Skip to main content
Erschienen in: Environmental Earth Sciences 6/2013

01.03.2013 | Original Article

The influence of environmental conditions on weathering of porous rocks by gypsum: a non-destructive study using acoustic emissions

verfasst von: Beatriz Menéndez, Christian David

Erschienen in: Environmental Earth Sciences | Ausgabe 6/2013

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Gypsum is one of the most universally distributed salts in weathered materials but little is known about the influence of environmental conditions on the damage generated by gypsum in stones. To quantify the damage induced by gypsum crystallization acoustic emission techniques are employed to record the elastic energy released during salt crystallization cycles in a limestone. Different environmental conditions have been established during the cooling and drying periods in traditional salt crystallization cycles. During drying two different temperatures (50 and 25 °C) and relative humidity (low, 25 % at 50 °C and 65 % at 25 °C, and high, 99 %) have been applied. The acoustic emission signals are filtered by a frequency analysis in order to eliminate signals corresponding to external noise or artifacts. Our experimental results show that acoustic emission activity is higher under high relative humidity conditions than under low relative humidity conditions, and also higher when drying at 50 °C than at room temperature. Microscopic observations on the weathered samples indicated that under high relative humidity conditions and at room temperature, gypsum crystallizes not on the sample surface, like in the other samples, but deeper in the inner part of the sample, in good agreement with previously published data. We show that using acoustic emissions as usually done in rock mechanics is also very useful in the study of stone decay and weathering processes in the laboratory.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
Zurück zum Zitat Alves CAS, Sequeira Braga MA (2000) Decay effects associated with soluble salts on granite buildings of Braga (NW Portugal). Environmental mineralogy: microbial interactions, anthropogenic influences, contaminated land and waste management. Book series, 9, cap. 10. Mineralogical Society of Great Britain and Ireland, London, pp 181–199 Alves CAS, Sequeira Braga MA (2000) Decay effects associated with soluble salts on granite buildings of Braga (NW Portugal). Environmental mineralogy: microbial interactions, anthropogenic influences, contaminated land and waste management. Book series, 9, cap. 10. Mineralogical Society of Great Britain and Ireland, London, pp 181–199
Zurück zum Zitat Angeli M, Bigas JP, Benavente D, Menéndez B, Hébert R, David C (2007) Salt crystallization in pores: quantification and estimation of damage. Environ Geol 52:187–195CrossRef Angeli M, Bigas JP, Benavente D, Menéndez B, Hébert R, David C (2007) Salt crystallization in pores: quantification and estimation of damage. Environ Geol 52:187–195CrossRef
Zurück zum Zitat Blanc A, Gély JP, Viré M (2001) Le calcaire lutetien, ses carrières, son utilisation dans les monuments. In: Le lutetien la pierre de Paris. Muséum d’histoire naturelle, Paris, pp 38–46 Blanc A, Gély JP, Viré M (2001) Le calcaire lutetien, ses carrières, son utilisation dans les monuments. In: Le lutetien la pierre de Paris. Muséum d’histoire naturelle, Paris, pp 38–46
