
34.
Zurück zum Zitat Harrison S, Kaml I, Prokoratova V, Mazanek M, Kenndler E (2005) Animal glues in mixtures of natural binding media used in artistic and historic objects: identification by capillary zone electrophoresis. Anal Bional Chem 382:1520–1526 Harrison S, Kaml I, Prokoratova V, Mazanek M, Kenndler E (2005) Animal glues in mixtures of natural binding media used in artistic and historic objects: identification by capillary zone electrophoresis. Anal Bional Chem 382:1520–1526
35.
Zurück zum Zitat Findeisen A, Kolivoska V, Kaml I, Baatz W, Kenndler E (2007) Analysis of diterpenoic compounds in natural resins applied as binders in museum objects by capillary electrophoresis. J Chromatogr 1157:454–461CrossRef Findeisen A, Kolivoska V, Kaml I, Baatz W, Kenndler E (2007) Analysis of diterpenoic compounds in natural resins applied as binders in museum objects by capillary electrophoresis. J Chromatogr 1157:454–461CrossRef
36.
Zurück zum Zitat Surowiec I, Kaml I, Kenndler E (2004) Analysis of drying oils used as binding media for objects of art by capillary electrophoresis with indirect UV and conductivity detection. J Chromatogr 1024:245–254CrossRef Surowiec I, Kaml I, Kenndler E (2004) Analysis of drying oils used as binding media for objects of art by capillary electrophoresis with indirect UV and conductivity detection. J Chromatogr 1024:245–254CrossRef
37.
Zurück zum Zitat Harrison S, Kaml I, Rainer F, Kenndler E (2005) Identification of drying oils in mixtures of natural binding media used for artistic and historic works by capillary electrophoresis. J Sep Sci 28:1587–1594 Harrison S, Kaml I, Rainer F, Kenndler E (2005) Identification of drying oils in mixtures of natural binding media used for artistic and historic works by capillary electrophoresis. J Sep Sci 28:1587–1594
38.
Zurück zum Zitat Maguregui M, Alonso R, Barandiaran M, Jimenez R, García N (2007) Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work. J Chromatogr 1154:429–436CrossRef Maguregui M, Alonso R, Barandiaran M, Jimenez R, García N (2007) Micellar electrokinetic chromatography method for the determination of several natural red dyestuff and lake pigments used in art work. J Chromatogr 1154:429–436CrossRef
39.
Zurück zum Zitat Puchalska M, Orlinska M, Ackacha M (2003) Identification of anthraquinone coloring matters in natural red dyes by electrspray mass spectrometry coupled to capillary electrophoresis. J Mass Spectrom 38:1252–1258CrossRef Puchalska M, Orlinska M, Ackacha M (2003) Identification of anthraquinone coloring matters in natural red dyes by electrspray mass spectrometry coupled to capillary electrophoresis. J Mass Spectrom 38:1252–1258CrossRef
40.
Zurück zum Zitat Kouznetsov DA, Ivanov A, Veletsky P (1994) Detection of alkylated cellulose derivatives in several archaeological linen textile samples by capillary electrophoresis/mass spectrometry. Anal Chem 66:4359–4365CrossRef Kouznetsov DA, Ivanov A, Veletsky P (1994) Detection of alkylated cellulose derivatives in several archaeological linen textile samples by capillary electrophoresis/mass spectrometry. Anal Chem 66:4359–4365CrossRef
41.
Zurück zum Zitat López-Montes A, Blanc R, Espejo T, Huertas-Pérez J, Navalón A, Vilchez JL (2007) Simultaneous identification of natural dyes in the collection of drawings and maps from the Royal Chancellery Archives in Granada (Spain) by CE. Electrophoresis 28:1243–1251CrossRef López-Montes A, Blanc R, Espejo T, Huertas-Pérez J, Navalón A, Vilchez JL (2007) Simultaneous identification of natural dyes in the collection of drawings and maps from the Royal Chancellery Archives in Granada (Spain) by CE. Electrophoresis 28:1243–1251CrossRef
42.
Zurück zum Zitat López-Montes A, Blanc R, Espejo T, Navalón A, Vilchez JL (2009) Characterization of sepia ink in ancient graphic documents by capillary electrophoresis. Microchim J 93:121–126CrossRef López-Montes A, Blanc R, Espejo T, Navalón A, Vilchez JL (2009) Characterization of sepia ink in ancient graphic documents by capillary electrophoresis. Microchim J 93:121–126CrossRef
43.
Zurück zum Zitat Chankvetadze B (1997) Capillary electrophoresis in chiral analysis. Willey, New York Chankvetadze B (1997) Capillary electrophoresis in chiral analysis. Willey, New York
44.
Zurück zum Zitat Dupont A-L, Egasse C, Morin A, Vasseur F (2007) Comprehensive characterisation of cellulose- and lignocellulose- degradation products in agent papers: Capillary zone electrophoresis of low-molar mass organic acids, carbohydrates, and aromatic lignin derivatives. Carbohydr Polym 68:1–16CrossRef Dupont A-L, Egasse C, Morin A, Vasseur F (2007) Comprehensive characterisation of cellulose- and lignocellulose- degradation products in agent papers: Capillary zone electrophoresis of low-molar mass organic acids, carbohydrates, and aromatic lignin derivatives. Carbohydr Polym 68:1–16CrossRef
45.
Zurück zum Zitat Doménech-Carbó M (2008) Novel analytical methods for characterising binding media and protective coatings in artworks. Anal Chim Acta 621:109–139CrossRef Doménech-Carbó M (2008) Novel analytical methods for characterising binding media and protective coatings in artworks. Anal Chim Acta 621:109–139CrossRef
Metadaten
Titel
Separation Techniques
verfasst von
Catherine Vieillescazes
Isabel Sierra
Sonia Morante-Zarcero
Copyright-Jahr
2013
Verlag
Springer Berlin Heidelberg
DOI
https://doi.org/10.1007/978-3-642-30985-4_2

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.