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Journal of Sol-Gel Science and Technology
Erschienen in: Journal of Sol-Gel Science and Technology 1/2020

17.05.2020 | Original Paper: Nano-structured materials (particles, fibers, colloids, composites, etc.)

The possibility of vanadium substitution on Co lattice sites in CoFe2O4 synthesized by sol–gel autocombustion method

verfasst von: Parvin Imanipour, Saeed Hasani, Amir Seifoddini, Atefeh Farnia, Fatemeh Karimabadi, Khadijeh Jahanbani-Ardakani, Fatemeh Davar

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 1/2020

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Abstract

In this study, the effect of vanadium addition on the structural and magnetic properties of cobalt ferrite (Co1−xVxFe2O4; where x = 0, 0.05, 0.10, 0.15, 0.20, and 0.25) prepared by a novel sol–gel autocombustion method was investigated. The formation of cubic spinel structure (space group Fd3m) was confirmed by X-ray diffraction in combination of Rietveld structure refinement analysis and transform infrared spectroscopic spectrum (FT-IR) analyses. Also, phase and elemental analyses confirmed that an inevitable secondary phase of hematite along with the spinel phase appears by addition of vanadium; therefore, a nanocomposite was formed in the sample containing vanadium. However, the SEM observations in combination of the results obtained by Rietveld structure refinement analysis showed that the presence of vanadium can affect the size of synthesized cobalt ferrite. VSM measurements showed that saturation magnetization and coercivity values are strongly dependent on the vanadium content and particle size, so that the maximum value of coercivity was obtained equal to ~916 Oe for Co0.85V0.15Fe2O4.
Vorheriger Artikel Effect of temperature and reaction time during solvothermal synthesis of BiOCl on microspheres formation: implications in the photocatalytic oxidation of gallic acid under simulated solar radiation
Nächster Artikel Hydroxyapatite scaffolds containing copper for bone tissue engineering

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Metadaten
Titel
The possibility of vanadium substitution on Co lattice sites in CoFe2O4 synthesized by sol–gel autocombustion method
verfasst von
Parvin Imanipour
Saeed Hasani
Amir Seifoddini
Atefeh Farnia
Fatemeh Karimabadi
Khadijeh Jahanbani-Ardakani
Fatemeh Davar
Publikationsdatum
17.05.2020
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 1/2020
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-020-05316-w

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