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Journal of Materials Engineering and Performance
Erschienen in:

26.10.2022 | Technical Article

The Synthesis and Crystal Phase Evolution of SiO2-Stabilized Zirconia Nanocomposites at Low Temperatures for the Production of Zircon

verfasst von: Sepide Akbarpour, Behnam Khoshandam, Samane Maroufi

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 14/2023

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Abstract

The aims of this paper were to reduce the operating temperature of SiO2-stabilized zirconia synthesis compared to previous works and produce a practical ZrSiO4 ceramic by the solution combustion method. The analysis of DSC, XRD, FTIR, FE-SEM, TEM, SAED, HR-TEM and Rietveld refinement were used to characterize the resulting products. The results demonstrated that the type and amount of fuels (i.e., urea and glycine) were important factors in self-sustained reaction and crystalline structures of zirconia. A comparison was also done to study the impact of the calcination temperature on the phase evolution of stabilized monoclinic zirconia, obtained 96.67% of m-ZrO2 with crystallite size of 31 nm. Finally, sintering process of m-ZrO2 was applied to synthesize ZrSiO4. The crystallization of ZrSiO4 from the binary system of m-ZrO2 and SiO2 has been the subject of extensive study, commonly obtained with cations at high temperatures. Interestingly, the present study achieved ZrSiO4 without the presence of cation at low temperature, and indicated 79.51% purity with compressive strength and Vickers hardness of 416.38 ± 6.79 MPa and 1143.2 ± 40.2 HV (11.21 ± 0.39 GPa), respectively. Due to appropriate appearance color and excellent mechanical properties of ZrSiO4 synthesized at low-temperature processing, this approach can be promising for the biomedical application.

Graphical Abstract

Vorheriger Artikel Investigation of Mechanical Properties and Corrosion Behavior of Three-Layered Brass/Interstitial Free Steel/Brass Composite Manufactured through Cold Roll Bonding Process
Nächster Artikel Effect of Gamma Radiation on the Electrochemical Behavior of AISI 8620 Steel Coated with Diamond-Like Carbon

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Metadaten
Titel
The Synthesis and Crystal Phase Evolution of SiO2-Stabilized Zirconia Nanocomposites at Low Temperatures for the Production of Zircon
verfasst von
Sepide Akbarpour
Behnam Khoshandam
Samane Maroufi
Publikationsdatum
26.10.2022
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 14/2023
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-022-07554-1

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