Zurück zum Zitat Bratasz L, Jakiela S, Lasyk L, Kozlowski R (2008) Direct monitoring of damage in clay-containing sandstone by acoustic emission. In: proceedings of the 11th international conference on deterioration and conservation of stone, Torun Bratasz L, Jakiela S, Lasyk L, Kozlowski R (2008) Direct monitoring of damage in clay-containing sandstone by acoustic emission. In: proceedings of the 11th international conference on deterioration and conservation of stone, Torun
Zurück zum Zitat Brimblecombe P (2000) Air pollution and architecture, past, present and future. J Archit Conserv 6–2:30–46 Brimblecombe P (2000) Air pollution and architecture, past, present and future. J Archit Conserv 6–2:30–46
Zurück zum Zitat Brimblecombe P (2003) The effects of air pollution on the built environment. World Scientific Publishing Company, Singapore, p 448CrossRef Brimblecombe P (2003) The effects of air pollution on the built environment. World Scientific Publishing Company, Singapore, p 448CrossRef
Zurück zum Zitat Brimblecombe P, Grossi CM, Harris I (2006) Climate change critical to cultural heritage. In: Fort R, Alvarez de Buergo M, Gimenez-Heras M, Vazquez-Calvo C (eds) Heritage, weathering and conservation. Taylor and Francis Group, London, pp 387–393 Brimblecombe P, Grossi CM, Harris I (2006) Climate change critical to cultural heritage. In: Fort R, Alvarez de Buergo M, Gimenez-Heras M, Vazquez-Calvo C (eds) Heritage, weathering and conservation. Taylor and Francis Group, London, pp 387–393
Zurück zum Zitat Cardell C, Benavente D, Rodriguez-Gordillo J (2008) Weathering of limestone building material by mixed sulfate solutions. Characterization of stone microstructure, reaction products and decay forms. Mater Charact 59:1371–1385CrossRef Cardell C, Benavente D, Rodriguez-Gordillo J (2008) Weathering of limestone building material by mixed sulfate solutions. Characterization of stone microstructure, reaction products and decay forms. Mater Charact 59:1371–1385CrossRef
Zurück zum Zitat Carpinteri A, Lacidogna G (2006) Damage monitoring of an historical masonry building by the acoustic emission technique. Mater Struct 39:161–167CrossRef Carpinteri A, Lacidogna G (2006) Damage monitoring of an historical masonry building by the acoustic emission technique. Mater Struct 39:161–167CrossRef
Zurück zum Zitat Charola AE, Pühringer J, Steiger M (2007) Gypsum: a review of its role in the deterioration of building materials. Environ Geol 52:339–352CrossRef Charola AE, Pühringer J, Steiger M (2007) Gypsum: a review of its role in the deterioration of building materials. Environ Geol 52:339–352CrossRef
Zurück zum Zitat Cosentino PL, Capizzi P, Fiandaca G, Martorana R, Messina P (2009) Advances in microgeophysics for engineering and cultural heritage. J Earth Sci 20(3):626–639CrossRef Cosentino PL, Capizzi P, Fiandaca G, Martorana R, Messina P (2009) Advances in microgeophysics for engineering and cultural heritage. J Earth Sci 20(3):626–639CrossRef
Zurück zum Zitat Coussy O (2006) Deformation and stress from in-pore drying-induced crystallization of salt. J Mech Phys Solids 54:1517–1547CrossRef Coussy O (2006) Deformation and stress from in-pore drying-induced crystallization of salt. J Mech Phys Solids 54:1517–1547CrossRef
Zurück zum Zitat Flatt RJ (2002) Salt damage in porous materials: how high supersaturations are generated. J Cryst Growth 242:435–454CrossRef Flatt RJ (2002) Salt damage in porous materials: how high supersaturations are generated. J Cryst Growth 242:435–454CrossRef
Zurück zum Zitat Fortin J, Stanchits S, Dresen G, Gueguen Y (2009) Acoustic emissions monitoring during inelastic deformation of porous sandstone: comparison of three modes of deformation. Pure Appl Geophys 166(5–7):823–841CrossRef Fortin J, Stanchits S, Dresen G, Gueguen Y (2009) Acoustic emissions monitoring during inelastic deformation of porous sandstone: comparison of three modes of deformation. Pure Appl Geophys 166(5–7):823–841CrossRef
