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Erschienen in: Journal of Materials Engineering and Performance 5/2019

29.04.2019

Tailoring Microstructure and Properties of a Superelastic Ti–Ta Alloy by Incorporating Spark Plasma Sintering with Thermomechanical Processing

verfasst von: Abdollah Bahador, Shota Kariya, Junko Umeda, Esah Hamzah, Katsuyoshi Kondoh

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 5/2019

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Abstract

A powder metallurgy Ti–35 at.% Ta alloy was produced using a spark plasma sintering process. The sintered alloy exhibited Ta-rich regions at a sintering temperature of 1100 °C. Complete diffusion of elemental powders was achieved via homogenization heat treatment at 1500 °C for 12 h, but the ductility declined drastically. The brittle behavior of the homogenized sample was due to the high-oxygen content, continuous grain boundary α-phase and high-angle grain boundaries. Excellent mechanical properties were achieved when hot forging was used along with preheating the homogenized specimen at 1100 °C. The mechanisms underlying this phenomenon were suppression of the solid grain boundary α-phase, high fraction of low-angle grain boundaries and dynamic recrystallization. Tensile strength improved to the maximum value of 868 MPa. The strain recovery ratio increased to 90% in the first cycle during a cyclic loading–unloading test. Incomplete strain recovery of the first cycle was due to the presence of the martensite phase (α″).

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Metadaten
Titel
Tailoring Microstructure and Properties of a Superelastic Ti–Ta Alloy by Incorporating Spark Plasma Sintering with Thermomechanical Processing
verfasst von
Abdollah Bahador
Shota Kariya
Junko Umeda
Esah Hamzah
Katsuyoshi Kondoh
Publikationsdatum
29.04.2019
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 5/2019
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-019-04061-8

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