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Journal of Sol-Gel Science and Technology

Erschienen in:

28.09.2016 | Original Paper: Sol-gel, hybrids and solution chemistries

Synthesis and characterization of room temperature sol–gel-assisted transparent tin-doped magnesium oxide nanoparticles’ protective coating

verfasst von: Shumaila Islam, Noriah Bidin, M. Alam Saeed, Saira Riaz, M. Aizat A. Bakar, Shahzad Naseem, Khaldoon Naji Abbas, Mohd Marsin Sanagi

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 2/2017

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Abstract

Using in-situ sol–gel processing, Sn-doped MgO₂ nanofilm has been fabricated by spin-coating technique. Cracked and uneven distribution of particles in the composite can lead to premature failures and material cannot be used as protective coating. Therefore, homogeneous porous nanoparticles with average size 27 nm were obtained without any voids. A stoichiometric ratio of dopant and matrix with low average roughness 2.52 nm of the thin film was observed. Furthermore, the refractive index 1.30 and average film thickness 221 nm at wavelength 632.8 nm has been estimated with optical transparency up to 94 % in the visible range by ultraviolet–visible spectroscopy. Band gap energy of 3.12 eV has also been estimated. The experimental findings show that the prepared nanoparticles can be used as protective coatings.

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Vorheriger Artikel Preparation of fluoroalkyl end-capped vinyltrimethoxysilane oligomeric silica/poly(tetrafluoroethylene) nanocomposites possessing a superoleophilic/superhydrophobic characteristic: application to the separation of oil and water

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Titel: Synthesis and characterization of room temperature sol–gel-assisted transparent tin-doped magnesium oxide nanoparticles’ protective coating
verfasst von: Shumaila Islam
Noriah Bidin
M. Alam Saeed
Saira Riaz
M. Aizat A. Bakar
Shahzad Naseem
Khaldoon Naji Abbas
Mohd Marsin Sanagi
Publikationsdatum: 28.09.2016
Verlag: Springer US
Erschienen in: Journal of Sol-Gel Science and Technology / Ausgabe 2/2017
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI: https://doi.org/10.1007/s10971-016-4207-9

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