Zurück zum Zitat Freyer D, Voigt W (2003) Crystallization and phase stability of CaSO4 and CaSO4-based salts. Monatshefte für Chimie 134:693–719CrossRef Freyer D, Voigt W (2003) Crystallization and phase stability of CaSO4 and CaSO4-based salts. Monatshefte für Chimie 134:693–719CrossRef
Zurück zum Zitat Goudie A, Viles H (1997) Salt weathering hazards. Wiley, London, p 241 Goudie A, Viles H (1997) Salt weathering hazards. Wiley, London, p 241
Zurück zum Zitat Grossi CM, Esbert RM, Suarez del Rio LM, Montoto M, Laurenzi-Tabasso M (1997) Acoustic emission monitoring to study sodium sulphate crystallization in monumental porous carbonate stones. Stud Conserv 42(1997):115–125CrossRef Grossi CM, Esbert RM, Suarez del Rio LM, Montoto M, Laurenzi-Tabasso M (1997) Acoustic emission monitoring to study sodium sulphate crystallization in monumental porous carbonate stones. Stud Conserv 42(1997):115–125CrossRef
Zurück zum Zitat Grossi CM, Brimblecombe P, Harris I (2007) Predicting long term freeze-thaw risk on Europe built heritage and archaeological sites in a changing climate. Sci Total Environ 377:273–281CrossRef Grossi CM, Brimblecombe P, Harris I (2007) Predicting long term freeze-thaw risk on Europe built heritage and archaeological sites in a changing climate. Sci Total Environ 377:273–281CrossRef
Zurück zum Zitat Grossi CM, Brimblecombe P, Menéndez B, Benavente D, Harris I (2008) Long term change in salt weathering of stone monuments in North-West France. In: proceedings of the 11th international conference on deterioration and conservation of stone, Torun Grossi CM, Brimblecombe P, Menéndez B, Benavente D, Harris I (2008) Long term change in salt weathering of stone monuments in North-West France. In: proceedings of the 11th international conference on deterioration and conservation of stone, Torun
Zurück zum Zitat Hammecker C (1995) The importance of the petrophysical properties and external factors in the stone decay on monuments. PAGEOPH 145:338–361CrossRef Hammecker C (1995) The importance of the petrophysical properties and external factors in the stone decay on monuments. PAGEOPH 145:338–361CrossRef
Zurück zum Zitat Koerner RM, McCabe WM, Lord AE (1981) Overview of acoustic emission monitoring of rock structures. Rock Mech 14:27–35CrossRef Koerner RM, McCabe WM, Lord AE (1981) Overview of acoustic emission monitoring of rock structures. Rock Mech 14:27–35CrossRef
Zurück zum Zitat Koerner R, Lord AE (1982) Use of acoustic emissions to predict ground stability. Report No. FHWA/RD-82/085, Federal Highway Administration, U.S. Department of Transportation, Washington, D.C Koerner R, Lord AE (1982) Use of acoustic emissions to predict ground stability. Report No. FHWA/RD-82/085, Federal Highway Administration, U.S. Department of Transportation, Washington, D.C
Zurück zum Zitat La Iglesia A, Gonzalez V, Lopez-Acevedo V, Viedma V (1997) Salt crystallization in porous construction materials. I Estimation of crystallization pressure. J Cryst Growth 177:111–118CrossRef La Iglesia A, Gonzalez V, Lopez-Acevedo V, Viedma V (1997) Salt crystallization in porous construction materials. I Estimation of crystallization pressure. J Cryst Growth 177:111–118CrossRef
