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Erschienen in: Journal of Sol-Gel Science and Technology 2/2017

16.09.2016 | Original Paper: Sol-gel and hybrid materials for catalytic, photoelectrochemical and sensor applications

Synthesis of spinel CuCo2O4 nanoparticles and its application in p-nitrophenol reduction

verfasst von: Shiduo Zhao, Qiming Li, Fang Li, Zhihua Liang

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 2/2017

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Abstract

CuCo2O4 spinel nanoparticles were successfully preparedvia a sol–gel method, which were firstly employed in catalytic reduction of p-nitrophenol to produce p-aminophenol. CuCo2O4 morphologies can be controlled in this paper. It can be found that the sintering temperature has an important impact on their phase structure and microstructure. Especially the treatment temperature above 700 °C can induce a rapid growth for CuCo2O4 nanoparticles. The catalytic test proved that CuCo2O4 nanoparticles exhibit excellent catalytic activity towards the reduction of p-nitrophenol. Comparative experiments indicated that CuO and CuCoOx nanoparticlesalso exhibit certain catalytic activity in the p-nitrophenol reduction but no any catalytic activity can be observed for Co3O4. Meanwhile, it can be found that the catalytic activity of CuCo2O4 is slightly higher than CuFe2O4 under the same synthesis condition.

Graphical Abstract

https://static-content.springer.com/image/art%3A10.1007%2Fs10971-016-4200-3/MediaObjects/10971_2016_4200_Figa_HTML.gif

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Metadaten
Titel
Synthesis of spinel CuCo2O4 nanoparticles and its application in p-nitrophenol reduction
verfasst von
Shiduo Zhao
Qiming Li
Fang Li
Zhihua Liang
Publikationsdatum
16.09.2016
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 2/2017
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-016-4200-3

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