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Journal of Materials Science: Materials in Electronics
Erschienen in: Journal of Materials Science: Materials in Electronics 4/2019

02.01.2019

Synthesis of phosphate-modified zeolite as a modifier in carbon paste electrode for nitrite electrochemical detection

verfasst von: Adamu Idris, Tawfik Saleh, Oki Muraza, Mohammed Sanhoob, Md. Abdul Aziz, Abdul-Rahman Al-Betar

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 4/2019

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Abstract

In this work, template-free synthesis of phosphate mordenite zeolites was carried out. Post synthesis impregnation using phosphoric acid was applied to add phosphate group to zeolite framework, i.e. P-loading. Phosphate modification led to disruption of bridging hydroxyl and silanol groups as confirmed by FT-IR spectra. EDX spectra showed that the Si/Al ratio of the zeolite increases with the amount of P-loading and 27Al NMR revealed the formation of aluminophosphate on mordenite. The modified electrodes of phosphate mordenite zeolite were used for the electrocatalytic oxidation of nitrite, which was investigated by using square wave voltammetry. The effect of different electrolytes and pH values were also investigated and the calibration curve of nitrite oxidation at phosphate mordenite carbon paste electrodes showed a linear dependence.
Vorheriger Artikel Design and fabrication of double AlGaN/GaN distributed Bragg reflector stack mirror for the application of GaN-based optoelectronic devices
Nächster Artikel High capable visible light driven photocatalytic activity of WO3/g-C3N4 hetrostructure catalysts synthesized by a novel one step microwave irradiation route

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Metadaten
Titel
Synthesis of phosphate-modified zeolite as a modifier in carbon paste electrode for nitrite electrochemical detection
verfasst von
Adamu Idris
Tawfik Saleh
Oki Muraza
Mohammed Sanhoob
Md. Abdul Aziz
Abdul-Rahman Al-Betar
Publikationsdatum
02.01.2019
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 4/2019
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-018-00601-5

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