Zurück zum Zitat Lefèvre RA, Ausset P (2002) Atmospheric pollution and building materials: stone and glass. In: Siegesmund S, Weiss T, Vollbrecht A (eds) Natural stone, weathering phenomena, conservation strategies and case studies, vol 205. Geological Society, London, special publications, pp 329–345 Lefèvre RA, Ausset P (2002) Atmospheric pollution and building materials: stone and glass. In: Siegesmund S, Weiss T, Vollbrecht A (eds) Natural stone, weathering phenomena, conservation strategies and case studies, vol 205. Geological Society, London, special publications, pp 329–345
Zurück zum Zitat McCabe WM, Koener RM, Lord AE (1979) Acoustic emission (microseismic) monitoring for ground control. In: Maevis AC, Hustrulid WA (eds) Proceedings of the rapid excavation and tunneling conference, Atlanta, GA McCabe WM, Koener RM, Lord AE (1979) Acoustic emission (microseismic) monitoring for ground control. In: Maevis AC, Hustrulid WA (eds) Proceedings of the rapid excavation and tunneling conference, Atlanta, GA
Zurück zum Zitat Menendez B, Grossi CM, Brimblecombe P, Benavente D, Déqué M, Harris I (2010a) Stone weathering predictions based on climate change models in North-West France, (Abstract) cultural heritage and climate change. In: Lefèvre RA, Sabbioni C (eds) Proceedings of the workshop “climate change and cultural heritage”, Ravello, 14–16 Mai 2009, and European master-doctorate course on vulnerability of cultural heritage to climate change, Council of Europe, Strasbourg, Edipuglia Publications, Bari, 7–11 September 2009 Menendez B, Grossi CM, Brimblecombe P, Benavente D, Déqué M, Harris I (2010a) Stone weathering predictions based on climate change models in North-West France, (Abstract) cultural heritage and climate change. In: Lefèvre RA, Sabbioni C (eds) Proceedings of the workshop “climate change and cultural heritage”, Ravello, 14–16 Mai 2009, and European master-doctorate course on vulnerability of cultural heritage to climate change, Council of Europe, Strasbourg, Edipuglia Publications, Bari, 7–11 September 2009
Zurück zum Zitat Menéndez B, David C, Zeitoun E, Candelier Y, Brouzet V (2010b) Using acoustic emission techniques to determine new estimators for salt damage in rocks. CRYSPOM II, Brienz (Switzerland) Menéndez B, David C, Zeitoun E, Candelier Y, Brouzet V (2010b) Using acoustic emission techniques to determine new estimators for salt damage in rocks. CRYSPOM II, Brienz (Switzerland)
Zurück zum Zitat Rivas T, Lamas BP, Silva B (1994) Plaque-shedding by granite in the Monastery of San Martìn Pinario (Santiago de Compostela, NW Spain). In: 3rd International symposium: the conservation of monuments in the mediterranean basin, Venice, pp 737–741 Rivas T, Lamas BP, Silva B (1994) Plaque-shedding by granite in the Monastery of San Martìn Pinario (Santiago de Compostela, NW Spain). In: 3rd International symposium: the conservation of monuments in the mediterranean basin, Venice, pp 737–741
Zurück zum Zitat Rodriguez-Navarro C, Doehne E, Sebastian E (2000) How does sodium sulfate crystallize? Implications for the decay and testing of building material. Cem Concr Res 30:1527–1534CrossRef Rodriguez-Navarro C, Doehne E, Sebastian E (2000) How does sodium sulfate crystallize? Implications for the decay and testing of building material. Cem Concr Res 30:1527–1534CrossRef
Zurück zum Zitat Ruiz-Agudo E, Mees F, Jacobs P, Rodriguez-Navarro C (2007) The role of saline solution properties on porous limestone salt weathering by magnesium and sodium sulfates. Environ Geol 52:269–281CrossRef Ruiz-Agudo E, Mees F, Jacobs P, Rodriguez-Navarro C (2007) The role of saline solution properties on porous limestone salt weathering by magnesium and sodium sulfates. Environ Geol 52:269–281CrossRef
