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Journal of Materials Engineering and Performance
Erschienen in: Journal of Materials Engineering and Performance 1/2015

01.01.2015

Structure-Property Relationship of Layered Metal Oxide Phosphonate/Chitosan Nanohybrids for Transducer in Biosensing Device

verfasst von: Sriparna De, Smita Mohanty, Sanjay Kumar Nayak

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 1/2015

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Abstract

A candid approach to analyze the performance characteristics of phenyl phosphonate-functionalized zirconium oxide and pure zirconium oxide (ZrO2) fillers reinforced chitosan nanocomposites and their suitability as a potential biomaterial for the development of transducer surface in biosensing device has been investigated in this communication. Functionalization of ZrO2 has been carried out using sulfophenylphosphonate which was confirmed using Fourier transform infrared spectrographs. The electrostatic intercalation of chitosan with filler particles was monitored using electrochemical impedance analyzer which exhibits lowest bulk resistance which is highly effective for ionic switching. Incorporation of zirconium sulfophenylphosphonate (ZrSP) the ionic conductivity of the chitosan film attained a value of 1.2 × 10−6 S/cm as compared to the unmodified one which is a prefeasibility work for the fabrication of biosensing platform. Variation in performance characteristics has been evaluated through morphological and thermal characterization. TGA and DSC analysis reveal that the thermal stability and decomposition temperature of the nanocomposites were improved by the addition of reinforcing filler particles. XRD and SEM and TEM results support the above assumption. The continuous alignment of the proton transfer channels of the nanocomposites was thoroughly investigated by AFM analysis which revealed phase morphology for improved enzyme entrapment. Further, surface functionalized nanofillers result considerable increment of mechanical properties in terms of elastic modulus and tensile stress.

Graphical Abstract

Vorheriger Artikel Recovery of Fatigue Damage and Life Prediction by Laser Irradiation Healing Treatment for Copper Film
Nächster Artikel Effect of Carbon Nanotubes on Corrosion and Tribological Properties of Pulse-Electrodeposited Co-W Composite Coatings

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Metadaten
Titel
Structure-Property Relationship of Layered Metal Oxide Phosphonate/Chitosan Nanohybrids for Transducer in Biosensing Device
verfasst von
Sriparna De
Smita Mohanty
Sanjay Kumar Nayak
Publikationsdatum
01.01.2015
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 1/2015
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-014-1293-0

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