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Erschienen in: Journal of Materials Science: Materials in Electronics 8/2019

12.03.2019

The low frequency relaxor properties of ferroelectric PZT-4 studied by DMA

verfasst von: Yun Chen, Xusheng Wang, Yanxia Li, Xi Yao

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 8/2019

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Abstract

Relaxation makes ferroelectrics a critical component in sensors, actuators and ultrasound devices, with large electromechanical coupling effects. Although various studies of ferroelectric relaxation have been undertaken, much remains to be investigated regarding the related the properties and mechanisms, with limited studies involving low frequency relaxation characteristics. In this study, an alternative mechanical method using a dynamic mechanical analyzer (DMA) was applied to investigate the low frequency relaxor behavior of PZT-4 ceramics, compared with conventional electric method. Ferroelectric to paraelectric phase transitions were clearly detected and an obvious low frequency relaxor behavior was characterized, induced by Debye relaxation. Then, the activation energy of each relaxation peak and relaxation limit time was theoretically analyzed using the Arrhenius relationship. In addition, the switching of 90° domains was shown to be responsible for relaxor behavior. In contrast, no low frequency relaxor behavior was detected by dielectric measurements, which meant that the mechanical method was more sensitive to internal structural changes. This study deepened the current knowledge on relaxor ferroelectrics, and offered the potential for provide new insights into the investigation of low frequency relaxor characterization.

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Metadaten
Titel
The low frequency relaxor properties of ferroelectric PZT-4 studied by DMA
verfasst von
Yun Chen
Xusheng Wang
Yanxia Li
Xi Yao
Publikationsdatum
12.03.2019
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 8/2019
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-019-01085-7

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