Zurück zum Zitat Sabbioni C, Cassar M, Brimblecombe P, Tidblaud J, Kozlowski R, Drdacky M, Saiz-Jumenez C, Grontoft T, Wainwright I, Arino X (2004) Global climate change impact on built heritage and cultural landscapes. In: 6th European commission conference on sustaining Europe’s cultural heritage. Research to Policy, London, September 2004 Sabbioni C, Cassar M, Brimblecombe P, Tidblaud J, Kozlowski R, Drdacky M, Saiz-Jumenez C, Grontoft T, Wainwright I, Arino X (2004) Global climate change impact on built heritage and cultural landscapes. In: 6th European commission conference on sustaining Europe’s cultural heritage. Research to Policy, London, September 2004
Zurück zum Zitat Sabbioni C, Cassar M, Brimblecombe P, Tidblaud J, Kozlowski R, Drdacky M, Saiz-Jumenez C, Grontoft T, Wainwright I, Arino X (2006) Global climate change impact on built heritage and cultural landscapes. In: Fort R, Anvarez de Buergo M, Gimez-Heras M, Vazquez-Calvo C (eds) Heritage, weathering and conservation. Taylor and Francis Group, London, pp 395–401 Sabbioni C, Cassar M, Brimblecombe P, Tidblaud J, Kozlowski R, Drdacky M, Saiz-Jumenez C, Grontoft T, Wainwright I, Arino X (2006) Global climate change impact on built heritage and cultural landscapes. In: Fort R, Anvarez de Buergo M, Gimez-Heras M, Vazquez-Calvo C (eds) Heritage, weathering and conservation. Taylor and Francis Group, London, pp 395–401
Zurück zum Zitat Sanjurjo Sanchez J, Alves CAS, Vidal Romani JR, Fernandez Mosquera D (2009) Origin of gypsum-rich coatings on historic buildings. Water Air Soil Pollut 204:53–68CrossRef Sanjurjo Sanchez J, Alves CAS, Vidal Romani JR, Fernandez Mosquera D (2009) Origin of gypsum-rich coatings on historic buildings. Water Air Soil Pollut 204:53–68CrossRef
Zurück zum Zitat Scherer GW (1999) Crystallization in pores. Cem Concr Res 29:1347–1358CrossRef Scherer GW (1999) Crystallization in pores. Cem Concr Res 29:1347–1358CrossRef
Zurück zum Zitat Scherer GW (2004) Stress from crystallization of salt. Cem Concr Res 34:1613–1624CrossRef Scherer GW (2004) Stress from crystallization of salt. Cem Concr Res 34:1613–1624CrossRef
Zurück zum Zitat Siegesmund S, Török A, Hüpers A, Müller C, Klemm W (2007) Mineralogical, geochemical and microfabric evidences of gypsum crust: a case study from Budapest. Environ Geol 52:385–397CrossRef Siegesmund S, Török A, Hüpers A, Müller C, Klemm W (2007) Mineralogical, geochemical and microfabric evidences of gypsum crust: a case study from Budapest. Environ Geol 52:385–397CrossRef
Zurück zum Zitat Silva Hermo B, Prieto Lamas B, Rivas Brea T, Pereira Pardo L (2010) Gypsum-induced decay in granite monuments in Northwestern Spain. Materiales de Construcción 60:97–110CrossRef Silva Hermo B, Prieto Lamas B, Rivas Brea T, Pereira Pardo L (2010) Gypsum-induced decay in granite monuments in Northwestern Spain. Materiales de Construcción 60:97–110CrossRef
Zurück zum Zitat Steiger M (2005a) Crystal growth in porous materials. I: the crystallization pressure of large crystal. J Cryst Growth 282:455–469CrossRef Steiger M (2005a) Crystal growth in porous materials. I: the crystallization pressure of large crystal. J Cryst Growth 282:455–469CrossRef
Zurück zum Zitat Steiger M (2005b) Crystal growth in porous materials. II Influence of crystal size on the crystallization pressure. J Cryst Growth 282:470–481CrossRef Steiger M (2005b) Crystal growth in porous materials. II Influence of crystal size on the crystallization pressure. J Cryst Growth 282:470–481CrossRef
Zurück zum Zitat Suarez del Río LM (1982) Estudio petrofísico de materiales graníticos geomecánicamente diferentes. Tesis Doctoral. Facultad de Geología, Universidad de Oviedo (España) Suarez del Río LM (1982) Estudio petrofísico de materiales graníticos geomecánicamente diferentes. Tesis Doctoral. Facultad de Geología, Universidad de Oviedo (España)
Zurück zum Zitat Thaulow N, Sahu S (2004) Mechanism of concrete deterioration due to salt crystallization. Mater Charact 53:123–127CrossRef Thaulow N, Sahu S (2004) Mechanism of concrete deterioration due to salt crystallization. Mater Charact 53:123–127CrossRef
Zurück zum Zitat Turkington AV, Paradise TR (2005) Sandstone weathering: a century of research and innovation. Geomorphology 67:229–253CrossRef Turkington AV, Paradise TR (2005) Sandstone weathering: a century of research and innovation. Geomorphology 67:229–253CrossRef
Zurück zum Zitat Vallet JM, Gosselin C, Bromblet P, Rolland O, Vergès-Belmin V, Kloppmann W (2006) Origin of salt in monuments degradation using sulphur and oxygen isotopes: first results of the Bourges cathedral (France). J Geochem Explor 88:58–362CrossRef Vallet JM, Gosselin C, Bromblet P, Rolland O, Vergès-Belmin V, Kloppmann W (2006) Origin of salt in monuments degradation using sulphur and oxygen isotopes: first results of the Bourges cathedral (France). J Geochem Explor 88:58–362CrossRef
Zurück zum Zitat Vil’yaminov SV, Voznesensky AS, Nabatov VV, Shkuratnik VL (2009) Regularities and mechanisms of thermal acoustic emission in gypseous rocks. J Min Sci 45(6):533–540CrossRef Vil’yaminov SV, Voznesensky AS, Nabatov VV, Shkuratnik VL (2009) Regularities and mechanisms of thermal acoustic emission in gypseous rocks. J Min Sci 45(6):533–540CrossRef
Zurück zum Zitat Viles HA (2005) Implications of future climate change for stone deterioration. In: Weiss T, Volbrecht A (eds) Natural stone, weathering phenomena, conservation strategies and case studies. Geological Society, London, special publication, pp 407–418 Viles HA (2005) Implications of future climate change for stone deterioration. In: Weiss T, Volbrecht A (eds) Natural stone, weathering phenomena, conservation strategies and case studies. Geological Society, London, special publication, pp 407–418
Zurück zum Zitat Winkler EM (1994) Stone in architecture, properties and durability, 3rd review and extended edition. Springer, New York Winkler EM (1994) Stone in architecture, properties and durability, 3rd review and extended edition. Springer, New York
Zurück zum Zitat Winkler EM, Singer PC (1972) Crystallization pressure of salts in stone and concrete. Geol Soc Am Bull 83(11):3509–35013CrossRef Winkler EM, Singer PC (1972) Crystallization pressure of salts in stone and concrete. Geol Soc Am Bull 83(11):3509–35013CrossRef
Zurück zum Zitat Zang A, Wagner CF, Dresen G (1996) Acoustic emission, microstructure, and damage model of dry and wet sandstone stressed to failure. J Geophys Res Solid Earth 101(B8):17507–17521CrossRef Zang A, Wagner CF, Dresen G (1996) Acoustic emission, microstructure, and damage model of dry and wet sandstone stressed to failure. J Geophys Res Solid Earth 101(B8):17507–17521CrossRef
Metadaten
Titel
The influence of environmental conditions on weathering of porous rocks by gypsum: a non-destructive study using acoustic emissions
verfasst von
Beatriz Menéndez
Christian David
Publikationsdatum
01.03.2013
Verlag
Springer-Verlag
Erschienen in
Environmental Earth Sciences / Ausgabe 6/2013
Print ISSN: 1866-6280
Elektronische ISSN: 1866-6299
DOI
https://doi.org/10.1007/s12665-012-1861-2

Weitere Artikel der Ausgabe 6/2013

Environmental Earth Sciences 6/2013 Zur Ausgabe